Jinlan Pharm-Drugs Technology Co.,Limited (with its export company Hangzhou Royall Import & Export Co.,Ltd.)is located in Hangzhou, Zhejiang Province. Neighboring Ningbo port, Shanghai port, Hangzhou Xiaoshan Int’l Airport and Shanghai Pu
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inquirySpecifciaiton: In-house; Certification: ISO 9001; US FDA and EDQM Approved Plant; Appearance:White Storage:Preserve in tight containers Application:Contrast agent Port:Shanghai, Ningbo, etc.
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inquiryProduct informations Product Name Dimethyl 5-nitroisophthalate CAS No. 13290-96-5 Appearance White crystalline powder Assay ≥99%
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inquiryDayangChem exported this product to many countries and regions at best price in China. If you are looking for the product’s supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product specifica
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inquiryName:Dimethyl 5-nitroisophthalate CAS NO: 13290-96-5 Grade:Medical scientific research and export Molecular formula:C10H9NO6 Molecular weight:239.18 Product Quality 12 years of chemical raw materials Mature operation of the industry System
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inquiryOur company engages in Sodium Tripolyphosphate (STPP) and Sodium Hexametabphosphate (SHMP) production; development of noble metal catalysts, synthesis of electronic chemical materials and general chemicals Imp&Exp trading business. The company
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inquiryAbout Product Details Item Specification Test Results Appearance White crystalline powder Conform
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inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
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inquiryAlias: 5-Nitro Isophthalic acid dimethyl ester; Dimethyl 5-nitrobenzene-1,3-dicarboxylate; 5-Nitroisophthalic acid dimethyl ester; Dimethyl 5-Nitrophthalate; Dimethyl 5-nitroisophthalate; 5-NIPA DME; 2,4-dimethyl-5-nitrobenzene-1,3-dicarboxylate;
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inquiryDimethyl 5-nitroisophthalate CAS:13290-96-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality orga
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
CAS-No. 13290-96-5 Molecular Formula: C10H9NO6 Molecular Weight:239.19 SYNONYMS Dimethyl 5-nitrobenzene-1,3-dicarboxylate; 5-Nitroisophthalic acid dimethyl ester;
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
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Cas:13290-96-5
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inquiry5-Nitroisophthalic acid dimethylester CAS No. 13290-96-5 MF: C10H9NO6 MP: 123-130℃ 5-NIPA : 0.1% max. ISO9001 Appearance:white powder Storage:Store in dry and cool place with good seal Package: 25kg/drum, or as per your request. Appli
methanol
5-nitrobenzene-1,3-dicarboxylic acid
dimethyl 5-nitroisophthalate
Conditions | Yield |
---|---|
With sulfuric acid for 3h; Inert atmosphere; Reflux; | 98% |
With hydrogenchloride |
dimethyl Isophthalate
dimethyl 5-nitroisophthalate
Conditions | Yield |
---|---|
With iron(III) chloride; Nitrogen dioxide; ozone In 1,2-dichloro-ethane at 5℃; for 1.5h; Product distribution; Further Variations:; Solvents; Reagents; | 92% |
With sulfur dioxide; dinitrogen pentoxide 1.) -78 to -11 deg C, 2 h, 2.) -11 deg C, 2 h; | 90% |
With sulfuric acid; sulfur trioxide; nitric acid |
5-nitrobenzene-1,3-dicarboxylic acid
dimethyl 5-nitroisophthalate
Conditions | Yield |
---|---|
With thionyl chloride In methanol at 0 - 80℃; for 6h; Inert atmosphere; | 90% |
With hydrogenchloride | |
With sulfuric acid In methanol; water; toluene |
5-nitro-1,3-benzenedicarbonylchloride
dimethyl 5-nitroisophthalate
Conditions | Yield |
---|---|
In methanol |
dimethyl 5-aminoisophthalate
dimethyl 5-nitroisophthalate
Conditions | Yield |
---|---|
With oxone In dichloromethane; water for 6h; Inert atmosphere; |
dimethyl 5-nitroisophthalate
serinol
N,N'-bis-(2-hydroxy-1-hydroxymethylethyl)-5-nitroisophthalamide
Conditions | Yield |
---|---|
In methanol at 20℃; for 48h; Reflux; | 99% |
dimethyl 5-nitroisophthalate
ethylenediamine
Conditions | Yield |
---|---|
at 0℃; for 24h; | 96.8% |
dimethyl 5-nitroisophthalate
dimethyl 5-aminoisophthalate
Conditions | Yield |
---|---|
With formic acid; triethylamine chemoselective reaction; | 95% |
With ammonium sulfide | |
With hydrogenchloride; methanol; zinc |
dimethyl 5-nitroisophthalate
ethanolamine
N,N’-bis(2-hydroxyethyl)-5-nitroisophthaldiamide
Conditions | Yield |
---|---|
In methanol at 70 - 75℃; for 70h; | 94% |
dimethyl 5-nitroisophthalate
propan-1-ol-3-amine
Conditions | Yield |
---|---|
In methanol at 70 - 75℃; for 70h; | 92% |
3-Amino-1,2-propanediol
dimethyl 5-nitroisophthalate
5-nitro-N,N'-bis-(2,3-dihydroxypropyl)isophthalamide
Conditions | Yield |
---|---|
In methanol at 70 - 75℃; for 70h; | 91% |
In methanol | 85% |
With sodium methylate In methanol for 80h; | |
With sodium methylate In methanol at 25 - 30℃; for 2h; Temperature; Solvent; | |
With sodium methylate In methanol at 20 - 50℃; |
dimethyl 5-nitroisophthalate
dimethyl 5-(N,N-dimethylamino)isophthalate
Conditions | Yield |
---|---|
With formaldehyd; hydrogen; propionic acid; aluminum nickel In methanol | 85% |
formaldehyd
dimethyl 5-nitroisophthalate
dimethyl 5-(N,N-dimethylamino)isophthalate
Conditions | Yield |
---|---|
With formic acid; triethylamine In water; tert-butyl alcohol at 100℃; for 44h; | 82% |
Conditions | Yield |
---|---|
In methanol at 20 - 65℃; for 24h; Time; | 75.3% |
dimethyl 5-nitroisophthalate
5-nitro-1,3-benzenedicarboxylic acid, monomethyl ester
Conditions | Yield |
---|---|
With water; sodium hydroxide In methanol for 2h; Reflux; | 75% |
3-Amino-1,2-propanediol
dimethyl 5-nitroisophthalate
Conditions | Yield |
---|---|
In methanol at 20 - 65℃; for 24.5h; | 56% |
dimethyl 5-nitroisophthalate
3-hydroxymethyl-5-nitrobenzoic acid methyl ester
Conditions | Yield |
---|---|
With diisobutylaluminium hydride In tetrahydrofuran; toluene at -78 - 20℃; | 50% |
dimethyl 5-nitroisophthalate
5-nitrobenzene-1,3-dicarbaldehyde
Conditions | Yield |
---|---|
With diisobutylaluminium hydride In toluene at -78℃; for 1h; Inert atmosphere; | 48% |
dimethyl 5-nitroisophthalate
Conditions | Yield |
---|---|
With lead; ammonium acetate In methanol at 20℃; for 24.25h; Inert atmosphere; | 34% |
dimethyl 5-nitroisophthalate
A
dimethyl 5-aminoisophthalate
Conditions | Yield |
---|---|
With ethanol; hydrogen sulfide; ammonia |
dimethyl 5-nitroisophthalate
5-nitro-isophthalic acid dihydrazide
Conditions | Yield |
---|---|
With hydrazine hydrate |
dimethyl 5-nitroisophthalate
Conditions | Yield |
---|---|
With hydrazine; Rh on carbon In tetrahydrofuran Catalytic hydrogenation; |
dimethyl 5-nitroisophthalate
1-amino-naphthalene
dimethyl 5-nitroisophthalate
acetone
Conditions | Yield |
---|---|
With potassium hydroxide In dimethylsulfoxide-d6 at 25℃; for 4h; Yanovsky reaction; |
dimethyl 5-nitroisophthalate
acetone
Conditions | Yield |
---|---|
With potassium methanolate In methanol at 25℃; Yanovsky reaction; Title compound not separated from byproducts; |
dimethyl 5-nitroisophthalate
C14H19N3O8
dimethyl 5-nitroisophthalate
[(2-{3-[2-(bis-carboxymethyl-amino)-ethylcarbamoyl]-5-nitro-benzoylamino}-ethyl)-carboxymethyl-amino]-acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 96.8 percent / 24 h / 0 °C 2: 89 percent / NaOH / H2O / 20 - 70 °C / pH 5 - 10 View Scheme |
dimethyl 5-nitroisophthalate
3-azidomethyl-5-nitrobenzoic acid methyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 50 percent / diisobutylaluminum hydride / tetrahydrofuran; toluene / -78 - 20 °C 2: 95 percent / triethylamine / CH2Cl2 / 0.5 h / 0 °C 3: 100 percent / sodium azide / dimethylformamide / 2 h / 50 °C View Scheme |
dimethyl 5-nitroisophthalate
3-[(tert-butyloxycarbonyl)aminomethyl]-5-nitrobenzoic acid methyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 50 percent / diisobutylaluminum hydride / tetrahydrofuran; toluene / -78 - 20 °C 2: 95 percent / triethylamine / CH2Cl2 / 0.5 h / 0 °C 3: 100 percent / sodium azide / dimethylformamide / 2 h / 50 °C 4: 85 percent / triethylamine; 1,3-propanedithiol / methanol / 12 h / 20 °C 5: 100 percent / triethylamine / tetrahydrofuran / 12 h / 0 °C View Scheme |
dimethyl 5-nitroisophthalate
3-[(tert-butyloxycarbonyl)aminomethyl]-5-nitrobenzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: 50 percent / diisobutylaluminum hydride / tetrahydrofuran; toluene / -78 - 20 °C 2: 95 percent / triethylamine / CH2Cl2 / 0.5 h / 0 °C 3: 100 percent / sodium azide / dimethylformamide / 2 h / 50 °C 4: 85 percent / triethylamine; 1,3-propanedithiol / methanol / 12 h / 20 °C 5: 100 percent / triethylamine / tetrahydrofuran / 12 h / 0 °C 6: 100 percent / NaOH / H2O; dioxane View Scheme |
dimethyl 5-nitroisophthalate
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1: 50 percent / diisobutylaluminum hydride / tetrahydrofuran; toluene / -78 - 20 °C 2: 95 percent / triethylamine / CH2Cl2 / 0.5 h / 0 °C 3: 100 percent / sodium azide / dimethylformamide / 2 h / 50 °C 4: 85 percent / triethylamine; 1,3-propanedithiol / methanol / 12 h / 20 °C 5: 100 percent / triethylamine / tetrahydrofuran / 12 h / 0 °C 6: 100 percent / NaOH / H2O; dioxane View Scheme |
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