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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

Dibutyl phosphate Manufacturer/High quality/Best price/In stock

Cas:107-66-4

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Dibutylphosphate supplier in China

Cas:107-66-4

Min.Order:1 Metric Ton

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Dibutylphosphate

Cas:107-66-4

Min.Order:1

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Type:Other

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Hebei yanxi chemical co.,LTD.

chengdu and import and export trade co., LTD., who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do res

Dibutyl phosphate

Cas:107-66-4

Min.Order:1 Kilogram

FOB Price: $30.0

Type:Trading Company

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Chemwill Asia Co., Ltd.

Dibutyl phosphate CAS 107-66-4 Phosphoric acid dibutyl ester di-n-butylhydrogenphosphate CAS no 107-66-4 Di-n-butyl phosphate Dibutyl phosphate IN Stock CAS 107-66-4 Dibutyl phosphate COA TDS price MSDS Dibutyl phosphate MSDS Product no. ch

Henan Tianfu Chemical Co., Ltd.

Phosphoric acid,dibutyl ester Henan Tianfu Chemical Co.,LTD was built in 2009 with an ISO certificate in the past 5 years, we have grown up as a famous fine chemicals supplier in china and we had established stable business relationships with sam

di-n-Butyl hydrogen phsophate

Cas:107-66-4

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hebei Nengqian Chemical Import and Export Co., LTD

Our Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con

99% Purity Good Supply Dibutyl Phosphate for Extractant CAS 107-66-4

Cas:107-66-4

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Manufacturer supply CAS 107-66-4 with best quality

Cas:107-66-4

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Product Name Dibutyl phosphate CAS No. 107-66-4 Appearance Colorless to light yellow transparent liquid

Dibutyl Phosphate

Cas:107-66-4

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Phosphoric acid,dibutyl ester 107-66-4

Cas:107-66-4

Min.Order:1 Kilogram

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Qingdao Beluga Import and Export Co., LTD

Dibutyl phosphate CAS:107-66-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedi

Dibutyl phosphate CAS:107-66-4

Cas:107-66-4

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Phosphoric acid,dibutyl ester

Cas:107-66-4

Min.Order:1 Kilogram

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Lonwin Chemical Group Limited

Dibutyl Phosphate CAS:107-66-4 Specification Product Name Dibutyl phosphate CAS No. 107-66-4 Appearance Colorless to light yellow transparent liquid

Factory Supply Dibutyl Phosphate

Cas:107-66-4

Min.Order:1 Kilogram

FOB Price: $100.0 / 150.0

Type:Other

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Phosphoric acid,dibutyl ester

Cas:107-66-4

Min.Order:0

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

Dibutylphosphate

Cas:107-66-4

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

Dibutyl phosphate

Cas:107-66-4

Min.Order:0 Metric Ton

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Dibutyl phosphate

Cas:107-66-4

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality Dibutylphosphate

Cas:107-66-4

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:clear liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:As extraction agent

Phosphoric acid,dibutyl ester

Cas:107-66-4

Min.Order:1 Gram

Negotiable

Type:Trading Company

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Siwei Development Group Ltd.

Product name: Dibutyl Phosphate CAS No.:107-66-4 Molecule Formula:C8H19O4P Molecule Weight:210.20 Purity: 97.0% Package: 200kg/drum Description:Colorless or light yellow liquid Manufacture Standards:Enterprise Standard TESTING IT

Best Quality Dibutyl Phosphate

Cas:107-66-4

Min.Order:1 Kilogram

Negotiable

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Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

Best OfferDibutyl phosphate

Cas:107-66-4

Min.Order:0

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Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

Dibutylphosphate

Cas:107-66-4

Min.Order:1 Milligram

Negotiable

Type:Trading Company

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Henan Kanbei Chemical Co.,LTD

High quality, competitive price, fast delivery and first-class service we possesses have won the trust and praise of customers. Standard: BP/USP/EP The purity is equal or greater than 99%. As a supplier, we can provide high-quality products. Cle

Dibutyl phosphate.99%

Cas:107-66-4

Min.Order:1 Metric Ton

Negotiable

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EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

Dibutyl Phosphate

Cas:107-66-4

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

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Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

Dibutyl Phosphate

Cas:107-66-4

Min.Order:1 Gram

Negotiable

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KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

Dibutyl Phosphate

Cas:107-66-4

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

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Golden Pharma Co., Limited

GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation

Dibutyl phosphate

Cas:107-66-4

Min.Order:1 Kilogram

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Type:Other

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Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

Dibutyl Phosphate

Cas:107-66-4

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

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GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

Dibutyl phosphate

Cas:107-66-4

Min.Order:0

Negotiable

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Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

Dibutyl Phosphate

Cas:107-66-4

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Synthetic route

phosphoric acid tributyl ester
126-73-8

phosphoric acid tributyl ester

dibutyl phosphate
107-66-4

dibutyl phosphate

Conditions
ConditionsYield
With sodium hydroxide In ethanol; water for 2.5h; Heating;97%
With sodium hydroxide
With hydrogenchloride In hydrogenchloride byproducts: C4H9Cl; hydrolysis of TBP in concd. HCl;; hydrolytic decompn. of 18.5 % TBP in 6 days at ambient temp.;;
With HCl In hydrogenchloride byproducts: C4H9Cl; hydrolysis of TBP in concd. HCl;; hydrolytic decompn. of 18.5 % TBP in 6 days at ambient temp.;;
butan-1-ol
71-36-3

butan-1-ol

A

n-butyl phosphoric acid
1623-15-0

n-butyl phosphoric acid

B

phosphoric acid tributyl ester
126-73-8

phosphoric acid tributyl ester

C

dibutyl phosphate
107-66-4

dibutyl phosphate

Conditions
ConditionsYield
With phosphorus; tetraethylammonium iodide In water; acetonitrile electrolysis;A n/a
B 87%
C n/a
butan-1-ol
71-36-3

butan-1-ol

A

phosphoric acid tributyl ester
126-73-8

phosphoric acid tributyl ester

B

dibutyl phosphate
107-66-4

dibutyl phosphate

Conditions
ConditionsYield
With sodium bromate; phosphan at 80℃; Kinetics; Condensation;A 20%
B 80%
With sodium hypophosphite; copper dichloride at 24.9℃; for 4h;A 22.2%
B 77.8%
With phosphorous; air; ruthenium hydroxide trichloride; copper dichloride at 80℃; oxidative alkoxylation;A 33.7%
B 11.3%
Di-n-butyl-(o-hydroxy-phenyl)-phosphat
38257-85-1

Di-n-butyl-(o-hydroxy-phenyl)-phosphat

dibutyl phosphate
107-66-4

dibutyl phosphate

Conditions
ConditionsYield
With [bis(acetoxy)iodo]benzene; water In acetonitrile at 20℃; for 1h; oxidative cleavage;72%
butan-1-ol
71-36-3

butan-1-ol

A

dibutyl phosphate
107-66-4

dibutyl phosphate

B

Phosphoric acid mono-n-butylester
16456-56-7

Phosphoric acid mono-n-butylester

Conditions
ConditionsYield
With oxygen; hypophosphorous acid; copper dichloride at 50℃; for 6h;A 4%
B 48%
dibutyl chlorophosphate
819-43-2

dibutyl chlorophosphate

dibutyl phosphate
107-66-4

dibutyl phosphate

Conditions
ConditionsYield
With sodium hydroxide In tetrahydrofuran; water at 0℃;46%
With water beim Erhitzen;
With water In toluene for 1h; Reflux;29.5 g
N-prolyl>proline
121252-83-3

N-prolyl>proline

A

(R)-1-[(R)-1-(Dibutoxy-phosphoryl)-pyrrolidine-2-carbonyl]-pyrrolidine-2-carboxylic acid butyl ester
121252-84-4

(R)-1-[(R)-1-(Dibutoxy-phosphoryl)-pyrrolidine-2-carbonyl]-pyrrolidine-2-carboxylic acid butyl ester

B

dibutyl phosphate
107-66-4

dibutyl phosphate

C

rac-octahydrodipyrrolo[1,2-a:1',2'-d]pyrazine-5,10-dione
19943-27-2

rac-octahydrodipyrrolo[1,2-a:1',2'-d]pyrazine-5,10-dione

Conditions
ConditionsYield
With butan-1-ol at 105 - 110℃; for 6h;A 28.6%
B 25%
C 42%
N-prolyl>proline
121252-83-3

N-prolyl>proline

butan-1-ol
71-36-3

butan-1-ol

A

(R)-1-[(R)-1-(Dibutoxy-phosphoryl)-pyrrolidine-2-carbonyl]-pyrrolidine-2-carboxylic acid butyl ester
121252-84-4

(R)-1-[(R)-1-(Dibutoxy-phosphoryl)-pyrrolidine-2-carbonyl]-pyrrolidine-2-carboxylic acid butyl ester

B

dibutyl phosphate
107-66-4

dibutyl phosphate

C

rac-octahydrodipyrrolo[1,2-a:1',2'-d]pyrazine-5,10-dione
19943-27-2

rac-octahydrodipyrrolo[1,2-a:1',2'-d]pyrazine-5,10-dione

Conditions
ConditionsYield
at 105 - 110℃; for 6h;A 28.6%
B 25%
C 42%
dibutyl phenyl phosphate
2528-36-1

dibutyl phenyl phosphate

dibutyl phosphate
107-66-4

dibutyl phosphate

Conditions
ConditionsYield
With ethanol Hydrogenation.an Platin;
butan-1-ol
71-36-3

butan-1-ol

dibutyl phosphate
107-66-4

dibutyl phosphate

Conditions
ConditionsYield
With water; trichlorophosphate
With triethylamine; trichlorophosphate In toluene at 60℃; for 1h;
dibutyl methyl phosphate
7242-59-3

dibutyl methyl phosphate

dibutyl phosphate
107-66-4

dibutyl phosphate

Conditions
ConditionsYield
With methanesulfonic acid; dimethylsulfide for 18h; Ambient temperature;
phosphoric acid tributyl ester
126-73-8

phosphoric acid tributyl ester

A

n-butyl phosphoric acid
1623-15-0

n-butyl phosphoric acid

B

phosphorofluoridic acid dibutyl ester
674-48-6

phosphorofluoridic acid dibutyl ester

C

phosphorofluoridic acid monobutyl ester
372-03-2

phosphorofluoridic acid monobutyl ester

D

phosphorodifluoridic acid butyl ester
26078-17-1

phosphorodifluoridic acid butyl ester

E

dibutyl phosphate
107-66-4

dibutyl phosphate

Conditions
ConditionsYield
In sulfuric acid; hydrogen fluoride Product distribution; time, composition of the aqueous solution;
thiophosphoric acid O,O'-dibutyl ester
10163-62-9

thiophosphoric acid O,O'-dibutyl ester

iodine
7553-56-2

iodine

furan-2,3,5(4H)-trione pyridine (1:1)

furan-2,3,5(4H)-trione pyridine (1:1)

dibutyl phosphate
107-66-4

dibutyl phosphate

phosphoric acid tributyl ester
126-73-8

phosphoric acid tributyl ester

A

n-butyl phosphoric acid
1623-15-0

n-butyl phosphoric acid

B

n-Butyl chloride
109-69-3

n-Butyl chloride

C

dibutyl phosphate
107-66-4

dibutyl phosphate

D

butan-1-ol
71-36-3

butan-1-ol

E

H3PO4

H3PO4

Conditions
ConditionsYield
With hydrogenchloride In water at 25℃; Mechanism; Product distribution; Rate constant; different HCl concentrations;
butan-1-ol
71-36-3

butan-1-ol

A

n-butyl phosphoric acid
1623-15-0

n-butyl phosphoric acid

B

dibutyl phosphate
107-66-4

dibutyl phosphate

Conditions
ConditionsYield
With phosphorus pentaoxide microwave irradiation;
phosphoric acid tributyl ester
126-73-8

phosphoric acid tributyl ester

A

n-butyl phosphoric acid
1623-15-0

n-butyl phosphoric acid

B

dibutyl phosphate
107-66-4

dibutyl phosphate

Conditions
ConditionsYield
With sodium hydroxide In methanol; water at 100℃; for 2h; Title compound not separated from byproducts.;
With (238)plutonium; nitric acid for 21h; Concentration; Irradiation; Radiolysis;
dibutyl hydrogen phosphite
1809-19-4

dibutyl hydrogen phosphite

dibutyl phosphate
107-66-4

dibutyl phosphate

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 78.6 percent / Et3N, CCl4 / ethanol; H2O / 14 h / 0 °C
2: Et3N, CCl4 / CH2Cl2 / 10 h / 0 °C
3: Et3N / 6 h / 0 °C
4: 76.3 percent / LiOH*H2O, H2O / tetrahydrofuran; methanol / 5 h / 60 °C / various bases, other time and temperature
5: 25 percent / butanol / 6 h / 105 - 110 °C
View Scheme
With copper diacetate In tetrahydrofuran-d8 at 20℃; Inert atmosphere;
Multi-step reaction with 2 steps
1: copper dichloride / tetrahydrofuran / 0.42 h / 0 - 20 °C
2: sodium hydroxide / tetrahydrofuran; water / 0 °C
View Scheme
With Nitrogen dioxide at 35℃; Cooling;
N-(dibutyloxyphosphinyl)proline
121252-81-1

N-(dibutyloxyphosphinyl)proline

dibutyl phosphate
107-66-4

dibutyl phosphate

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: Et3N, CCl4 / CH2Cl2 / 10 h / 0 °C
2: Et3N / 6 h / 0 °C
3: 76.3 percent / LiOH*H2O, H2O / tetrahydrofuran; methanol / 5 h / 60 °C / various bases, other time and temperature
4: 25 percent / butanol / 6 h / 105 - 110 °C
View Scheme
N-proline methyl ester
121252-82-2

N-proline methyl ester

dibutyl phosphate
107-66-4

dibutyl phosphate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 76.3 percent / LiOH*H2O, H2O / tetrahydrofuran; methanol / 5 h / 60 °C / various bases, other time and temperature
2: 25 percent / butanol / 6 h / 105 - 110 °C
View Scheme
[(R)-2-(Diethoxy-phosphoryloxycarbonyl)-pyrrolidin-1-yl]-phosphonic acid dibutyl ester

[(R)-2-(Diethoxy-phosphoryloxycarbonyl)-pyrrolidin-1-yl]-phosphonic acid dibutyl ester

dibutyl phosphate
107-66-4

dibutyl phosphate

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: Et3N / 6 h / 0 °C
2: 76.3 percent / LiOH*H2O, H2O / tetrahydrofuran; methanol / 5 h / 60 °C / various bases, other time and temperature
3: 25 percent / butanol / 6 h / 105 - 110 °C
View Scheme
hydrogenchloride
7647-01-0

hydrogenchloride

zinc(II) phosphide

zinc(II) phosphide

oxygen
80937-33-3

oxygen

butan-1-ol
71-36-3

butan-1-ol

A

phosphoric acid tributyl ester
126-73-8

phosphoric acid tributyl ester

B

n-Butyl chloride
109-69-3

n-Butyl chloride

C

dibutyl phosphate
107-66-4

dibutyl phosphate

D

zinc(II) chloride
7646-85-7

zinc(II) chloride

Conditions
ConditionsYield
copper dichloride In butan-1-ol Kinetics;
dibutyl (1,1-dioxido-4-oxo-3-phenyl-4H-thiochromen-2-yl)methyl phosphate
1369964-80-6

dibutyl (1,1-dioxido-4-oxo-3-phenyl-4H-thiochromen-2-yl)methyl phosphate

dibutyl phosphate
107-66-4

dibutyl phosphate

Conditions
ConditionsYield
In chloroform-d1 for 0.183333h; Irradiation;> 99 %Spectr.
dibutyl phosphate
107-66-4

dibutyl phosphate

sodium salt of dibutyl phosphate
16298-74-1

sodium salt of dibutyl phosphate

Conditions
ConditionsYield
With sodium hydrogencarbonate In water at 20℃; for 1h;100%
With sodium hydroxide
With sodium hydrogencarbonate In water
((2S,3aS,5R,6R,6aS)-6-Benzyloxy-2-methoxy-2-phenyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-ylmethoxy)-triisopropyl-silane

((2S,3aS,5R,6R,6aS)-6-Benzyloxy-2-methoxy-2-phenyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-ylmethoxy)-triisopropyl-silane

dibutyl phosphate
107-66-4

dibutyl phosphate

dibutyl (2-O-benzoyl-3-O-benzyl-5-O-tri-isopropylsilyl-α-D-arabinofuranosyl) phosphate

dibutyl (2-O-benzoyl-3-O-benzyl-5-O-tri-isopropylsilyl-α-D-arabinofuranosyl) phosphate

Conditions
ConditionsYield
With 4 A molecular sieve In dichloromethane at 20℃; for 1h;100%
(2S,3aR,5R,6R,7S,7aR)-6,7-Bis-benzyloxy-5-benzyloxymethyl-2-methoxy-2-phenyl-tetrahydro-[1,3]dioxolo[4,5-b]pyran

(2S,3aR,5R,6R,7S,7aR)-6,7-Bis-benzyloxy-5-benzyloxymethyl-2-methoxy-2-phenyl-tetrahydro-[1,3]dioxolo[4,5-b]pyran

dibutyl phosphate
107-66-4

dibutyl phosphate

dibutyl (2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl) phosphate
208656-42-2

dibutyl (2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl) phosphate

Conditions
ConditionsYield
With 4 A molecular sieve In dichloromethane at 20℃; for 0.5h;100%
1-butyl-4-methylpyridin-1-ium iodide
32353-64-3

1-butyl-4-methylpyridin-1-ium iodide

dibutyl phosphate
107-66-4

dibutyl phosphate

1-butyl-4-methylpyridinium dibutylphosphate
1289675-21-3

1-butyl-4-methylpyridinium dibutylphosphate

Conditions
ConditionsYield
Stage #1: dibutyl phosphate With Amberlyst A-26 (OH- form) In methanol; water at 20℃;
Stage #2: 1-butyl-4-methylpyridin-1-ium iodide In methanol
100%
1,3-dimethylimidazolim iodide
4333-62-4

1,3-dimethylimidazolim iodide

dibutyl phosphate
107-66-4

dibutyl phosphate

[mmim]Bu2PO4
1382354-65-5

[mmim]Bu2PO4

Conditions
ConditionsYield
Stage #1: dibutyl phosphate With Amberlyst A-26 (OH- form) In methanol; water at 20℃;
Stage #2: 1,3-dimethylimidazolim iodide In methanol
100%
1-methyl-3-(n-butyl)imidazolium iodide
65039-05-6

1-methyl-3-(n-butyl)imidazolium iodide

dibutyl phosphate
107-66-4

dibutyl phosphate

1-n-butyl-3-methylimidazolium dibutyl phosphate

1-n-butyl-3-methylimidazolium dibutyl phosphate

Conditions
ConditionsYield
Stage #1: dibutyl phosphate With Amberlyst A-26 (OH- form) In methanol; water at 20℃;
Stage #2: 1-methyl-3-(n-butyl)imidazolium iodide In methanol
100%
1,3-bis(n-butyl)imidazolium iodide
143085-46-5

1,3-bis(n-butyl)imidazolium iodide

dibutyl phosphate
107-66-4

dibutyl phosphate

C8H18O4P(1-)*C11H21N2(1+)
654058-05-6

C8H18O4P(1-)*C11H21N2(1+)

Conditions
ConditionsYield
Stage #1: dibutyl phosphate With Amberlyst A-26 (OH- form) In methanol; water at 20℃;
Stage #2: 1,3-dibutyl-1,3-imidazolium iodide In methanol
100%
dibutyl phosphate
107-66-4

dibutyl phosphate

1-butyl-2,3-dimethylimidazolium bromide

1-butyl-2,3-dimethylimidazolium bromide

1-butyl-2,3-dimethylimidazolium dibutylphosfonate
1289675-18-8

1-butyl-2,3-dimethylimidazolium dibutylphosfonate

Conditions
ConditionsYield
Stage #1: dibutyl phosphate With Amberlyst A-26 (OH- form) In methanol; water at 20℃;
Stage #2: 1-butyl-2,3-dimethylimidazolium bromide In methanol
100%
methyl 3-O-benzyl-4-O-tert-butyldimethylsilyl-β-L-idopyranuronate 1,2-(methyl-orthoacetate)
1448263-56-6

methyl 3-O-benzyl-4-O-tert-butyldimethylsilyl-β-L-idopyranuronate 1,2-(methyl-orthoacetate)

dibutyl phosphate
107-66-4

dibutyl phosphate

methyl (dibutylphosphate-2-O-acetyl-3-O-benzyl-4-O-tert-butyldimethylsilyl-β-L-idopyranosid)uronate

methyl (dibutylphosphate-2-O-acetyl-3-O-benzyl-4-O-tert-butyldimethylsilyl-β-L-idopyranosid)uronate

Conditions
ConditionsYield
Stage #1: methyl 3-O-benzyl-4-O-tert-butyldimethylsilyl-β-L-idopyranuronate 1,2-(methyl-orthoacetate) In dichloromethane at 20℃; for 0.25h; Inert atmosphere; Molecular sieve;
Stage #2: dibutyl phosphate In dichloromethane Inert atmosphere; Molecular sieve;
100%
methyl 3-O-benzyl-4-O-tert-butyldimethylsilyl-β-L-idopyranuronate 1,2-(methyl-orthoacetate)
1448263-56-6

methyl 3-O-benzyl-4-O-tert-butyldimethylsilyl-β-L-idopyranuronate 1,2-(methyl-orthoacetate)

dibutyl phosphate
107-66-4

dibutyl phosphate

methyl (dibutylphosphate-2-O-acetyl-3-O-benzyl-4-O-tert-butyldimethylsilyl-α-L-idopyranosid)uronate

methyl (dibutylphosphate-2-O-acetyl-3-O-benzyl-4-O-tert-butyldimethylsilyl-α-L-idopyranosid)uronate

Conditions
ConditionsYield
In dichloromethane at 20℃; Molecular sieve;100%
In dichloromethane at 20℃; Molecular sieve;100%
cholinium hydrogen carbonate
78-73-9

cholinium hydrogen carbonate

dibutyl phosphate
107-66-4

dibutyl phosphate

cholinium dibutyl phosphate
1241962-99-1

cholinium dibutyl phosphate

Conditions
ConditionsYield
In water at 20℃;100%
tetra(n-butyl)ammonium hydroxide
2052-49-5

tetra(n-butyl)ammonium hydroxide

dibutyl phosphate
107-66-4

dibutyl phosphate

dibutylphosphoric acid tetrabutylammonium salt

dibutylphosphoric acid tetrabutylammonium salt

Conditions
ConditionsYield
In methanol100%
In methanol at 0 - 20℃;98%
In methanol at 0 - 20℃; for 1h;98%
2-O-benzyl-3,4-di-O-pivaloyl-α-L-fucopyranosyl trichloroacetimidate
373606-55-4

2-O-benzyl-3,4-di-O-pivaloyl-α-L-fucopyranosyl trichloroacetimidate

dibutyl phosphate
107-66-4

dibutyl phosphate

dibutyl 2-O-benzyl-3,4-di-O-pivaloyl-β-L-fucopyranoside phosphate
373606-28-1

dibutyl 2-O-benzyl-3,4-di-O-pivaloyl-β-L-fucopyranoside phosphate

Conditions
ConditionsYield
In dichloromethane at 20℃; for 0.5h;99%
ethyl 2,4-di-O-benzyl-3,6-di-O-picoloyl-1-thio-α-D-mannopyranoside

ethyl 2,4-di-O-benzyl-3,6-di-O-picoloyl-1-thio-α-D-mannopyranoside

dibutyl phosphate
107-66-4

dibutyl phosphate

C40H47N2O11P

C40H47N2O11P

Conditions
ConditionsYield
Stage #1: ethyl 2,4-di-O-benzyl-3,6-di-O-picoloyl-1-thio-α-D-mannopyranoside; dibutyl phosphate In dichloromethane at 20℃; for 1h; Molecular sieve; Inert atmosphere;
Stage #2: With N-iodo-succinimide; trifluorormethanesulfonic acid In dichloromethane at 20℃; for 1h; Molecular sieve; Inert atmosphere; diastereoselective reaction;
99%
dibutyl phosphate
107-66-4

dibutyl phosphate

3,4-di-O-benzyl-2-deoxy-6-O-levulinyl-2-phthalimido-β-D-glucopyranosyl trichloroacetamidate
208047-71-6

3,4-di-O-benzyl-2-deoxy-6-O-levulinyl-2-phthalimido-β-D-glucopyranosyl trichloroacetamidate

3,4-di-O-benzyl-2-deoxy-6-O-levulinyl-2-phthalimido-D-glucopyranose-1-dibutylphosphate

3,4-di-O-benzyl-2-deoxy-6-O-levulinyl-2-phthalimido-D-glucopyranose-1-dibutylphosphate

Conditions
ConditionsYield
In toluene for 14h;98%
Trimethyl orthoacetate
1445-45-0

Trimethyl orthoacetate

dibutyl phosphate
107-66-4

dibutyl phosphate

dibutyl methyl phosphate
7242-59-3

dibutyl methyl phosphate

Conditions
ConditionsYield
In various solvent(s) at 80℃; for 1h;98%
aluminum L-lactate

aluminum L-lactate

dibutyl phosphate
107-66-4

dibutyl phosphate

3C8H18O4P(1-)*Al(3+)

3C8H18O4P(1-)*Al(3+)

Conditions
ConditionsYield
In water at 20℃; for 0.25h;98%
With triethylamine
dibutyl phosphate
107-66-4

dibutyl phosphate

N,N,N',N'-tetramethylguanidine
80-70-6

N,N,N',N'-tetramethylguanidine

C8H19O4P*C5H13N3

C8H19O4P*C5H13N3

Conditions
ConditionsYield
In dichloromethane at 20℃; for 12h; Inert atmosphere;98%
(2S,3aS,5R,6R,7S,7aS)-6,7-Bis-benzyloxy-5-benzyloxymethyl-2-methoxy-2-phenyl-tetrahydro-[1,3]dioxolo[4,5-b]pyran

(2S,3aS,5R,6R,7S,7aS)-6,7-Bis-benzyloxy-5-benzyloxymethyl-2-methoxy-2-phenyl-tetrahydro-[1,3]dioxolo[4,5-b]pyran

dibutyl phosphate
107-66-4

dibutyl phosphate

dibutyl (2-O-benzoyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl) phosphate

dibutyl (2-O-benzoyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl) phosphate

Conditions
ConditionsYield
With 4 A molecular sieve In dichloromethane at 20℃; for 0.5h;97%
C27H26O6

C27H26O6

dibutyl phosphate
107-66-4

dibutyl phosphate

dibutyl (2-O-benzoyl-3,4-di-O-benzyl-α-D-mannopyranosyl) phosphate
1059116-10-7

dibutyl (2-O-benzoyl-3,4-di-O-benzyl-α-D-mannopyranosyl) phosphate

Conditions
ConditionsYield
Molecular sieve; Inert atmosphere;97%
1,3-dibutyl-5,6-dimethylbenzimidazolium iodide
1382354-48-4

1,3-dibutyl-5,6-dimethylbenzimidazolium iodide

dibutyl phosphate
107-66-4

dibutyl phosphate

C8H18O4P(1-)*C17H27N2(1+)
1382354-51-9

C8H18O4P(1-)*C17H27N2(1+)

Conditions
ConditionsYield
Stage #1: dibutyl phosphate With Amberlyst A-26 (OH- form) In methanol; water at 20℃;
Stage #2: 1,3-dibutyl-5,6-dimethylbenzimidazolium iodide In methanol
97%
phenyl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside
62774-33-8

phenyl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside

dibutyl phosphate
107-66-4

dibutyl phosphate

bis(butyl)phosphoryl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranoside

bis(butyl)phosphoryl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranoside

Conditions
ConditionsYield
Stage #1: phenyl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside; dibutyl phosphate In dichloromethane at 20℃; for 1h; Molecular sieve; Inert atmosphere;
Stage #2: With N-iodo-succinimide; trifluorormethanesulfonic acid In dichloromethane at 20℃; for 18h; Molecular sieve; Inert atmosphere;
97%
ethyl O-(2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1→4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

ethyl O-(2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1→4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

dibutyl phosphate
107-66-4

dibutyl phosphate

di-O-butyl O-(2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1→4)-4,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosylphosphate

di-O-butyl O-(2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1→4)-4,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosylphosphate

Conditions
ConditionsYield
With N-iodo-succinimide; trifluorormethanesulfonic acid In dichloromethane at 0 - 20℃; for 1.33333h; Molecular sieve; Inert atmosphere;97%
2-iodo-propane
75-30-9

2-iodo-propane

dibutyl phosphate
107-66-4

dibutyl phosphate

phosphoric acid dibutyl ester isopropyl ester
60140-72-9

phosphoric acid dibutyl ester isopropyl ester

Conditions
ConditionsYield
With cesium fluoride In acetonitrile for 6h; Ambient temperature;96%
dibutyl phosphate
107-66-4

dibutyl phosphate

n-butyl pyrophosphate
1474-75-5

n-butyl pyrophosphate

Conditions
ConditionsYield
With N,N,N',N'-tetramethylchlorformamidinium chloride; triethylamine In dichloromethane at 0 - 20℃; for 2h;96%
3,4,6-tri-O-benzyl-1,2-O-(methoxyethylidene)-β-D-mannopyranose
16697-49-7

3,4,6-tri-O-benzyl-1,2-O-(methoxyethylidene)-β-D-mannopyranose

dibutyl phosphate
107-66-4

dibutyl phosphate

di-n-butyl (2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl) phosphate
604767-74-0

di-n-butyl (2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl) phosphate

Conditions
ConditionsYield
With 4 A molecular sieve In dichloromethane at 20℃; for 0.366667h;96%
Molecular sieve; Inert atmosphere;93%
With triethylamine In dichloromethane at 0 - 25℃; Molecular sieve; Inert atmosphere;
C23H24Cl3NO11S

C23H24Cl3NO11S

dibutyl phosphate
107-66-4

dibutyl phosphate

methyl (5-amido-7,8,9-tri-O-chloroacetyl-5-N,4-O-carbonyl-2-(dibutylphosphoryl)-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranoside)onate

methyl (5-amido-7,8,9-tri-O-chloroacetyl-5-N,4-O-carbonyl-2-(dibutylphosphoryl)-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranoside)onate

Conditions
ConditionsYield
Stage #1: C23H24Cl3NO11S; dibutyl phosphate In dichloromethane at 20℃; for 3h; Inert atmosphere; Molecular sieve;
Stage #2: With N-iodo-succinimide; trifluorormethanesulfonic acid In diethyl ether; dichloromethane at 0 - 4℃; Inert atmosphere;
96%
C23H24Cl3NO11S
1246533-72-1

C23H24Cl3NO11S

dibutyl phosphate
107-66-4

dibutyl phosphate

C25H37Cl3NO15P
1246533-73-2

C25H37Cl3NO15P

Conditions
ConditionsYield
With N-iodo-succinimide; trifluorormethanesulfonic acid In dichloromethane at 0℃;96%
C62H66O7SSi
1572443-60-7

C62H66O7SSi

dibutyl phosphate
107-66-4

dibutyl phosphate

dibutyl 6-O-triisopropylsilyl-2-O-(2-((4-methoxybenzyloxy)methyl)benzoyl)-2,3-di-O-(2-methylnaphthyl)-α-D-mannopyranoside phosphate
1572443-75-4

dibutyl 6-O-triisopropylsilyl-2-O-(2-((4-methoxybenzyloxy)methyl)benzoyl)-2,3-di-O-(2-methylnaphthyl)-α-D-mannopyranoside phosphate

Conditions
ConditionsYield
With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate In dichloromethane Inert atmosphere;96%
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