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Dibutyl phosphate CAS 107-66-4 Phosphoric acid dibutyl ester di-n-butylhydrogenphosphate CAS no 107-66-4 Di-n-butyl phosphate Dibutyl phosphate IN Stock CAS 107-66-4 Dibutyl phosphate COA TDS price MSDS Dibutyl phosphate MSDS Product no. ch
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inquiryPhosphoric acid,dibutyl ester Henan Tianfu Chemical Co.,LTD was built in 2009 with an ISO certificate in the past 5 years, we have grown up as a famous fine chemicals supplier in china and we had established stable business relationships with sam
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inquiryProduct Name Dibutyl phosphate CAS No. 107-66-4 Appearance Colorless to light yellow transparent liquid
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inquiryDibutyl Phosphate CAS:107-66-4 Specification Product Name Dibutyl phosphate CAS No. 107-66-4 Appearance Colorless to light yellow transparent liquid
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Product name: Dibutyl Phosphate CAS No.:107-66-4 Molecule Formula:C8H19O4P Molecule Weight:210.20 Purity: 97.0% Package: 200kg/drum Description:Colorless or light yellow liquid Manufacture Standards:Enterprise Standard TESTING IT
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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Conditions | Yield |
---|---|
With sodium hydroxide In ethanol; water for 2.5h; Heating; | 97% |
With sodium hydroxide | |
With hydrogenchloride In hydrogenchloride byproducts: C4H9Cl; hydrolysis of TBP in concd. HCl;; hydrolytic decompn. of 18.5 % TBP in 6 days at ambient temp.;; | |
With HCl In hydrogenchloride byproducts: C4H9Cl; hydrolysis of TBP in concd. HCl;; hydrolytic decompn. of 18.5 % TBP in 6 days at ambient temp.;; |
butan-1-ol
A
n-butyl phosphoric acid
B
phosphoric acid tributyl ester
C
dibutyl phosphate
Conditions | Yield |
---|---|
With phosphorus; tetraethylammonium iodide In water; acetonitrile electrolysis; | A n/a B 87% C n/a |
Conditions | Yield |
---|---|
With sodium bromate; phosphan at 80℃; Kinetics; Condensation; | A 20% B 80% |
With sodium hypophosphite; copper dichloride at 24.9℃; for 4h; | A 22.2% B 77.8% |
With phosphorous; air; ruthenium hydroxide trichloride; copper dichloride at 80℃; oxidative alkoxylation; | A 33.7% B 11.3% |
Di-n-butyl-(o-hydroxy-phenyl)-phosphat
dibutyl phosphate
Conditions | Yield |
---|---|
With [bis(acetoxy)iodo]benzene; water In acetonitrile at 20℃; for 1h; oxidative cleavage; | 72% |
Conditions | Yield |
---|---|
With oxygen; hypophosphorous acid; copper dichloride at 50℃; for 6h; | A 4% B 48% |
Conditions | Yield |
---|---|
With sodium hydroxide In tetrahydrofuran; water at 0℃; | 46% |
With water beim Erhitzen; | |
With water In toluene for 1h; Reflux; | 29.5 g |
N-prolyl>proline
A
(R)-1-[(R)-1-(Dibutoxy-phosphoryl)-pyrrolidine-2-carbonyl]-pyrrolidine-2-carboxylic acid butyl ester
B
dibutyl phosphate
C
rac-octahydrodipyrrolo[1,2-a:1',2'-d]pyrazine-5,10-dione
Conditions | Yield |
---|---|
With butan-1-ol at 105 - 110℃; for 6h; | A 28.6% B 25% C 42% |
N-prolyl>proline
butan-1-ol
A
(R)-1-[(R)-1-(Dibutoxy-phosphoryl)-pyrrolidine-2-carbonyl]-pyrrolidine-2-carboxylic acid butyl ester
B
dibutyl phosphate
C
rac-octahydrodipyrrolo[1,2-a:1',2'-d]pyrazine-5,10-dione
Conditions | Yield |
---|---|
at 105 - 110℃; for 6h; | A 28.6% B 25% C 42% |
Conditions | Yield |
---|---|
With ethanol Hydrogenation.an Platin; |
Conditions | Yield |
---|---|
With water; trichlorophosphate | |
With triethylamine; trichlorophosphate In toluene at 60℃; for 1h; |
Conditions | Yield |
---|---|
With methanesulfonic acid; dimethylsulfide for 18h; Ambient temperature; |
phosphoric acid tributyl ester
A
n-butyl phosphoric acid
B
phosphorofluoridic acid dibutyl ester
C
phosphorofluoridic acid monobutyl ester
D
phosphorodifluoridic acid butyl ester
E
dibutyl phosphate
Conditions | Yield |
---|---|
In sulfuric acid; hydrogen fluoride Product distribution; time, composition of the aqueous solution; |
phosphoric acid tributyl ester
A
n-butyl phosphoric acid
B
n-Butyl chloride
C
dibutyl phosphate
D
butan-1-ol
Conditions | Yield |
---|---|
With hydrogenchloride In water at 25℃; Mechanism; Product distribution; Rate constant; different HCl concentrations; |
Conditions | Yield |
---|---|
With phosphorus pentaoxide microwave irradiation; |
phosphoric acid tributyl ester
A
n-butyl phosphoric acid
B
dibutyl phosphate
Conditions | Yield |
---|---|
With sodium hydroxide In methanol; water at 100℃; for 2h; Title compound not separated from byproducts.; | |
With (238)plutonium; nitric acid for 21h; Concentration; Irradiation; Radiolysis; |
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 78.6 percent / Et3N, CCl4 / ethanol; H2O / 14 h / 0 °C 2: Et3N, CCl4 / CH2Cl2 / 10 h / 0 °C 3: Et3N / 6 h / 0 °C 4: 76.3 percent / LiOH*H2O, H2O / tetrahydrofuran; methanol / 5 h / 60 °C / various bases, other time and temperature 5: 25 percent / butanol / 6 h / 105 - 110 °C View Scheme | |
With copper diacetate In tetrahydrofuran-d8 at 20℃; Inert atmosphere; | |
Multi-step reaction with 2 steps 1: copper dichloride / tetrahydrofuran / 0.42 h / 0 - 20 °C 2: sodium hydroxide / tetrahydrofuran; water / 0 °C View Scheme | |
With Nitrogen dioxide at 35℃; Cooling; |
N-(dibutyloxyphosphinyl)proline
dibutyl phosphate
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: Et3N, CCl4 / CH2Cl2 / 10 h / 0 °C 2: Et3N / 6 h / 0 °C 3: 76.3 percent / LiOH*H2O, H2O / tetrahydrofuran; methanol / 5 h / 60 °C / various bases, other time and temperature 4: 25 percent / butanol / 6 h / 105 - 110 °C View Scheme |
N-proline methyl ester
dibutyl phosphate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 76.3 percent / LiOH*H2O, H2O / tetrahydrofuran; methanol / 5 h / 60 °C / various bases, other time and temperature 2: 25 percent / butanol / 6 h / 105 - 110 °C View Scheme |
dibutyl phosphate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: Et3N / 6 h / 0 °C 2: 76.3 percent / LiOH*H2O, H2O / tetrahydrofuran; methanol / 5 h / 60 °C / various bases, other time and temperature 3: 25 percent / butanol / 6 h / 105 - 110 °C View Scheme |
hydrogenchloride
oxygen
butan-1-ol
A
phosphoric acid tributyl ester
B
n-Butyl chloride
C
dibutyl phosphate
D
zinc(II) chloride
Conditions | Yield |
---|---|
copper dichloride In butan-1-ol Kinetics; |
dibutyl (1,1-dioxido-4-oxo-3-phenyl-4H-thiochromen-2-yl)methyl phosphate
dibutyl phosphate
Conditions | Yield |
---|---|
In chloroform-d1 for 0.183333h; Irradiation; | > 99 %Spectr. |
dibutyl phosphate
sodium salt of dibutyl phosphate
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water at 20℃; for 1h; | 100% |
With sodium hydroxide | |
With sodium hydrogencarbonate In water |
dibutyl phosphate
Conditions | Yield |
---|---|
With 4 A molecular sieve In dichloromethane at 20℃; for 1h; | 100% |
dibutyl phosphate
dibutyl (2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl) phosphate
Conditions | Yield |
---|---|
With 4 A molecular sieve In dichloromethane at 20℃; for 0.5h; | 100% |
1-butyl-4-methylpyridin-1-ium iodide
dibutyl phosphate
1-butyl-4-methylpyridinium dibutylphosphate
Conditions | Yield |
---|---|
Stage #1: dibutyl phosphate With Amberlyst A-26 (OH- form) In methanol; water at 20℃; Stage #2: 1-butyl-4-methylpyridin-1-ium iodide In methanol | 100% |
Conditions | Yield |
---|---|
Stage #1: dibutyl phosphate With Amberlyst A-26 (OH- form) In methanol; water at 20℃; Stage #2: 1,3-dimethylimidazolim iodide In methanol | 100% |
1-methyl-3-(n-butyl)imidazolium iodide
dibutyl phosphate
Conditions | Yield |
---|---|
Stage #1: dibutyl phosphate With Amberlyst A-26 (OH- form) In methanol; water at 20℃; Stage #2: 1-methyl-3-(n-butyl)imidazolium iodide In methanol | 100% |
1,3-bis(n-butyl)imidazolium iodide
dibutyl phosphate
C8H18O4P(1-)*C11H21N2(1+)
Conditions | Yield |
---|---|
Stage #1: dibutyl phosphate With Amberlyst A-26 (OH- form) In methanol; water at 20℃; Stage #2: 1,3-dibutyl-1,3-imidazolium iodide In methanol | 100% |
dibutyl phosphate
1-butyl-2,3-dimethylimidazolium dibutylphosfonate
Conditions | Yield |
---|---|
Stage #1: dibutyl phosphate With Amberlyst A-26 (OH- form) In methanol; water at 20℃; Stage #2: 1-butyl-2,3-dimethylimidazolium bromide In methanol | 100% |
methyl 3-O-benzyl-4-O-tert-butyldimethylsilyl-β-L-idopyranuronate 1,2-(methyl-orthoacetate)
dibutyl phosphate
Conditions | Yield |
---|---|
Stage #1: methyl 3-O-benzyl-4-O-tert-butyldimethylsilyl-β-L-idopyranuronate 1,2-(methyl-orthoacetate) In dichloromethane at 20℃; for 0.25h; Inert atmosphere; Molecular sieve; Stage #2: dibutyl phosphate In dichloromethane Inert atmosphere; Molecular sieve; | 100% |
methyl 3-O-benzyl-4-O-tert-butyldimethylsilyl-β-L-idopyranuronate 1,2-(methyl-orthoacetate)
dibutyl phosphate
Conditions | Yield |
---|---|
In dichloromethane at 20℃; Molecular sieve; | 100% |
In dichloromethane at 20℃; Molecular sieve; | 100% |
cholinium hydrogen carbonate
dibutyl phosphate
cholinium dibutyl phosphate
Conditions | Yield |
---|---|
In water at 20℃; | 100% |
Conditions | Yield |
---|---|
In methanol | 100% |
In methanol at 0 - 20℃; | 98% |
In methanol at 0 - 20℃; for 1h; | 98% |
2-O-benzyl-3,4-di-O-pivaloyl-α-L-fucopyranosyl trichloroacetimidate
dibutyl phosphate
dibutyl 2-O-benzyl-3,4-di-O-pivaloyl-β-L-fucopyranoside phosphate
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 0.5h; | 99% |
dibutyl phosphate
Conditions | Yield |
---|---|
Stage #1: ethyl 2,4-di-O-benzyl-3,6-di-O-picoloyl-1-thio-α-D-mannopyranoside; dibutyl phosphate In dichloromethane at 20℃; for 1h; Molecular sieve; Inert atmosphere; Stage #2: With N-iodo-succinimide; trifluorormethanesulfonic acid In dichloromethane at 20℃; for 1h; Molecular sieve; Inert atmosphere; diastereoselective reaction; | 99% |
dibutyl phosphate
3,4-di-O-benzyl-2-deoxy-6-O-levulinyl-2-phthalimido-β-D-glucopyranosyl trichloroacetamidate
Conditions | Yield |
---|---|
In toluene for 14h; | 98% |
Conditions | Yield |
---|---|
In various solvent(s) at 80℃; for 1h; | 98% |
Conditions | Yield |
---|---|
In water at 20℃; for 0.25h; | 98% |
With triethylamine |
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 12h; Inert atmosphere; | 98% |
dibutyl phosphate
Conditions | Yield |
---|---|
With 4 A molecular sieve In dichloromethane at 20℃; for 0.5h; | 97% |
dibutyl phosphate
dibutyl (2-O-benzoyl-3,4-di-O-benzyl-α-D-mannopyranosyl) phosphate
Conditions | Yield |
---|---|
Molecular sieve; Inert atmosphere; | 97% |
1,3-dibutyl-5,6-dimethylbenzimidazolium iodide
dibutyl phosphate
C8H18O4P(1-)*C17H27N2(1+)
Conditions | Yield |
---|---|
Stage #1: dibutyl phosphate With Amberlyst A-26 (OH- form) In methanol; water at 20℃; Stage #2: 1,3-dibutyl-5,6-dimethylbenzimidazolium iodide In methanol | 97% |
phenyl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside
dibutyl phosphate
Conditions | Yield |
---|---|
Stage #1: phenyl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside; dibutyl phosphate In dichloromethane at 20℃; for 1h; Molecular sieve; Inert atmosphere; Stage #2: With N-iodo-succinimide; trifluorormethanesulfonic acid In dichloromethane at 20℃; for 18h; Molecular sieve; Inert atmosphere; | 97% |
dibutyl phosphate
Conditions | Yield |
---|---|
With N-iodo-succinimide; trifluorormethanesulfonic acid In dichloromethane at 0 - 20℃; for 1.33333h; Molecular sieve; Inert atmosphere; | 97% |
2-iodo-propane
dibutyl phosphate
phosphoric acid dibutyl ester isopropyl ester
Conditions | Yield |
---|---|
With cesium fluoride In acetonitrile for 6h; Ambient temperature; | 96% |
Conditions | Yield |
---|---|
With N,N,N',N'-tetramethylchlorformamidinium chloride; triethylamine In dichloromethane at 0 - 20℃; for 2h; | 96% |
3,4,6-tri-O-benzyl-1,2-O-(methoxyethylidene)-β-D-mannopyranose
dibutyl phosphate
di-n-butyl (2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl) phosphate
Conditions | Yield |
---|---|
With 4 A molecular sieve In dichloromethane at 20℃; for 0.366667h; | 96% |
Molecular sieve; Inert atmosphere; | 93% |
With triethylamine In dichloromethane at 0 - 25℃; Molecular sieve; Inert atmosphere; |
dibutyl phosphate
Conditions | Yield |
---|---|
Stage #1: C23H24Cl3NO11S; dibutyl phosphate In dichloromethane at 20℃; for 3h; Inert atmosphere; Molecular sieve; Stage #2: With N-iodo-succinimide; trifluorormethanesulfonic acid In diethyl ether; dichloromethane at 0 - 4℃; Inert atmosphere; | 96% |
Conditions | Yield |
---|---|
With N-iodo-succinimide; trifluorormethanesulfonic acid In dichloromethane at 0℃; | 96% |
C62H66O7SSi
dibutyl phosphate
dibutyl 6-O-triisopropylsilyl-2-O-(2-((4-methoxybenzyloxy)methyl)benzoyl)-2,3-di-O-(2-methylnaphthyl)-α-D-mannopyranoside phosphate
Conditions | Yield |
---|---|
With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate In dichloromethane Inert atmosphere; | 96% |
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