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SICHUAN ZHONGBANG NEW MATERIAL CO., LTD

SICHUAN ZHONGBANG with its subsidiaries LUZHOU FUBANG& LUZHOU DAZHOU are specializing in the research, development, manufacturing and trade of fine chemicals, pesticide intermediates and pharmaceutical intermediates.

2-Ethyl-2-adamantanol

Cas:14648-57-8

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 2-Ethyl-2-Adamantanol supplier in China

Cas:14648-57-8

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Wuhan Fortuna Chemical Co.,Ltd

Good quality 2-Ethyl-2-adamantanol CAS 14648-57-8 with factory price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed

Good quality 2-Ethyl-2-adamantanol CAS 14648-57-8 with factory price

Cas:14648-57-8

Min.Order:10 Kilogram

FOB Price: $10.0

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Henan Allgreen Chemical Co.,Ltd

high quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai

2-Ethyl-2-adamantanol

Cas:14648-57-8

Min.Order:1 Kilogram

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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis

2-Ethyl-2-adamantanol

Cas:14648-57-8

Min.Order:1 Kilogram

FOB Price: $6.0

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Chemwill Asia Co., Ltd.

14648-57-8 2-Ethyl-2-adamantanol price 14648-57-8 2-Ethyl-2-adamantanol Manufacturer Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and s

14648-57-8 2-Ethyl-2-adamantanol price 14648-57-8 2-Ethyl-2-adamantanol Manufacturer

Cas:14648-57-8

Min.Order:5 Kiloliter

FOB Price: $3.5 / 5.0

Type:Manufacturers

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Hebei yanxi chemical co.,LTD.

chengdu and import and export trade co., LTD., who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do res

dobutramine

Cas:14648-57-8

Min.Order:1000 Gram

FOB Price: $130.0

Type:Trading Company

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Henan Tianfu Chemical Co., Ltd.

Product Name: 2-Ethyl-2-adamantanol Synonyms: 2-ETHYL-2-HYDROXYTRICYCLO[3,3,1,1(3,7)])DECANE;2-ETHYL-2-HYDROXYADAMANTANE;TRICYCLO[3.3.1.13,7]DECAN-2-OL, 2-ETHYL-;2-ETHYL-ADAMANTAN-2-OL;2-Ethyl-2-adamantanol ,99%;2-Ethyl-2-adamantane;2-

14648-57-8 2-Ethyl-2-adamantanol

Cas:14648-57-8

Min.Order:1 Gram

FOB Price: $8900.0

Type:Lab/Research institutions

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Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

2-Ethyl-2-adamantanol CAS:14648-57-8

Cas:14648-57-8

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Pharmaceutical Grade CAS 14648-57-8 with competitive price

Cas:14648-57-8

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W

2-Ethyl-2-adamantanol CAS:14648-57-8

Cas:14648-57-8

Min.Order:1 Metric Ton

FOB Price: $380.0 / 590.0

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Henan Sinotech Import&Export Corporation

Brief introduction: Chemical Name:2-Ethyl-2-Adamantanol CAS No:14648-57-8 Molecular Formula:C12H20O Molecular Weight:180.29 Packing:25kg/bag,Composite woven bag(plastic bag inside)or PE bag. Storage&Transportation:Store in a tightly closed conta

2-Ethyl-2-Adamantanol CAS:14648-57-8

Cas:14648-57-8

Min.Order:1 Kilogram

FOB Price: $1.0 / 2.0

Type:Other

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

2-Ethyl-2-adamantanol 14648-57-8

Cas:14648-57-8

Min.Order:1 Kilogram

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Type:Lab/Research institutions

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Baoji Guokang Healthchem co.,ltd

Product Name: Beta Alanine Powder Other name: Beta-aminopropionic acid CAS No.: 107-95-9 Molecular Formula: C3H7NO2 Appearance: White crystals or crystalline powder Assay: 99% Grade: Food Appearance:White powder Storage:Store at RT.

99% high quality with CAS 14648-57-8 best price.

Cas:14648-57-8

Min.Order:1 Kilogram

FOB Price: $332.0 / 693.0

Type:Trading Company

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

2-Ethyl-2-adamantanol

Cas:14648-57-8

Min.Order:1 Kilogram

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

2-Ethyl-2-AdaMantanol

Cas:14648-57-8

Min.Order:10 Kilogram

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Type:Trading Company

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Hebei Mojin Biotechnology Co.,Ltd

Hebei Mojin Biotechnology Co., Ltd, Our company is a professional chemical raw materials and chemical reagents research and development production enterprises. We have several production line,So we can control the lowest price. We also have several

2-Ethyl-2-adamantanol cas:14648-57-8

Cas:14648-57-8

Min.Order:25 Gram

FOB Price: $90.0 / 100.0

Type:Trading Company

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Leader Biochemical Group

PRODUCT DETAILS

China Largest Factory Manufacturer sales 2-Ethyl-2-Adamantanol CAS 14648-57-8

Cas:14648-57-8

Min.Order:500 Kilogram

FOB Price: $1.0 / 2.0

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

2-Ethyl-2-adamantanol

Cas:14648-57-8

Min.Order:0

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Type:Lab/Research institutions

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Hubei Jiutian Bio-medical Technology Co., Ltd

1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie

CAS 14648-57-8 2-Ethyl-2-adamantanol

Cas:14648-57-8

Min.Order:1 Kilogram

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

2-Ethyl-2-Adamantanol

Cas:14648-57-8

Min.Order:0 Metric Ton

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Afine Chemicals Limited

Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

2-ETHYL-2-ADAMANTANOL

Cas:14648-57-8

Min.Order:1 Gram

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Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

2-Ethyl-2-adamantanol

Cas:14648-57-8

Min.Order:0

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Type:Lab/Research institutions

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 2-Ethyl-2-adamantanol

Cas:14648-57-8

Min.Order:0 Metric Ton

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Type:Other

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

2-Ethyl-2-adamantanol

Cas:14648-57-8

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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Hangzhou Lingrui Chemical Co.,Ltd.

our strengths: 1: Fast and guaranteed shipment (TNT;EMS;FEDEX;DHL;UPS;EUB, special line) 2: Various payment items accepted (Btc; MoneyGram; WU) 3: Valued package (Paraffin coating; Double aluminum foil bag; Vacuum packaging) 4: Efficient delivery

Best price 2-Ethyl-2-adamantanol In stock

Cas:14648-57-8

Min.Order:1 Gram

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Type:Other

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SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

2-Ethyl-2-AdaMantanol

Cas:14648-57-8

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

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Siwei Development Group Ltd.

Product name: 2-Ethyl-2-Adamantanol CAS No.:14648-57-8 Molecule Formula:C12H20O Molecule Weight:180.29 Purity: 99.0% Package: 25kg/drum Description:White to off-white crystalline powder Manufacture Standards:Enterprise Standard

High Quality 2-Ethyl-2-Adamantanol

Cas:14648-57-8

Min.Order:1 Kilogram

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Type:Trading Company

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Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

2-Ethyl-2-adamantanol

Cas:14648-57-8

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

2-Ethyl-2-adamantanol

Cas:14648-57-8

Min.Order:1 Milligram

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Synthetic route

2-Adamantanone
700-58-3

2-Adamantanone

ethyllithium
811-49-4

ethyllithium

2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

Conditions
ConditionsYield
In tetrahydrofuran at 0℃; for 2h; Inert atmosphere;100%
Stage #1: 2-Adamantanone; ethyllithium In tetrahydrofuran; diethyl ether; benzene at 0 - 20℃; for 2h; Inert atmosphere;
Stage #2: With ammonium chloride In tetrahydrofuran; diethyl ether; water; benzene Inert atmosphere;
94%
In tetrahydrofuran; benzene at 0℃;94%
In diethyl ether; benzene
2-Adamantanone
700-58-3

2-Adamantanone

ethylmagnesium bromide
925-90-6

ethylmagnesium bromide

A

1-adamantanol
700-57-2

1-adamantanol

B

2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

Conditions
ConditionsYield
Stage #1: ethylmagnesium bromide With (trimethylsilyl)methylmagnesium chloride; lithium chloride; zinc(II) chloride In tetrahydrofuran; diethyl ether at 20℃; Grignard addition;
Stage #2: 2-Adamantanone In tetrahydrofuran; diethyl ether at 0℃; for 3h; Grignard addition;
A 16%
B 80%
In tetrahydrofuran; diethyl ether at 0℃; Grignard addition;A 80%
B 18%
ethylmagnesium iodide
10467-10-4

ethylmagnesium iodide

2-Adamantanone
700-58-3

2-Adamantanone

ethyl iodide
75-03-6

ethyl iodide

A

1-adamantanol
700-57-2

1-adamantanol

B

2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

Conditions
ConditionsYield
With magnesium In tetrahydrofuran
2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

2-ethyladamantane
14451-87-7

2-ethyladamantane

Conditions
ConditionsYield
With trifluoroacetic acid In hexane at 25 - 50℃; for 51h;89%
2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

C12H19N3

C12H19N3

Conditions
ConditionsYield
With sodium azide; trifluoroacetic acid In dichloromethane at 0 - 20℃; for 28h;80%
With sodium azide; trifluoroacetic acid In dichloromethane at 0 - 20℃; for 28h;80%
With sodium azide; sulfuric acid; water In chloroform at 0 - 20℃;
2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

5-(1-iodoethylydene)-4-oxatricyclo<4.3.1.1.3,8>undecane
74693-81-5

5-(1-iodoethylydene)-4-oxatricyclo<4.3.1.1.3,8>undecane

Conditions
ConditionsYield
With lead(IV) acetate; iodine; calcium carbonate In benzene for 3h; Heating;33%
2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

A

2-Adamantanone
700-58-3

2-Adamantanone

B

2-Hydroxy-2-adamantyl methyl ketone
66633-37-2

2-Hydroxy-2-adamantyl methyl ketone

C

2-Acetoxy-2-adamantyl methyl ketone

2-Acetoxy-2-adamantyl methyl ketone

D

2-(1-Acetoxyethyl)-2-adamantanol

2-(1-Acetoxyethyl)-2-adamantanol

Conditions
ConditionsYield
With nitric acid; acetic anhydride at 20℃; for 1h; Further byproducts given;A 32%
B 10%
C 15%
D 19%
2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

A

2-Adamantanone
700-58-3

2-Adamantanone

B

1-(2-Adamantylidene)-1-nitroethane

1-(2-Adamantylidene)-1-nitroethane

C

2-Acetoxy-2-adamantyl methyl ketone

2-Acetoxy-2-adamantyl methyl ketone

D

2-(1-Acetoxyethyl)-2-adamantanol

2-(1-Acetoxyethyl)-2-adamantanol

Conditions
ConditionsYield
With nitric acid; acetic anhydride at 20℃; for 1h; Further byproducts given;A 32%
B 7%
C 15%
D 19%
2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

acetic anhydride
108-24-7

acetic anhydride

A

2-Adamantanone
700-58-3

2-Adamantanone

B

2-Hydroxy-2-adamantyl methyl ketone
66633-37-2

2-Hydroxy-2-adamantyl methyl ketone

C

2-Acetoxy-2-adamantyl methyl ketone

2-Acetoxy-2-adamantyl methyl ketone

D

2-(1-Acetoxyethyl)-2-adamantanol

2-(1-Acetoxyethyl)-2-adamantanol

Conditions
ConditionsYield
With nitric acid at 20℃; for 1h; Further byproducts given;A 32%
B 10%
C 15%
D 19%
2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

chloroacetyl chloride
79-04-9

chloroacetyl chloride

2-chloroacetoxy-2-ethyladamantane
625122-38-5

2-chloroacetoxy-2-ethyladamantane

Conditions
ConditionsYield
With pyridine In tetrahydrofuran at 0 - 20℃; for 24.25h;22.2%
2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

(1r,3r,5R*,7S*)-2-ethylideneadamantane
13376-16-4

(1r,3r,5R*,7S*)-2-ethylideneadamantane

Conditions
ConditionsYield
With iodine In xylene Heating;
With pyridine; thionyl chloride at -5℃;
With toluene-4-sulfonic acid In toluene
2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

2-Bromo-2-ethyl-adamantane

2-Bromo-2-ethyl-adamantane

Conditions
ConditionsYield
With phosphorus tribromide
2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

C12H19(1+)

C12H19(1+)

Conditions
ConditionsYield
With fluorosulfonylchloride; antimony pentafluoride; fluorosulphonic acid In dichloromethane-d2 at -140℃;
2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

C13H18Cl2

C13H18Cl2

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: I2 / xylene / Heating
2: aq. NaOH, 2NEt3>Cl / benzene
View Scheme
2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

C12H19(2)H
129302-82-5

C12H19(2)H

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: PBr3
2: (n-Bu)3SnD / Irradiation
View Scheme
2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

2-ethyl-2-adamantyl alkoxy lithium
374595-26-3

2-ethyl-2-adamantyl alkoxy lithium

Conditions
ConditionsYield
With n-butyllithium In tetrahydrofuran; hexane at 0 - 20℃; for 1.68333 - 1.7h;
2-Adamantanone
700-58-3

2-Adamantanone

adamantane
281-23-2

adamantane

2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

A

2-ethyladamantan-2-yl methacrylate
209982-56-9

2-ethyladamantan-2-yl methacrylate

B

N,N,N',N'-tetraethylurea
1187-03-7

N,N,N',N'-tetraethylurea

Conditions
ConditionsYield
A n/a
B 6.3 wt %
2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

2-ethyltricyclo[3.3.1.1]decan-2-amine hydrochloride
1215574-74-5

2-ethyltricyclo[3.3.1.1]decan-2-amine hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium azide; trifluoroacetic acid / dichloromethane / 28 h / 0 - 20 °C
2: lithium aluminium tetrahydride / diethyl ether / 5 h / Reflux
View Scheme
2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

C21H28O5

C21H28O5

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: dmap / tetrahydrofuran / 0.5 h / 23 - 50 °C
1.2: 10 h / 50 °C
2.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 6 h / 23 °C
View Scheme
2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

C22H14F7O2S(1+)*C23H27F2O9S(1-)

C22H14F7O2S(1+)*C23H27F2O9S(1-)

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: dmap / tetrahydrofuran / 0.5 h / 23 - 50 °C
1.2: 10 h / 50 °C
2.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 6 h / 23 °C
3.1: 1 h / 23 °C
View Scheme
5-norbornene-2,3-dicarboxylic anhydride
826-62-0, 85081-15-8, 85081-16-9

5-norbornene-2,3-dicarboxylic anhydride

2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

C21H28O4

C21H28O4

Conditions
ConditionsYield
Stage #1: 5-norbornene-2,3-dicarboxylic anhydride With dmap In tetrahydrofuran at 23 - 50℃; for 0.5h;
Stage #2: 2-ethyl-2-adamantanol In tetrahydrofuran at 50℃; for 10h;
2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

C5H3F2N2O4S(1-)*C22H14F7O2S(1+)

C5H3F2N2O4S(1-)*C22H14F7O2S(1+)

C22H14F7O2S(1+)*C14H19F2O5S(1-)

C22H14F7O2S(1+)*C14H19F2O5S(1-)

Conditions
ConditionsYield
at 23℃; for 1h;
2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

C18H15S(1+)*C20H25F2O9S(1-)

C18H15S(1+)*C20H25F2O9S(1-)

C18H15S(1+)*C32H43F2O9S(1-)

C18H15S(1+)*C32H43F2O9S(1-)

Conditions
ConditionsYield
Stage #1: C18H15S(1+)*C20H25F2O9S(1-) With 1,1'-carbonyldiimidazole In chloroform at 23℃; for 0.5h;
Stage #2: 2-ethyl-2-adamantanol In chloroform at 23℃; for 18h;
2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

C18H15S(1+)*C21H23F2O9S(1-)

C18H15S(1+)*C21H23F2O9S(1-)

C18H15S(1+)*C33H41F2O9S(1-)

C18H15S(1+)*C33H41F2O9S(1-)

Conditions
ConditionsYield
Stage #1: C18H15S(1+)*C21H23F2O9S(1-) With 1,1'-carbonyldiimidazole In chloroform at 23℃; for 0.5h;
Stage #2: 2-ethyl-2-adamantanol In chloroform at 23℃; for 18h;
2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

Camphorsulfonyl chloride
21286-54-4

Camphorsulfonyl chloride

C22H34O4S

C22H34O4S

Conditions
ConditionsYield
Stage #1: 2-ethyl-2-adamantanol With pyridine In tetrahydrofuran at 23℃; for 0.5h;
Stage #2: Camphorsulfonyl chloride In tetrahydrofuran at 5 - 23℃; for 19h;
2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

2-ethyltricyclo[3.3.1.13,7]decan-2-amine
313241-19-9

2-ethyltricyclo[3.3.1.13,7]decan-2-amine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium azide; trifluoroacetic acid / dichloromethane / 28 h / 0 - 20 °C
2: lithium aluminium tetrahydride / diethyl ether / 5 h / Reflux
View Scheme
2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

2,3,5,6-tetrafluoro-4-hydroxybenzoic acid
652-34-6

2,3,5,6-tetrafluoro-4-hydroxybenzoic acid

C19H20F4O3

C19H20F4O3

Conditions
ConditionsYield
Stage #1: 2,3,5,6-tetrafluoro-4-hydroxybenzoic acid With 1,1'-carbonyldiimidazole In acetonitrile at 23 - 60℃; for 2h;
Stage #2: 2-ethyl-2-adamantanol In acetonitrile at 60℃; for 2h;
2-ethyl-2-adamantanol
14648-57-8

2-ethyl-2-adamantanol

5-Hydroxyisophthalic acid
618-83-7

5-Hydroxyisophthalic acid

C32H42O5

C32H42O5

Conditions
ConditionsYield
Stage #1: 5-Hydroxyisophthalic acid With 1,1'-carbonyldiimidazole In acetonitrile at 23 - 60℃; for 2h;
Stage #2: 2-ethyl-2-adamantanol In acetonitrile at 60℃; for 2h;

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