Conditions | Yield |
---|---|
With H3PO4-activated and WOx-loaded montmorillonite nanocatalyst In water at 320℃; for 3h; Reagent/catalyst; Flow reactor; | A n/a B n/a C 67.3% |
With phosphorus containing Fe2O3 nanoparticles In water at 320℃; for 24h; Inert atmosphere; | |
With 10 w% WO3/ZrO2 at 250℃; Temperature; Time; Inert atmosphere; | |
With HZSM5/Fe/Rb In water at 340℃; under 760.051 Torr; Inert atmosphere; | |
With oxygen In water at 285℃; under 760.051 Torr; for 1h; Flow reactor; | A 10.65 %Chromat. B 19.63 %Chromat. C 57.96 %Chromat. |
Conditions | Yield |
---|---|
With piperazine; hydrogen In ethanol at 80℃; under 4500.45 Torr; for 24h; | 99% |
With hydrogen In methanol at 20℃; under 760.051 Torr; for 4.5h; Green chemistry; | 98% |
With hydrogen In methanol under 760.051 Torr; for 5h; | 97% |
Conditions | Yield |
---|---|
With hydrogen In water at 110℃; under 22502.3 Torr; for 2.33333h; Reagent/catalyst; Pressure; Temperature; | 96% |
With sulfuric acid; zinc diacetate; iron(II) sulfate at 25℃; bei der elektrolytischen Reduktion an einer amalgamierten Bleikathode; Reagens 4: Hydrochinon; | |
With aluminum isopropoxide; isopropyl alcohol |
Conditions | Yield |
---|---|
With trans-[(2,6-bis(di-tert-butylphosphinomethyl)pyridine)Fe(H)2(CO)]; hydrogen; sodium methylate In 1,4-dioxane at 40℃; under 18751.9 Torr; for 16h; Glovebox; Inert atmosphere; | A 95% B n/a |
With trimethylamine-N-oxide; tricarbonyl(η4-1,3-bis(trimethylsilyl)-4,5,6,7-tetrahydro-2H-inden-2-one)iron; hydrogen; triethylamine In toluene at 90℃; under 52505.3 Torr; for 17h; Inert atmosphere; Glovebox; | |
With C21H35BrMnN2O2P; hydrogen; potassium hydride; 1,3,5-trimethyl-benzene In toluene at 100℃; under 15001.5 Torr; for 60h; Autoclave; Inert atmosphere; | A 97 %Spectr. B 96 %Spectr. |
With C21H35BrMnN2O2P; hydrogen; potassium hydride In toluene at 100℃; under 15001.5 Torr; for 60h; | A 97 %Spectr. B 96 %Spectr. |
2-Allyl-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
allyl alcohol
Conditions | Yield |
---|---|
With [bis(acetoxy)iodo]benzene; water; triethylamine In acetonitrile at 20℃; for 1h; | 67% |
With sodium periodate; iodobenzene In water; acetonitrile at 80℃; for 8h; | 64% |
Conditions | Yield |
---|---|
With formic acid at 235℃; | 98% |
With rhenium trioxide; hydrogen at 140℃; Temperature; Reagent/catalyst; Solvent; Time; | 91% |
In water at 148℃; for 2.5h; Catalytic behavior; Reagent/catalyst; Temperature; Solvent; Sealed tube; | 91% |
2-(prop-2-en-1-yloxy)oxane
allyl alcohol
Conditions | Yield |
---|---|
With methanol at 20℃; for 0.5h; | 98% |
With methanol; zirconium(IV) chloride at 20℃; for 4h; | 96% |
ruthenium trichloride In water; acetonitrile at 20℃; for 0.333333h; | 96% |
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; water; sodium hydroxide In hexane at 25℃; pH=5; | 90% |
With water; sodium hydrogencarbonate at 150℃; | |
With copper; potassium carbonate | |
With fluoride In gas Rate constant; reaction efficiency; |
Conditions | Yield |
---|---|
palladium anchored polystyrene In neat (no solvent) at 25℃; under 41371.8 Torr; for 15h; | A 5% B 90% |
With hydrogen; copper-palladium; silica gel In ethanol at 25℃; under 760 Torr; Kinetics; | A n/a B 85% |
With hydrogen; palladium dichloride In N,N-dimethyl-formamide under 18751.5 Torr; for 0.316667h; Product distribution; Ambient temperature; various time; | A 2.6% B 76.3% |
Conditions | Yield |
---|---|
With KOH/ZrO2 In water at 225℃; Reagent/catalyst; Temperature; Solvent; | 47% |
(E)-4-(acetoxy)-1-phenyl-2-buten-1-one
A
3-hydroxy-1-phenyl-but-2-en-1-one
B
allyl alcohol
Conditions | Yield |
---|---|
Stage #1: (E)-4-(acetoxy)-1-phenyl-2-buten-1-one With bis(iodozinc)methane In tetrahydrofuran at 25℃; Inert atmosphere; Stage #2: With ammonium chloride In tetrahydrofuran; water Inert atmosphere; | A 91% B n/a |
Conditions | Yield |
---|---|
With H3PO4-activated and WOx-loaded montmorillonite nanocatalyst In water at 320℃; for 3h; Flow reactor; | A n/a B n/a C 50.7% |
tris(allyl)borate
n-perfluorohexyl iodide
A
2-iodo-4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononan-1-ol
B
allyl alcohol
Conditions | Yield |
---|---|
Stage #1: tris(allyl)borate; n-perfluorohexyl iodide With 2,2'-azobis(isobutyronitrile) at 60 - 70℃; for 3h; Stage #2: With water at 60℃; | A 99% B n/a |
glycerol
A
acetaldehyde
B
allyl alcohol
C
hydroxy-2-propanone
D
acrolein
Conditions | Yield |
---|---|
With H3PO4-activated and WOx-loaded montmorillonite nanocatalyst In water at 320℃; for 3h; Reagent/catalyst; Flow reactor; | A n/a B n/a C n/a D 46.7% |
glycerol
A
propan-1-ol
B
propylene glycol
C
allyl alcohol
D
isopropyl alcohol
Conditions | Yield |
---|---|
With hydrogen In 1,4-dioxane at 20 - 140℃; under 7500.75 - 60006 Torr; for 32h; Autoclave; |
glycerol
A
propan-1-ol
B
propylene glycol
C
propene
D
allyl alcohol
Conditions | Yield |
---|---|
With hydrogen In 1,4-dioxane at 20 - 140℃; under 7500.75 - 60006 Torr; for 4h; Time; Autoclave; |
Conditions | Yield |
---|---|
With lithium phosphate at 245 - 250℃; | |
With aluminum oxide at 275℃; | |
With chromium(III) oxide at 350℃; | |
With gold nanoparticles supported on hollow mesoporous silica (Au/SiO2) at 370℃; |
Conditions | Yield |
---|---|
With alumina-supported iron In water at 340℃; Inert atmosphere; | 17.5% |
Conditions | Yield |
---|---|
With water; ion exchange resin Diaion SK104H at 80℃; under 3750.38 Torr; | |
With water; ion exchange resin Diaion SK104H at 80℃; under 3750.38 Torr; | |
With water Product distribution / selectivity; |
Conditions | Yield |
---|---|
With di(n-butyl)tin oxide at 180℃; under 0.975098 - 9.976 Torr; for 2h; |
Conditions | Yield |
---|---|
With dibutyltin oxide at 180℃; under 0.975098 - 9.976 Torr; for 1h; |
Conditions | Yield |
---|---|
With dibutyltin oxide at 180℃; under 0.975098 - 9.976 Torr; for 1h; |
4,4'-isopropylidenebis[2-(2,6-dibromophenoxy)ethanol]
diallyl isophthalate
B
allyl alcohol
Conditions | Yield |
---|---|
With dibutyltin oxide at 180℃; under 0.975098 - 9.976 Torr; for 1h; |
4,4'-isopropylidenebis[2-(2,6-dibromophenoxy)ethanol]
diallyl terephthalate
B
allyl alcohol
Conditions | Yield |
---|---|
With dibutyltin oxide at 180℃; under 0.975098 - 9.976 Torr; for 1h; |
methyloxirane
allyl alcohol
Conditions | Yield |
---|---|
With lithium phosphate at 280℃; | |
lithium phosphate containing about 0.1-0.3 wt percent of sodium and 0.3-0.5 wt percent of boron at 253 - 273℃; Conversion of starting material; | |
lithium phosphate containing 0.3 wt percent of boron at 273℃; Conversion of starting material; |
allyloxytrimethylsilane
allyl alcohol
Conditions | Yield |
---|---|
With oxygen; manganese(II) p-aminobenzoate; cobalt(II) p-aminobenzoate; silica gel In hexane for 10.5h; Heating; | 88% |
With oxygen; silica gel-supported Co/Mn p-aminobenzoate (1:1 mixture) In hexane for 12h; Heating; | 88% |
Conditions | Yield |
---|---|
at 315℃; Gas phase; |
propene
A
allyl alcohol
B
acrolein
C
methyloxirane
Conditions | Yield |
---|---|
With oxygen at 349.84℃; under 1125.11 Torr; Reagent/catalyst; Temperature; |
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