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Product Description Name 10-Hydroxy-2-decenoic acid CAS 14113-05-4 Assay 99% Appearance
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inquiry10-Hydroxy-2-decenoic acid Basic information Product Name: 10-Hydroxy-2-decenoic acid Synonyms: OMEGA-HYDROXY C10:1 (2-TRANS);ROYAL JELLY ACID;QUEEN BEE ACID;(E)-10
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inquiryProducts: 10-Hydroxy-2-decenoic acid Cas No.: 14113-05-4 Molecular Formula: C10H18O3 Molecular Weight: 186.25 Assay: 99% Mo
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inquiryAppearance:White crystalline powder Storage:Room temperature Package:1kg/bag,25kg/drum Application:Health products raw materials Transportation:Express/Sea/Air Port:Any port in China
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inquiryProduct Name: 10-Hydroxy-2-decenoic acid CAS: 14113-05-4 MF: C10H18O3 MW: 186.25 EINECS: 808-119-7 Product Categories: 1 Mol File: 14113-05-4.mol 10-Hydroxy-2-decenoic acid Structure 10-Hydroxy-2-decenoic acid Chemical Propertie
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PRODUCT DETAILS 10-Hydroxy-2-decenoic acid Basic information
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inquiry(E)-ethyl 10-acetoxydec-2-enoate
(E)-10-hydroxy-dec-2-enoic acid
Conditions | Yield |
---|---|
With water; sodium hydroxide In ethanol at 60℃; for 4h; | 99.2% |
10-hydroxy-dec-2t-enoic acid methyl ester
(E)-10-hydroxy-dec-2-enoic acid
Conditions | Yield |
---|---|
With sodium hydroxide at 20℃; for 4h; Time; | 97% |
10-hydroxy 8-decenoic acid ethyl ester
(E)-10-hydroxy-dec-2-enoic acid
Conditions | Yield |
---|---|
With potassium hydroxide; water In ethanol for 8h; | 83% |
With potassium hydroxide In ethanol for 1.5h; Heating; | 73% |
With sodium hydroxide In ethanol for 5h; Heating; | 62% |
With potassium hydroxide | |
With potassium hydroxide In ethanol; water at 30℃; for 1h; Yield given; |
10-hydroxy-3-decenoic acid
(E)-10-hydroxy-dec-2-enoic acid
Conditions | Yield |
---|---|
With potassium hydroxide for 3h; Heating; | 65% |
Conditions | Yield |
---|---|
With pyridine 1.) ambient temperature, 72 h, 2.) heating on water-bath, 4 h; | 61% |
With piperidine 1) pyridine, 20 deg C, 16 h, 2) 110 - 115 deg C, 1 h; | 49% |
With pyridine |
malonic acid
acetic acid 8-oxo-octyl ester
(E)-10-hydroxy-dec-2-enoic acid
Conditions | Yield |
---|---|
Stage #1: malonic acid; acetic acid 8-oxo-octyl ester With piperidine; pyridine at 22 - 120℃; for 24.5h; Doebner reaction; Stage #2: With potassium carbonate In methanol at 20℃; for 24h; | 60% |
Conditions | Yield |
---|---|
(i) aq. H2SO4, EtOH, (ii) /BRN= 1751370/, Py, piperidine; Multistep reaction; | |
(i) aq. H2SO4, EtOH, (ii) /BRN= 1751370/; Multistep reaction; |
Conditions | Yield |
---|---|
(i) aq. KIO4, H2SO4, EtOH, (ii) /BRN= 1751370/, Py; Multistep reaction; |
10-acetoxydecanoic acid
(E)-10-hydroxy-dec-2-enoic acid
Conditions | Yield |
---|---|
(i) SOCl2, (ii) Br2, (iii) NaI, butanone, (iv) KOH, MeOH; Multistep reaction; | |
Multi-step reaction with 2 steps 1: (i) SOCl2, (ii) Br2, (iii) /BRN= 1098229/, Py 2: (i) NaI, acetone, (ii) KOH, MeOH View Scheme |
trans-10-Iod-2-decensaeure
(E)-10-hydroxy-dec-2-enoic acid
Conditions | Yield |
---|---|
(i) KOAc, AcOH, Py, (ii) KOH; Multistep reaction; |
2-Brom-10-acetoxy-decansaeure-methylester
(E)-10-hydroxy-dec-2-enoic acid
Conditions | Yield |
---|---|
(i) NaI, acetone, (ii) KOH, MeOH; Multistep reaction; |
3,10-dihydroxydecanoic acid
(E)-10-hydroxy-dec-2-enoic acid
Conditions | Yield |
---|---|
(i) Ac2O, (ii) KOH, EtOH; Multistep reaction; |
(E)-10-hydroxy-dec-2-enoic acid
Conditions | Yield |
---|---|
(i) KOEt, (ii) aq. KOH; Multistep reaction; |
8-chloro-1-octanal
(E)-10-hydroxy-dec-2-enoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: Py, piperidine 2: NaI / acetone 3: (i) KOAc, AcOH, Py, (ii) KOH View Scheme |
trans-10-Chlor-2-decensaeure
(E)-10-hydroxy-dec-2-enoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NaI / acetone 2: (i) KOAc, AcOH, Py, (ii) KOH View Scheme |
(E)-10-hydroxy-dec-2-enoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: (i) KN3, (ii) (heating), benzene, (iii) KOH 2: Py, piperidine 3: NaI / acetone 4: (i) KOAc, AcOH, Py, (ii) KOH View Scheme |
8,8-diethoxy-octanoic acid ethyl ester
(E)-10-hydroxy-dec-2-enoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: LiAlH4 / diethyl ether 2: (i) aq. H2SO4, EtOH, (ii) /BRN= 1751370/, Py, piperidine View Scheme | |
Multi-step reaction with 2 steps 1: LiAlH4 / diethyl ether 2: (i) aq. H2SO4, EtOH, (ii) /BRN= 1751370/ View Scheme |
(E)-8-Oxo-oct-2-enoic acid ethyl ester
(E)-10-hydroxy-dec-2-enoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: H2SO4 / ethanol 2: H2 / PtO2 / ethanol 3: LiAlH4 / diethyl ether 4: (i) aq. H2SO4, EtOH, (ii) /BRN= 1751370/ View Scheme |
(E)-8,8-Diethoxy-oct-2-enoic acid ethyl ester
(E)-10-hydroxy-dec-2-enoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: H2 / PtO2 / ethanol 2: LiAlH4 / diethyl ether 3: (i) aq. H2SO4, EtOH, (ii) /BRN= 1751370/ View Scheme |
(E)-10-hydroxy-dec-2-enoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: H2 / PtO2 / 2,2,4-trimethyl-pentane 2: LiAlH4 / diethyl ether 3: (i) aq. H2SO4, EtOH, (ii) /BRN= 1751370/, Py, piperidine View Scheme |
(E)-10-hydroxy-dec-2-enoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: O3; NaHCO3 / methanol; CH2Cl2 / -70 °C 1.2: 72.4 percent / Me2S; NaHCO3 / methanol; CH2Cl2 / 3 h / -40 - 20 °C 2.1: pyridine; piperidine / 24.5 h / 22 - 120 °C 2.2: 60 percent / K2CO3 / methanol / 24 h / 20 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 81 percent / mixture of ozone and oxygen (5.5percent masspercent of O3) / acetic acid; cyclohexane 2: 90 percent / TsOH / 16 h / 20 °C 3: 1) DIBAH, 2) water / 1) -10 deg C, toluene, 1.5 h, toluene, THF, 2) 20 deg C, 2 h 4: 97 percent / 10percent HCl / tetrahydrofuran / 16 h / 20 °C 5: 49 percent / piperidine / 1) pyridine, 20 deg C, 16 h, 2) 110 - 115 deg C, 1 h View Scheme |
8,8-dimethoxy-octan-1-ol
(E)-10-hydroxy-dec-2-enoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 97 percent / 10percent HCl / tetrahydrofuran / 16 h / 20 °C 2: 49 percent / piperidine / 1) pyridine, 20 deg C, 16 h, 2) 110 - 115 deg C, 1 h View Scheme |
7-formylheptanoic acid
(E)-10-hydroxy-dec-2-enoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 90 percent / TsOH / 16 h / 20 °C 2: 1) DIBAH, 2) water / 1) -10 deg C, toluene, 1.5 h, toluene, THF, 2) 20 deg C, 2 h 3: 97 percent / 10percent HCl / tetrahydrofuran / 16 h / 20 °C 4: 49 percent / piperidine / 1) pyridine, 20 deg C, 16 h, 2) 110 - 115 deg C, 1 h View Scheme |
8,8-dimethoxyoctanoic acid methyl ester
(E)-10-hydroxy-dec-2-enoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 1) DIBAH, 2) water / 1) -10 deg C, toluene, 1.5 h, toluene, THF, 2) 20 deg C, 2 h 2: 97 percent / 10percent HCl / tetrahydrofuran / 16 h / 20 °C 3: 49 percent / piperidine / 1) pyridine, 20 deg C, 16 h, 2) 110 - 115 deg C, 1 h View Scheme |
7-Formyl-4Z-heptenoic acid
(E)-10-hydroxy-dec-2-enoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 98 percent / hydrogen / 5percent Pd/C / acetic acid / 15 h / 20 °C / 15200 Torr 2: 90 percent / TsOH / 16 h / 20 °C 3: 1) DIBAH, 2) water / 1) -10 deg C, toluene, 1.5 h, toluene, THF, 2) 20 deg C, 2 h 4: 97 percent / 10percent HCl / tetrahydrofuran / 16 h / 20 °C 5: 49 percent / piperidine / 1) pyridine, 20 deg C, 16 h, 2) 110 - 115 deg C, 1 h View Scheme |
8-tetrahydropyranyloxyoctanal
(E)-10-hydroxy-dec-2-enoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 2: 79 percent / p-toluenesulfonic acid / ethanol / 1 h / Heating 3: 73 percent / KOH / ethanol / 1.5 h / Heating View Scheme |
ethyl (E)-10-(2-tetrahydropyranyloxy)-2-decenoate
(E)-10-hydroxy-dec-2-enoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 79 percent / p-toluenesulfonic acid / ethanol / 1 h / Heating 2: 73 percent / KOH / ethanol / 1.5 h / Heating View Scheme |
oct-7-enal
(E)-10-hydroxy-dec-2-enoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 65 percent / NaH / hexane; tetrahydrofuran / 3 h / Ambient temperature 2: 1.) 9-borabicyclo<3.3.1>nonane (9-BBN), 2.) aq. NaOH, 30percent aq. H2O2 / 1.) THF, RT, 5 h, 2.) THF, 50 deg C, 1 h 3: 62 percent / aq. NaOH / ethanol / 5 h / Heating View Scheme |
(E)-10-hydroxy-dec-2-enoic acid
acetic anhydride
trans-10-acetoxydec-2-enoic acid
Conditions | Yield |
---|---|
at 60 - 80℃; for 3h; | 97.6% |
(E)-10-hydroxy-dec-2-enoic acid
propionic acid anhydride
Conditions | Yield |
---|---|
at 60 - 80℃; for 3h; | 96.1% |
diazomethane
(E)-10-hydroxy-dec-2-enoic acid
methyl 9-formyl-(E)-2-nonecate
Conditions | Yield |
---|---|
With pyridinium chlorochromate | 75% |
1-hydroxy-pyrrolidine-2,5-dione
(E)-10-hydroxy-dec-2-enoic acid
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In N,N-dimethyl-formamide at 5 - 20℃; for 24h; | 52% |
(E)-10-hydroxy-dec-2-enoic acid
A
(2E,12E,22E)-triaconta-2,12,22-triene-1,11,21-triolide
B
(2E,12E)-eicosa-2,12-diene-1,11-diolide
Conditions | Yield |
---|---|
With triphenylphosphine; diethylazodicarboxylate In benzene at 20℃; for 72h; | A n/a B 24% C n/a D n/a |
diazomethane
(E)-10-hydroxy-dec-2-enoic acid
10-hydroxy-dec-2t-enoic acid methyl ester
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