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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

3,8-Dibromophenanthroline

Cas:100125-12-0

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 3,8-Dibromo-[1,10]Phenanthroline supplier in China

Cas:100125-12-0

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 3,8-Dibromo-[1,10]Phenanthroline

Cas:100125-12-0

Min.Order:1

Negotiable

Type:Other

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Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Factory Price OLED 99% 100125-12-0 3,8-Dibromophenanthroline Manufacturer

Cas:100125-12-0

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

3,8-Dibromo[1,10]phenanthroline

Cas:100125-12-0

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

Competitive Price High Quality Fast Delivery custom-made Welcome to Henan Tianfu Chemical Co., Ltd. website. Our company engages in Sodium Tripolyphosphate (STPP) and Sodium Hexametabphosphate (SHMP) production; development of noble me

3,8-Dibromophenanthroline 100125-12-0

Cas:100125-12-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

3,8-Dibromophenanthroline

Cas:100125-12-0

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supply CAS 100125-12-0 with best quality

Cas:100125-12-0

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Name: 3,8-Dibromo-1,10-phenanthroline Synonyms: 3,8-Dibromophenanthroline CAS:100125-12-0 MF: C12H6Br2N2 Appearance:White powder Storage:Store in cool and dry place, away from sun light. Package:25kg Application:OLED organic electroluminescence ma

3,8-Dibromo-1,10-phenanthroline

Cas:100125-12-0

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

1,10-Phenanthroline,3,8-dibromo- 100125-12-0

Cas:100125-12-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Shanghai Minstar Chemical Co., Ltd

Product Name: 3,8-Dibromophenanthroline CAS: 100125-12-0 MF: C12H6Br2N2 MW: 338 EINECS: 1308068-626-2 Mol File: 100125-12-0.mol 3,8-Dibromophenanthroline Structure 3,8-Dibromophenanthroline Chemical Properties Melting point 22

3,8-Dibromophenanthroline

Cas:100125-12-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Qingdao Beluga Import and Export Co., LTD

3,8-Dibromophenanthroline CAS:100125-12-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organi

3,8-Dibromophenanthroline CAS:100125-12-0

Cas:100125-12-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

1,10-Phenanthroline,3,8-dibromo-

Cas:100125-12-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s

3,8-Dibromophenanthroline

Cas:100125-12-0

Min.Order:1 Kilogram

FOB Price: $80.0 / 100.0

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

1,10-Phenanthroline,3,8-dibromo-

Cas:100125-12-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

3,8-Dibromo-1,10-Phenanthroline

Cas:100125-12-0

Min.Order:0

Negotiable

Type:Manufacturers

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

3,8-Dibromo-[1,10]phenanthroline

Cas:100125-12-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality 3,8-Dibromo-[1,10]Phenanthroline

Cas:100125-12-0

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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Hunan chemfish Pharmaceutical co.,Ltd

Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as

3,?8-?dibromo-1,?10-?Phenanthroline

Cas:100125-12-0

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

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HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:white powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:10g/bag,or as your request Application:Used as Pharmaceutical Intermediates Transporta

3,8-Dibromophenanthroline

Cas:100125-12-0

Min.Order:1 Gram

Negotiable

Type:Trading Company

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

3,8-Dibromophenanthroline

Cas:100125-12-0

Min.Order:1 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

3,8-Dibromophenanthroline

Cas:100125-12-0

Min.Order:1 Milligram

Negotiable

Type:Trading Company

inquiry

TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

3,8-Dibromophenanthroline

Cas:100125-12-0

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

Hangzhou Zhongqi chem Co.,Ltd.

Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and h

1,10-Phenanthroline,3,8-dibromo-

Cas:100125-12-0

Min.Order:0

Negotiable

Type:Other

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Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

3,8-Dibromophenanthroline

Cas:100125-12-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

3,8-Dibromo-1,10-phenanthroline cas no. 100125-12-0 98%

Cas:100125-12-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

3,8-Dibromophenanthroline

Cas:100125-12-0

Min.Order:0

Negotiable

Type:Other

inquiry

Lonwin Chemical Group Limited

Shanghai Lonwin Chemical company is a subsidiary of Lonwin Industry Group Limited, was established in 2011 and is headquartered in Shanghai, adjacent to China National Convention and Exhibition Center and Hongqiao transportation hub.Lonwinchem is

Best price 3,8-Dibromo-[1,10]Phenanthroline 100125-12-0

Cas:100125-12-0

Min.Order:100 Kilogram

FOB Price: $100.0 / 150.0

Type:Other

inquiry

GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier

3,8-Dibromo-[1,10]phenanthroline

Cas:100125-12-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

JINHUA HUAYI CHEMICAL CO., LTD.

Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands

3,8-Dibromo-[1,10]Phenanthrolin

Cas:100125-12-0

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

1,10-Phenanthroline
66-71-7

1,10-Phenanthroline

3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

Conditions
ConditionsYield
With pyridine; disulfur dichloride; bromine In various solvent(s) at 78℃; for 12h;75%
With pyridine; thiothionyl chloride; n-Butyl chloride; bromine for 24h; Reflux;70%
With pyridine; disulfur dichloride; bromine In water64%
1,10-Phenanthroline
66-71-7

1,10-Phenanthroline

A

3-bromophenanthroline
66127-01-3

3-bromophenanthroline

B

3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

Conditions
ConditionsYield
With bromine In nitrobenzeneA 38%
B 60%
1,10-phenanthroline hydrochloride
3829-86-5

1,10-phenanthroline hydrochloride

A

3-bromophenanthroline
66127-01-3

3-bromophenanthroline

B

3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

Conditions
ConditionsYield
With bromine In nitrobenzene at 130 - 140℃; for 3h;A 33%
B 17%
With water; bromine In nitrobenzene
With bromine In bromobenzene at 135℃; for 36h;
3-bromo-8-aminoquinoline
139399-67-0

3-bromo-8-aminoquinoline

3,3-diacetoxy-2-bromo-propene
408529-03-3

3,3-diacetoxy-2-bromo-propene

3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

Conditions
ConditionsYield
With phosphoric acid; orthoarsenic acid
3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

trimethylsilylacetylene
1066-54-2

trimethylsilylacetylene

3,8-bis(trimethylsilanylethynyl)-[1,10]phenanthroline
320573-10-2

3,8-bis(trimethylsilanylethynyl)-[1,10]phenanthroline

Conditions
ConditionsYield
With copper(l) iodide; N-ethyl-N,N-diisopropylamine; bis-triphenylphosphine-palladium(II) chloride In benzene at 95℃; for 40h; Sonogashira coupling;100%
With copper(l) iodide; diisopropylamine; bis-triphenylphosphine-palladium(II) chloride In tetrahydrofuran at 20℃; Sonogashira coupling reaction;90%
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine In tetrahydrofuran at 60℃; under 2068.59 Torr; for 6h;88%
potassium hexafluorophosphate
17084-13-8

potassium hexafluorophosphate

cis-bis-(2,2′-bipyridine) dichlororuthenium(II) dihydrate

cis-bis-(2,2′-bipyridine) dichlororuthenium(II) dihydrate

3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

[Ru(bpy)(3,8-dibromo-1,10-phenanthroline)](PF6)2

[Ru(bpy)(3,8-dibromo-1,10-phenanthroline)](PF6)2

Conditions
ConditionsYield
Stage #1: cis-bis-(2,2′-bipyridine) dichlororuthenium(II) dihydrate; 3,8-dibromo-1,10-phenathroline In methanol for 16h; Reflux;
Stage #2: potassium hexafluorophosphate In methanol; water at 4℃; for 16h;
100%
2,2'-p-[2,5-bis(dodecyloxy)-1,4-phenylene]bis(5,5-dimethyl-1,3,2-dioxaborinane)

2,2'-p-[2,5-bis(dodecyloxy)-1,4-phenylene]bis(5,5-dimethyl-1,3,2-dioxaborinane)

3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

polymer, Mn 7000 Da, Mw/Mn 2.0; monomer(s): 3,8-dibromo-1,10-phenanthroline; 2,2-[2,5-bis(dodecyloxy)-1,4-phenylene]bis(5,5-dimethyl-1,3,2-dioxaborinane)

polymer, Mn 7000 Da, Mw/Mn 2.0; monomer(s): 3,8-dibromo-1,10-phenanthroline; 2,2-[2,5-bis(dodecyloxy)-1,4-phenylene]bis(5,5-dimethyl-1,3,2-dioxaborinane)

Conditions
ConditionsYield
With base; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran; water at 60℃; Suzuki reaction;97%
3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

3,5-bis-trifluromethylphenylboronic acid
73852-19-4

3,5-bis-trifluromethylphenylboronic acid

3,8-bis[(3,5-bis(trifluoromethyl))phenyl]-1,10-phenanthroline
1228032-35-6

3,8-bis[(3,5-bis(trifluoromethyl))phenyl]-1,10-phenanthroline

Conditions
ConditionsYield
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate In tetrahydrofuran; water at 80℃; Suzuki cross-coupling; Inert atmosphere;95%
Stage #1: 3,8-dibromo-1,10-phenathroline; 3,5-bis-trifluromethylphenylboronic acid With potassium carbonate In 1,4-dioxane; water Suzuki Coupling; Inert atmosphere; Glovebox;
Stage #2: With palladium diacetate; tricyclohexylphosphine In 1,4-dioxane; water for 17h; Suzuki Coupling; Reflux;
91%
2-bromothiophene
1003-09-4

2-bromothiophene

3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

3,8-bis(thiophen-2',2"-yl)-1,10-phenanthroline

3,8-bis(thiophen-2',2"-yl)-1,10-phenanthroline

Conditions
ConditionsYield
Stage #1: 2-bromothiophene With magnesium In tetrahydrofuran at 20℃; for 2h;
Stage #2: 3,8-dibromo-1,10-phenathroline; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II) In tetrahydrofuran for 14h;
94%
3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

2-(4-(5,5-dimethyl-1,3-dioxan-2-yl)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
305344-39-2

2-(4-(5,5-dimethyl-1,3-dioxan-2-yl)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

3,8-di[p-(5,5-dimethyl-1,3-dioxan-2-yl)]phenyl-1,10-phenanthroline

3,8-di[p-(5,5-dimethyl-1,3-dioxan-2-yl)]phenyl-1,10-phenanthroline

Conditions
ConditionsYield
With barium dihydroxide; tetrakis(triphenylphosphine) palladium(0) In water; toluene for 48h; Suzuki cross-coupling; Heating;92%
3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

3,8-dibromo-5,6-dihydro-1,10-phenanthroline-5,6-dione
602331-25-9

3,8-dibromo-5,6-dihydro-1,10-phenanthroline-5,6-dione

Conditions
ConditionsYield
With sulfuric acid; nitric acid; potassium bromide at 130℃; for 3h;92%
With sulfuric acid; nitric acid; potassium bromide for 3h; Heating;91.6%
Stage #1: 3,8-dibromo-1,10-phenathroline With sulfuric acid; nitric acid; potassium bromide at 0 - 110℃; for 3h;
Stage #2: With sodium hydroxide In water pH=7; Temperature; Cooling with ice;
90%
ammonium hexafluorophosphate

ammonium hexafluorophosphate

3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

bis(4,4'-di-tert-butyl-2,2'-bipyridine)-ruthenium(II)-dichloride

bis(4,4'-di-tert-butyl-2,2'-bipyridine)-ruthenium(II)-dichloride

bis(4,4'-di-tert-butyl-2,2'-bipyridine)(3,8-dibromo-1,10-phenanthroline)ruthenium(II) hexafluorophosphate

bis(4,4'-di-tert-butyl-2,2'-bipyridine)(3,8-dibromo-1,10-phenanthroline)ruthenium(II) hexafluorophosphate

Conditions
ConditionsYield
In ethanol; water other Radiation; (Ar or N2), Ru complex and ligand (1:1) suspnd. on EtOH/H2O 5:3 v/v, refluxed for 2 h under microwave irradiation, cooled to room temp., filtered, concd., pptd. with aq.NH4PF6; filtered, washed (h2O, EtOH, Et2O), dried (air);91%
3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

phenylacetylene
536-74-3

phenylacetylene

3,8-bis(phenylacetylene)-1,10-phenanthroline
168003-69-8

3,8-bis(phenylacetylene)-1,10-phenanthroline

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine In methanol for 4h; Ambient temperature;90%
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine In methanol at 40 - 50℃; Sonogashira cross-coupling; Inert atmosphere; Sonication;81%
methanol
67-56-1

methanol

3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

3,8-dimethoxy-1,10-phenanthroline

3,8-dimethoxy-1,10-phenanthroline

Conditions
ConditionsYield
Stage #1: methanol With sodium hydride for 0.75h; Heating;
Stage #2: 3,8-dibromo-1,10-phenathroline In N,N-dimethyl-formamide at 50℃; for 15h;
90%
copper(II) choride dihydrate

copper(II) choride dihydrate

3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

(S,S)-1,2-diaminocyclohexane
21436-03-3

(S,S)-1,2-diaminocyclohexane

potassium perchlorate

potassium perchlorate

[copper(II)((1S,2S)-diaminocyclohexane)(3,8-dibromo-1,10-phenanthroline)](perchlorate) monohydrate

[copper(II)((1S,2S)-diaminocyclohexane)(3,8-dibromo-1,10-phenanthroline)](perchlorate) monohydrate

Conditions
ConditionsYield
In ethanol; water at 60℃; for 3.5h;90%
[iridium(III)(μ-chloro)(2-phenylpyridine)2]2

[iridium(III)(μ-chloro)(2-phenylpyridine)2]2

3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

C34H22Br2IrN4(1+)*Cl(1-)

C34H22Br2IrN4(1+)*Cl(1-)

Conditions
ConditionsYield
In methanol; dichloromethane for 6h; Reflux;90%
In methanol; dichloromethane for 6h; Reflux;70%
3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

potassium vinyltrifluoroborate

potassium vinyltrifluoroborate

3,8-divinyl-1,10-phenanthroline

3,8-divinyl-1,10-phenanthroline

Conditions
ConditionsYield
With potassium phosphate; tetrakis(triphenylphosphine) palladium(0) In 1,4-dioxane; water for 48h; Inert atmosphere; Reflux;90%
3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

4-methoxyphenylacetylen
768-60-5

4-methoxyphenylacetylen

3,8-di(4-methoxyphenylethynyl)-1,10-phenanthroline
168003-71-2

3,8-di(4-methoxyphenylethynyl)-1,10-phenanthroline

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine In methanol for 4h; Ambient temperature;89%
3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

3,4,5-trimethoxyphenylboronic Acid
182163-96-8

3,4,5-trimethoxyphenylboronic Acid

3,8-bis(3,4,5-tris(methoxy)phenyl)-1,10-phenanthroline

3,8-bis(3,4,5-tris(methoxy)phenyl)-1,10-phenanthroline

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In tetrahydrofuran; ethanol; water for 18h; Suzuki Coupling; Inert atmosphere; Reflux;88%
3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

4-n-methylphenylacetylene
766-97-2

4-n-methylphenylacetylene

3,8-Bis-p-tolylethynyl-[1,10]phenanthroline

3,8-Bis-p-tolylethynyl-[1,10]phenanthroline

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine In methanol for 4h; Ambient temperature;87%
3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

2-bromo-1-(trimethylsilylethynyl)benzene
38274-16-7

2-bromo-1-(trimethylsilylethynyl)benzene

3,8-bis-(2-trimethylsilanylethynyl-phenyl)-[1,10]phenanthroline
503809-92-5

3,8-bis-(2-trimethylsilanylethynyl-phenyl)-[1,10]phenanthroline

Conditions
ConditionsYield
Stage #1: 2-bromo-1-(trimethylsilylethynyl)benzene With n-butyllithium In tetrahydrofuran at -78℃;
Stage #2: 3,8-dibromo-1,10-phenathroline With tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran; N,N-dimethyl-formamide for 72h; Heating;
87%
tetrakis(acetonitrile)copper(I) perchlorate
14057-91-1

tetrakis(acetonitrile)copper(I) perchlorate

3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

dichloromethane
75-09-2

dichloromethane

4,5-bis(diphenylphosphino)-9,9-dimethylxanthene
161265-03-8

4,5-bis(diphenylphosphino)-9,9-dimethylxanthene

[Cu(3,8-dibromo-1,10-phenanthroline)(9,9-dimethyl-4,5-bis(diphenylphosphino)-9H-xanthene)]ClO4*2CH2Cl2

[Cu(3,8-dibromo-1,10-phenanthroline)(9,9-dimethyl-4,5-bis(diphenylphosphino)-9H-xanthene)]ClO4*2CH2Cl2

Conditions
ConditionsYield
at 20℃; for 5h; Inert atmosphere; Schlenk technique;86.1%
3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

C25H20N2

C25H20N2

C62H44N6

C62H44N6

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene at 110℃; Inert atmosphere;85%
3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

C25H20N2

C25H20N2

C62H44N6

C62H44N6

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene at 110 - 120℃; Inert atmosphere;85%
3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

C25H20N2

C25H20N2

C62H44N6

C62H44N6

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene at 110 - 120℃; Inert atmosphere;85%
3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

C25H20N2

C25H20N2

C62H44N6

C62H44N6

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene at 110 - 120℃; Inert atmosphere;85%
3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

ethylene dibromide
106-93-4

ethylene dibromide

N,N'-ethyl-3,8-dibromo-1,10-phenanthrolinium dibromide

N,N'-ethyl-3,8-dibromo-1,10-phenanthrolinium dibromide

Conditions
ConditionsYield
at 100℃; for 48h; Autoclave;85%
3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

2-(4-methoxyphenyl)-5,5-dimethyl-1,3,2-dioxaborolane
213596-33-9

2-(4-methoxyphenyl)-5,5-dimethyl-1,3,2-dioxaborolane

3,8-bis-(4-methoxyphenyl)-1,10-phenanthroline
209795-84-6

3,8-bis-(4-methoxyphenyl)-1,10-phenanthroline

Conditions
ConditionsYield
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In toluene at 80℃; for 12h;84%
3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

4-methoxyphenylboronic acid
5720-07-0

4-methoxyphenylboronic acid

3,8-bis-(4-methoxyphenyl)-1,10-phenanthroline
209795-84-6

3,8-bis-(4-methoxyphenyl)-1,10-phenanthroline

Conditions
ConditionsYield
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In methanol; toluene for 24h; Suzuki cross-coupling; Heating;84%
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In ethanol; water; toluene at 80℃; for 12h; Inert atmosphere;78%
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In tetrahydrofuran; ethanol; water for 18h; Suzuki Coupling; Inert atmosphere; Reflux;75%
2,7-bis(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-9,9-dioctylfluorene

2,7-bis(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-9,9-dioctylfluorene

3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

polymer, Mn 6700 Da, Mw/Mn 1.8; monomer(s): 3,8-dibromo-1,10-phenanthroline; 2,2\-(9,9-dioctyl-9H-fluorene-2,7-diyl)bis(5,5-dimethyl-1,3,2-dioxaborinane)

polymer, Mn 6700 Da, Mw/Mn 1.8; monomer(s): 3,8-dibromo-1,10-phenanthroline; 2,2\-(9,9-dioctyl-9H-fluorene-2,7-diyl)bis(5,5-dimethyl-1,3,2-dioxaborinane)

Conditions
ConditionsYield
With base; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran; water at 60℃; Suzuki reaction;84%
2-{9,9-bis[6-(N-carbazolyl)hexyl]fluoren-2-yl}[1,3,2]dioxaborolane
1032392-75-8

2-{9,9-bis[6-(N-carbazolyl)hexyl]fluoren-2-yl}[1,3,2]dioxaborolane

3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

3,8-bis(9,9-bis(6-(9H-carbazol-9-yl)hexyl)-9H-fluoren-2-yl)-1,10-phenanthroline
1032392-82-7

3,8-bis(9,9-bis(6-(9H-carbazol-9-yl)hexyl)-9H-fluoren-2-yl)-1,10-phenanthroline

Conditions
ConditionsYield
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran; toluene at 88℃; for 48h; Susuki-Miyaura cross-coupling reaction;84%
3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

3,3'-bis(hydroxycarbonyl)-2,2'-bipyridine
4433-01-6

3,3'-bis(hydroxycarbonyl)-2,2'-bipyridine

cobalt(II) diacetate tetrahydrate
6147-53-1

cobalt(II) diacetate tetrahydrate

C28H20Br2CoN4O8
1460349-93-2

C28H20Br2CoN4O8

Conditions
ConditionsYield
With sodium hydroxide In tetrahydrofuran; methanol; water for 6h; Reflux;83%
2-bromo-3-methylthiophene
14282-76-9

2-bromo-3-methylthiophene

3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

3,8-di(3-methylthiophen-2-yl)-1,10-phenanthroline
1083197-15-2

3,8-di(3-methylthiophen-2-yl)-1,10-phenanthroline

Conditions
ConditionsYield
Stage #1: 2-bromo-3-methylthiophene With iodine; magnesium In tetrahydrofuran at 20℃; Inert atmosphere; Reflux;
Stage #2: 3,8-dibromo-1,10-phenathroline With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II) In tetrahydrofuran at 20℃; for 14h; Kumada-Corriu coupling reaction; Inert atmosphere; Reflux;
82.3%
fluoranthene-8-ylboronic acid
401813-32-9

fluoranthene-8-ylboronic acid

3,8-dibromo-1,10-phenathroline
100125-12-0

3,8-dibromo-1,10-phenathroline

C44H24N2
676542-62-4

C44H24N2

Conditions
ConditionsYield
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In ethanol; water; toluene at 20 - 77℃; for 3.5h;82%

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