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methylthiol
benzothiadiazole-7-carboxylic acid chloride
S-methyl-benzo[1,2,3]thiadiazole-7-carbothioate
Conditions | Yield |
---|---|
Esterification; | |
With triethylamine In toluene | |
With sodium hydroxide |
benzothiadiazole-7-carboxylic acid chloride
sodium thiomethoxide
S-methyl-benzo[1,2,3]thiadiazole-7-carbothioate
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 5h; | 0.12 g |
benzo[d][1,2,3 ]thiadiazol-7-carboxylic acid
S-methyl-benzo[1,2,3]thiadiazole-7-carbothioate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: SOCl2 / 8 h / 90 °C 2: 0.12 g / CH2Cl2 / 5 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: SOCl2 View Scheme | |
Multi-step reaction with 2 steps 1: thionyl chloride 2: sodium hydroxide View Scheme |
Benzo[1,2,3]thiadiazole-7-nitrile
S-methyl-benzo[1,2,3]thiadiazole-7-carbothioate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 88 percent / KOH / butan-1-ol 2: SOCl2 View Scheme |
2-chloro-3-nitrobenzoic acid methyl ester
S-methyl-benzo[1,2,3]thiadiazole-7-carbothioate
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: 99 percent 2: H2 / Raney nickel / tetrahydrofuran 3: 86 percent / NaNO2; H(+) 4: 98 percent / NaOH; H2O 5: SOCl2 View Scheme |
1,2-Dichloro-3-nitrobenzene
S-methyl-benzo[1,2,3]thiadiazole-7-carbothioate
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1: K2CO3 / N,N-dimethyl-acetamide 2: Na2S / propan-2-ol; H2O 3: 76 percent / Ni(PPh3)4 4: 97 percent / isoamyl nitrite; HCl / butan-1-ol 5: 88 percent / KOH / butan-1-ol 6: SOCl2 View Scheme |
2-chloro-3,5-dinitrobenzoic acid
S-methyl-benzo[1,2,3]thiadiazole-7-carbothioate
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1.1: K2CO3 / dimethylformamide 2.1: K2CO3 3.1: H2 / Raney nickel / tetrahydrofuran 4.1: NaNO2; H(+) 4.2: 65 percent / H3PO2 5.1: 98 percent / NaOH; H2O 6.1: SOCl2 View Scheme |
benzo[1,2,3]thiadiazole-7-carboxylic acid methtyl ester
S-methyl-benzo[1,2,3]thiadiazole-7-carbothioate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 98 percent / NaOH; H2O 2: SOCl2 View Scheme |
2-chloro-3-nitrobezoic acid
S-methyl-benzo[1,2,3]thiadiazole-7-carbothioate
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1: 99 percent / H2SO4 2: 99 percent 3: H2 / Raney nickel / tetrahydrofuran 4: 86 percent / NaNO2; H(+) 5: 98 percent / NaOH; H2O 6: SOCl2 View Scheme |
2-amino-6-chlorophenyl-isopropylsulfane
S-methyl-benzo[1,2,3]thiadiazole-7-carbothioate
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 76 percent / Ni(PPh3)4 2: 97 percent / isoamyl nitrite; HCl / butan-1-ol 3: 88 percent / KOH / butan-1-ol 4: SOCl2 View Scheme |
2-chloro-6-nitrophenyl isopropyl sulfide
S-methyl-benzo[1,2,3]thiadiazole-7-carbothioate
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: Na2S / propan-2-ol; H2O 2: 76 percent / Ni(PPh3)4 3: 97 percent / isoamyl nitrite; HCl / butan-1-ol 4: 88 percent / KOH / butan-1-ol 5: SOCl2 View Scheme |
3-amino-2-isopropylthiobenzonitrile
S-methyl-benzo[1,2,3]thiadiazole-7-carbothioate
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 97 percent / isoamyl nitrite; HCl / butan-1-ol 2: 88 percent / KOH / butan-1-ol 3: SOCl2 View Scheme |
Methyl 3-amino-2-benzylthiobenzoate
S-methyl-benzo[1,2,3]thiadiazole-7-carbothioate
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 86 percent / NaNO2; H(+) 2: 98 percent / NaOH; H2O 3: SOCl2 View Scheme |
2-benzylthio-3-nitrobenzoic acid methyl ester
S-methyl-benzo[1,2,3]thiadiazole-7-carbothioate
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: H2 / Raney nickel / tetrahydrofuran 2: 86 percent / NaNO2; H(+) 3: 98 percent / NaOH; H2O 4: SOCl2 View Scheme |
2-benzylthio-3,5-diamino-benzoic acid methyl ester
S-methyl-benzo[1,2,3]thiadiazole-7-carbothioate
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: NaNO2; H(+) 1.2: 65 percent / H3PO2 2.1: 98 percent / NaOH; H2O 3.1: SOCl2 View Scheme |
2-(phenylmethylsulfanyl)-3,5-dinitrobenzenecarboxylic acid
S-methyl-benzo[1,2,3]thiadiazole-7-carbothioate
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: K2CO3 2.1: H2 / Raney nickel / tetrahydrofuran 3.1: NaNO2; H(+) 3.2: 65 percent / H3PO2 4.1: 98 percent / NaOH; H2O 5.1: SOCl2 View Scheme |
methyl 2-(phenylmethylsulfanyl)-3,5-dinitrobenzenecarboxylate
S-methyl-benzo[1,2,3]thiadiazole-7-carbothioate
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: H2 / Raney nickel / tetrahydrofuran 2.1: NaNO2; H(+) 2.2: 65 percent / H3PO2 3.1: 98 percent / NaOH; H2O 4.1: SOCl2 View Scheme |
Lawessons reagent
S-methyl-benzo[1,2,3]thiadiazole-7-carbothioate
Conditions | Yield |
---|---|
In 5,5-dimethyl-1,3-cyclohexadiene |
S-methyl-benzo[1,2,3]thiadiazole-7-carbothioate
potassium benzo[1,2,3]thiadiazole-7-carboxylate
Conditions | Yield |
---|---|
With potassium hydroxide In water; toluene at 110℃; for 12h; | 90% |
dimethyl sulfate
S-methyl-benzo[1,2,3]thiadiazole-7-carbothioate
C9H9N2OS2(1+)*CH3O4S(1-)
Conditions | Yield |
---|---|
at 80 - 110℃; | 82% |
methyl trifluoromethanesulfonate
S-methyl-benzo[1,2,3]thiadiazole-7-carbothioate
C9H9N2OS2(1+)*CF3O3S(1-)
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 120 - 155℃; for 0.333333h; Inert atmosphere; | 65% |
S-methyl-benzo[1,2,3]thiadiazole-7-carbothioate
choline benzothiadiazole-7-carboxylate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium hydroxide / water; toluene / 12 h / 110 °C 2: methanol / 12 h View Scheme |
S-methyl-benzo[1,2,3]thiadiazole-7-carbothioate
C9H9N2OS2(1+)*C20H37O7S(1-)
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 80 - 110 °C 2: water; dichloromethane View Scheme |
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