Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:151-10-0
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiry1,3-Dimethoxybenzene CAS 151-10-0 Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed additives, Fine chemicals in distri
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inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
1,3 Dimethoxybenzene CAS No.: 151-10-0 Molecular Formula: C8H10O2 Molecular Weight: 138.16 Structural formula: A. Physical & Chemical Properties: 1.Density:1.05 2.Melting point: -52℃ 3.Boiling point: 217℃ 4.Refractive lndex: 1.533-1
Cas:151-10-0
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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inquiryHebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car
Cas:151-10-0
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inquiryProduct Name: Dimethoxybenzene Synonyms: 1,3-methoxybenzenel;1,3-Dimethoxybenzene, 97+%;Dimethylresorcinol, Resorcinol dimethyl ether;3-DiMethoxybenzene;1,3-DiMethoxybenzene, 99% 100GR;1,3-DiMethoxybenzene, 99% 5GR;RESORCINOL DIMETHYL
Cas:151-10-0
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
Cas:151-10-0
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:151-10-0
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inquiryName: m-Dimethoxybenzene CAS:151-10-0 MF: C8H10O2 Appearance:clear colorless liquid Storage:Preserve in well-closed, light-resistant and airtight containers. Package:25kg Application: intermediate for organic synthesis Transportation:By sea Port:Q
Cas:151-10-0
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:151-10-0
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inquiryProduct Name: Dimethoxybenzene Synonyms: 1,3-methoxybenzenel;1,3-Dimethoxybenzene, 97+%;3-DiMethoxybenzene;Benzene,1,3-dimethoxy-;Dimethylether resorcinolu;dimethyletherresorcinolu;Dimethylresorinol;m-dimethoxy-benzen CAS: 151-10-0 MF: C8
Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:151-10-0
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:151-10-0
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Cas:151-10-0
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inquiryAdvantage 1: The product passed the professional production process and quality inspection, the purity is 99% +. 2: Highly qualified engineers to provide technical documents and service. 3: We could provide sample for your test. 4: High qualit
Cas:151-10-0
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:151-10-0
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Cas:151-10-0
Min.Order:1 Gram
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:151-10-0
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inquiryProduct name: 1,3-Dimethoxybenzene CAS No.: 151-10-0 Molecule Formula:C8H10O2 Molecule Weight:138.16 Purity: 99.0% Package: 200kg/drum Description:Clear colorless to light yellow liquid Manufacture Standards:Enterprise Standard
Cas:151-10-0
Min.Order:1 Kilogram
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:151-10-0
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:151-10-0
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inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe
Cas:151-10-0
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inquiryCapability on chemical synthesis1. Beijing High-Tech Enterprises2. Strong R&D Team3. 8 years of experiences in R & D of high-tech Catalyst;4. 5000 production techniques, 69 items of national patents, and 360 kinds of products on sales;5. The producti
Conditions | Yield |
---|---|
With trifluoroacetic acid; palladium(II) trifluoroacetate In dimethyl sulfoxide; N,N-dimethyl-formamide at 70℃; for 24h; | 100% |
With palladium(II) trifluoroacetate; trifluoroacetic acid In dimethyl sulfoxide; N,N-dimethyl-formamide at 70℃; for 24h; | 100% |
With copper(I) oxide; N,N,N,N,-tetramethylethylenediamine In 1-methyl-pyrrolidin-2-one at 140℃; for 2h; Inert atmosphere; | 92% |
Conditions | Yield |
---|---|
With 1,1,1,3',3',3'-hexafluoro-propanol at 20℃; for 7h; UV-irradiation; | A 100% B n/a |
Conditions | Yield |
---|---|
With Methyl formate; copper(l) chloride In methanol at 110℃; for 2h; Autoclave; | 98% |
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 65℃; for 25h; | 96% |
With potassium carbonate In acetone for 4h; Reflux; | 94% |
With potassium carbonate In acetone for 0.0666667h; Heating; Microwave irradiation; | 91% |
Conditions | Yield |
---|---|
With silver carbonate In dimethyl sulfoxide at 140℃; for 16h; | 96% |
With silver(I) acetate; potassium carbonate In 1-methyl-pyrrolidin-2-one at 120℃; for 16h; Inert atmosphere; | 89% |
With palladium diacetate; dimethyl sulfoxide; silver carbonate; copper(ll) bromide In tetrahydrofuran at 110℃; for 36h; | 15% |
(2,6-dimethoxyphenyl)boronic acid
1,3-Dimethoxybenzene
Conditions | Yield |
---|---|
With n-butyl acrylate; SiO2-Rh(0) In water; toluene at 100℃; for 48h; | 95% |
With acetic acid In 1,4-dioxane at 100℃; for 5h; Enzymatic reaction; | 91% |
With acetic acid at 130℃; for 3h; Green chemistry; | 88% |
Conditions | Yield |
---|---|
Stage #1: 3-methoxyphenyl bromide With potassium hydroxide; tris-(dibenzylideneacetone)dipalladium(0); tert-butyl XPhos In 1,4-dioxane; water at 100℃; for 1.5h; Stage #2: methyl iodide With cetyltrimethylammonim bromide In 1,4-dioxane; water at 100℃; for 1h; | 94% |
2,4-dimethoxyphenylboronic acid
1,3-Dimethoxybenzene
Conditions | Yield |
---|---|
With acetic acid In 1,4-dioxane at 100℃; for 5h; Enzymatic reaction; | 93% |
Conditions | Yield |
---|---|
With sodium In toluene; butan-1-ol at 111℃; for 3.5h; | A 8% B 92% |
A
2-(4'-methoxyphenyl)-7-methoxynaphthalene
B
1,3-Dimethoxybenzene
Conditions | Yield |
---|---|
With trifluoroacetic acid In water at 80℃; for 0.5h; Diels-Alder Cycloaddition; | A 92% B n/a |
1-bromo-3,5-dimethoxybenzene
1,3-Dimethoxybenzene
Conditions | Yield |
---|---|
With isopropyl alcohol for 10h; Schlenk technique; Inert atmosphere; Irradiation; Heating; | 92% |
With 4-methyl-morpholine; tetrahydroxydiboron; 5%-palladium/activated carbon In 1,2-dichloro-ethane at 50℃; for 2h; | 86% |
With 1,4-dioxane; 1,10-Phenanthroline; sodium hydride In mineral oil at 140℃; for 22h; Schlenk technique; Inert atmosphere; | 65% |
With N-ethyl-N,N-diisopropylamine In acetonitrile for 16h; Irradiation; | 86 %Spectr. |
With 1,3-dimethyl-2-phenyl-2,3-dihydro-1H-benzo[d]imidazole; C41H39IrN6 In N,N-dimethyl-formamide at 45℃; for 24h; Reagent/catalyst; Irradiation; Glovebox; | 95 %Chromat. |
trifluoromethanesulfonic acid 2,6-dimethoxyphenyl ester
1,3-Dimethoxybenzene
Conditions | Yield |
---|---|
With hydrogen; triethylamine; palladium on activated charcoal In methanol under 3361.5 Torr; other solvent, other temp., other reagents, other catalysts; | 90% |
With hydrogen; palladium on activated charcoal In methanol under 3361.5 Torr; Product distribution; other catalysts, other solvent, other temp., other reagent; | 90% |
With tetra-n-butyltin(IV); bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; lithium chloride | 86% |
With 2,6-di-tert-butyl-4-methyl-phenol; tetra-n-butyltin(IV); bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; lithium chloride In N,N-dimethyl-formamide at 120℃; | 86% |
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 20℃; for 48h; | 90% |
With potassium carbonate In acetone at 20℃; Inert atmosphere; | 87.69% |
With potassium carbonate In N,N-dimethyl-formamide for 3h; |
1-iodo-2,4-dimethoxybenzene
1,3-Dimethoxybenzene
Conditions | Yield |
---|---|
With tetrahydrofuran; 1,10-Phenanthroline; potassium tert-butylate at 70℃; for 24h; Schlenk technique; Inert atmosphere; | 90% |
With potassium tert-butylate at 80℃; for 12h; Inert atmosphere; Schlenk technique; | 87% |
Stage #1: 1-iodo-2,4-dimethoxybenzene With chloro-trimethyl-silane; ethylene dibromide; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; lithium chloride; cobalt(II) chloride; zinc In tetrahydrofuran at 20℃; for 7h; Inert atmosphere; Stage #2: With iodine In tetrahydrofuran for 0.5h; | 7 %Chromat. |
1,3-Dimethoxybenzene
Conditions | Yield |
---|---|
With dihydrogen peroxide In tetrahydrofuran for 1h; Heating; | 89% |
Conditions | Yield |
---|---|
With layered double hydroxide - supported L-methionine at 180℃; for 6h; Autoclave; chemoselective reaction; | 89% |
Conditions | Yield |
---|---|
With trifluoroacetic acid In water at 80℃; for 0.5h; Diels-Alder Cycloaddition; | A 87% B n/a |
Conditions | Yield |
---|---|
With potassium In tetrahydrofuran for 24h; Ambient temperature; | 86% |
With ethanol; sodium | |
With water 1) THF, RT, 24h; Yield given. Multistep reaction; | |
With 2-iodo-propane; potassium 1.) THF, rt, 24 h; 2.) 0 deg C, 4 h; Yield given. Multistep reaction; |
1,2,3-trimethoxybenzene
A
1,3-dimethoxy-2-hydroxy-benzene
B
2,3-dimethoxyphenol
C
1,3-Dimethoxybenzene
Conditions | Yield |
---|---|
With potassium In tetrahydrofuran for 24h; Ambient temperature; | A n/a B n/a C 85% |
Conditions | Yield |
---|---|
With iodine at 60℃; for 2h; | 85% |
Trimethyl borate
potassium 4-methoxybenzoate
A
methyl 4-methoxybenzoate
B
1,3-Dimethoxybenzene
Conditions | Yield |
---|---|
With oxygen; copper diacetate; silver carbonate In N,N-dimethyl-formamide at 150℃; under 760.051 Torr; for 36h; | A 8% B 83% |
Conditions | Yield |
---|---|
With oxygen; copper diacetate; silver carbonate In N,N-dimethyl-formamide at 140℃; under 760.051 Torr; for 36h; | 82% |
With silver carbonate; copper(ll) bromide In N,N-dimethyl-formamide at 170℃; for 0.666667h; Microwave irradiation; | 41% |
2,4 dimethoxybenzoic acid
Benzo[b]thiophene
A
2-(3',5'-dimethoxyphenyl)benzothiophene
B
1,3-Dimethoxybenzene
Conditions | Yield |
---|---|
With dipotassium hydrogenphosphate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver carbonate In N,N-dimethyl-formamide at 100℃; for 24h; Inert atmosphere; Glovebox; Schlenk technique; | A 82% B 16% |
1-Bromo-2,4-dimethoxybenzene
1,3-Dimethoxybenzene
Conditions | Yield |
---|---|
Stage #1: 1-Bromo-2,4-dimethoxybenzene With palladium dichloride In water at 20℃; for 0.0333333h; Stage #2: With 1,1,3,3-Tetramethyldisiloxane for 0.133333h; | 81% |
With bis(1,5-cyclooctadiene)nickel (0); triphenylphosphine; trifluoroacetic acid In toluene at 70℃; for 2h; | 53% |
With 2,2'-azobis(isobutyronitrile); hypophosphorous acid; sodium hydrogencarbonate In ethanol for 5h; Heating; | 9% |
With N-ethyl-N,N-diisopropylamine In acetonitrile for 16h; Irradiation; | 89 %Spectr. |
2-iodo-1,3-dimethoxybenzene
1,3-Dimethoxybenzene
Conditions | Yield |
---|---|
With 2-(2-methoxyethoxy)ethyl alcohol; oxygen; sodium hydride In 1,4-dioxane at 20℃; for 24h; Schlenk technique; chemoselective reaction; | 81% |
2,4-Dimethoxyaniline
A
2,4-dimethoxybenzenediazonium tetrafluoroborate
B
1,3-Dimethoxybenzene
Conditions | Yield |
---|---|
With tetrafluoroboric acid; sodium nitrite In water | A 79% B n/a |
N-acetylindole
2,4 dimethoxybenzoic acid
A
C18H17NO3
B
2-(2',4'-dimethoxyphenyl)-N-acetylindole
C
1,3-Dimethoxybenzene
Conditions | Yield |
---|---|
With 1-oxothiolane; palladium(II) trifluoroacetate; propionic acid; silver carbonate In 1,4-dioxane at 80℃; for 24h; Inert atmosphere; | A n/a B 78% C 84 %Chromat. |
3,5-dimethoxyphenyl pivalate
1,3-Dimethoxybenzene
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)nickel(0); (dimethoxy)methylsilane; tricyclohexylphosphine In toluene at 80℃; for 12h; Inert atmosphere; | 78% |
With bis(1,5-cyclooctadiene)nickel (0); sodium formate; 1,2-bis-(dicyclohexylphosphino)ethane In toluene at 140℃; for 24h; Inert atmosphere; Schlenk technique; | 72% |
3,5-dimethoxy-benzonitrile
1,3-Dimethoxybenzene
Conditions | Yield |
---|---|
With chloro(1,5-cyclooctadiene)rhodium(I) dimer; tri-n-butyl phosphite; chlorotriisopropylsilane In ethylcyclohexane at 130℃; for 15h; Inert atmosphere; | 76% |
1,3-Dimethoxybenzene
1-Bromo-2,4-dimethoxybenzene
Conditions | Yield |
---|---|
With benzyltriphenylphosphonium peroxodisulfate; potassium bromide In acetonitrile for 4.5h; Heating; | 100% |
With N-Bromosuccinimide | 100% |
With N-Bromosuccinimide; silica gel In tetrachloromethane at 30℃; for 2h; | 99% |
1,3-Dimethoxybenzene
1,3-dichloro-4,6-dimethoxybenzene
Conditions | Yield |
---|---|
With sulfuryl dichloride In dichloromethane at 0 - 20℃; | 100% |
With N-chloro-succinimide; diphenyldisulfane In acetonitrile at 20℃; | 97% |
With sulfuryl dichloride In dichloromethane at 0 - 20℃; for 8h; Chlorination; | 94% |
1,3-Dimethoxybenzene
4,6-dibromo-1,3-dimethoxybenzene
Conditions | Yield |
---|---|
With oxygen; lithium bromide; copper(ll) bromide In acetic acid at 60℃; under 760.051 Torr; regioselective reaction; | 100% |
With N-Bromosuccinimide; diphenyldisulfane In acetonitrile at 20℃; for 1h; Reagent/catalyst; | 100% |
With bromine In dichloromethane Product distribution; other substrates, amounts of reagent; | 99% |
4-nitrobenzaldehdye
1,3-Dimethoxybenzene
4,4'-((4-nitrophenyl)methylene)bis(1,3-dimethoxybenzene)
Conditions | Yield |
---|---|
With o-benzenedisulfonimide at 20℃; for 2h; Friedel Crafts alkylation; neat (no solvent); | 100% |
With 1-methyl-3-(propyl-3-sulfonyl)imidazolium trifluoromethanesulfonate In neat (no solvent) at 40℃; for 6h; Friedel-Crafts Alkylation; Green chemistry; | 87% |
With sulfuric acid | 80% |
With 3-methyl-1-(4-sulfobutyl)imidazol-3-ium bis((trifluoromethyl)sulfonyl)azanide In neat (no solvent) at 40℃; for 1h; | 80% |
With silica-supported sodium hydrogen sulfate at 115℃; for 3h; Inert atmosphere; Neat (no solvent); | 79% |
trifluorormethanesulfonic acid
1H-2,4,6-tri-isopropyl-1,3,5-triazinium triflate
1,3-Dimethoxybenzene
2-(2,4-dimethoxyphenyl)-2,4,6-tri-isopropyl-1,2-dihydro-1,3,5-triazinium triflate
Conditions | Yield |
---|---|
In benzene for 1.5h; Ambient temperature; | 100% |
bis(2,2,2-trichloroethyl)azodicarboxylate
1,3-Dimethoxybenzene
1-(2,4-dimethoxyphenyl)-1,2-hydrazinedicarboxylic acid bis(2,2,2-trichloroethyl) ester
Conditions | Yield |
---|---|
With zinc(II) iodide In dichloromethane at 25℃; for 0.25h; | 100% |
1,3-Dimethoxybenzene
Conditions | Yield |
---|---|
With perchloric acid; d(4)-methanol at 75℃; for 72h; Inert atmosphere; | 100% |
With water-d2; sulfuric acid-d2 for 48h; Ambient temperature; | |
With deuteromethanol; toluene-4-sulfonic acid at 70℃; for 72h; deuteration; |
3-Bromopropionyl chloride
1,3-Dimethoxybenzene
3-bromo-1-(2,4-dimethoxy-phenyl)-propan-1-one
Conditions | Yield |
---|---|
titanium tetrachloride In dichloromethane at 0 - 20℃; for 0.5h; Friedel-Crafts reaction; | 100% |
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid; 1,1,1,3',3',3'-hexafluoro-propanol at 60℃; for 24h; | 100% |
With aluminum (III) chloride In 1,2-dichloro-ethane for 0.5h; Reflux; | 85% |
diphenylmethyl trimethylsilyl ether
1,3-Dimethoxybenzene
((4,6-dimethoxy-1,3-phenylene)bis(methanetriyl))tetrabenzene
Conditions | Yield |
---|---|
With iron(III) chloride In 1,2-dichloro-ethane at 20℃; for 20h; Friedel-Crafts Alkylation; Inert atmosphere; regioselective reaction; | 100% |
1,3-Dimethoxybenzene
4,6-Bis(4,4’-difluorobenzhydryl)-1,3-dimethoxybenzene
Conditions | Yield |
---|---|
With iron(III) chloride In 1,2-dichloro-ethane at 20℃; for 0.25h; Friedel-Crafts Alkylation; Inert atmosphere; regioselective reaction; | 100% |
nitropentafluoroacetone
1,3-Dimethoxybenzene
1,3-Dimethoxy-4-(1-hydroxy-2-nitropentafluoroisopropyl)benzene
Conditions | Yield |
---|---|
In nitromethane at 20℃; for 144h; | 99.7% |
Conditions | Yield |
---|---|
With scandium tris(trifluoromethanesulfonate) In acetonitrile for 0.5h; Time; Friedel-Crafts Acylation; Inert atmosphere; Microwave irradiation; Heating; Green chemistry; | 99% |
With GALDEN(R) SV 135; hafnium(IV) bis(perfluorooctanesulfonyl)amide complex In chlorobenzene at 70℃; for 1h; Friedel-Crafts acylation; | 94% |
With Hierarchical-Beta zeolite In neat (no solvent) at 119.84℃; for 4h; Catalytic behavior; Reagent/catalyst; Friedel-Crafts Acylation; Green chemistry; | 94% |
Conditions | Yield |
---|---|
With indium(III) tosylate In dodecane; nitromethane for 2h; Solvent; Reagent/catalyst; Temperature; Time; Friedel-Crafts Acylation; Schlenk technique; Reflux; | 99% |
With aluminum (III) chloride In dichloromethane at 0 - 20℃; for 1h; | 88% |
With CuII-based Polymeric Sulfonic Acid Catalyst In nitromethane for 0.5h; Reagent/catalyst; Friedel-Crafts Acylation; Schlenk technique; Reflux; | 84% |
1,3-Dimethoxybenzene
1-iodo-2,4-dimethoxybenzene
Conditions | Yield |
---|---|
With iodine; urea hydrogen peroxide adduct for 10h; Sonication; | 99% |
With β-pyridinium dichloroiodide In 2,2,2-trifluoroethanol Reagent/catalyst; Solvent; | 99% |
With hydrogenchloride; α,α,α-trifluorotoluene; dihydrogen peroxide; iodine In water; acetonitrile at 20℃; for 4h; | 99% |
1,3-Dimethoxybenzene
1,5-diiodo-2,4-dimethoxy-benzene
Conditions | Yield |
---|---|
With dihydrogen peroxide; iodine In water for 0.75h; Sonication; | 99% |
With N,N,N-trimethylbenzenemethanaminium dichloroiodate; zinc(II) chloride In acetic acid for 0.166667h; Ambient temperature; | 98% |
With dihydrogen peroxide; iodine In water at 50℃; for 24h; Green chemistry; | 96% |
Hexafluoroacetone
1,3-Dimethoxybenzene
2-(2,4-Dimethoxy-phenyl)-1,1,1,3,3,3-hexafluoro-propan-2-ol
Conditions | Yield |
---|---|
at 20℃; for 124h; | 99% |
methyl 3,3,3-trifluoropyruvate
1,3-Dimethoxybenzene
2-(2,4-Dimethoxy-phenyl)-3,3,3-trifluoro-2-hydroxy-propionic acid methyl ester
Conditions | Yield |
---|---|
at 20℃; for 24h; | 99% |
With In(OSO2CF3)3 In water at 20℃; for 12h; Friedel-Crafts reaction; | 84% |
samarium diiodide bis(tetrahydrofuran) In dichloromethane at 20℃; for 114h; Friedel-Crafts reaction; | 75% |
2',3',4',5',6'-pentamethylacetophenone
1,3-Dimethoxybenzene
A
pentamethylbenzene,
B
2',4'-dimethoxyacetophenone
Conditions | Yield |
---|---|
trifluoroacetic acid for 10h; Heating; | A 99% B 37% |
bis(2,2,2-trichlorethyl)azodicarboxylate
1,3-Dimethoxybenzene
1-(2,4-dimethoxyphenyl)-1,2-hydrazinedicarboxylic acid bis(2,2,2-trichloroethyl) ester
Conditions | Yield |
---|---|
With lithium perchlorate In diethyl ether for 2h; Ambient temperature; | 99% |
4-hydroxymethyl-1,2,5-trimethyl-1H-pyrrole-3-carboxylic acid dibutylamide
1,3-Dimethoxybenzene
Conditions | Yield |
---|---|
With scandium tris(trifluoromethanesulfonate) In nitromethane; 1,2-dichloro-ethane at 20℃; for 24h; Alkylation; Friedel-Crafts alkylation; | 99% |
1,3-Dimethoxybenzene
2,3,5,6-tetramethyl-4'-thiaspiro[cyclohexane-4,3'-isochroman]-2,5-dien-1,1'-dione
Conditions | Yield |
---|---|
With trimethylsilyl trifluoromethanesulfonate In acetonitrile at 0℃; for 0.166667h; | 99% |
bis(pinacol)diborane
1,3-Dimethoxybenzene
3,5-dimethoxyphenylboronic acid pinacol ester
Conditions | Yield |
---|---|
With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 1,1'-di(pyridin-2-yl)-1,1',3,3'-tetrahydro-2,2'-bibenzo[d][1,3,2]diazaborole at 100℃; for 16h; Inert atmosphere; | 99% |
With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; cyclopentyl methyl ether; 1,1'-di(pyridin-2-yl)-1,1',3,3'-tetrahydro-2,2'-bibenzo[d][1,3,2]diazaborole at 100℃; for 16h; Schlenk technique; Inert atmosphere; | 95% |
With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine In tert-butyl methyl ether at 80℃; for 1h; Solvent; Microwave irradiation; | 90% |
1,3-Dimethoxybenzene
Conditions | Yield |
---|---|
With silver hexafluoroantimonate; (triphenylphosphine)gold(I) chloride In diethyl ether at 20℃; for 2h; | 99% |
Stage #1: 1,3-Dimethoxybenzene With silver hexafluoroantimonate; (triphenylphosphine)gold(I) chloride In diethyl ether at 20℃; for 0.05h; Inert atmosphere; Stage #2: (E)-(1-phenylhept-1-en-6-yne-4,4-diyldisulfonyl)dibenzene In diethyl ether at 20℃; for 2h; Inert atmosphere; diastereoselective reaction; | 99% |
1,3-Dimethoxybenzene
2-(2',4'-dimethoxyphenyl)-4-methoxy-6-tert-butylphenol
Conditions | Yield |
---|---|
With aluminium pillared montmorillonite In dichloromethane; 1,1,1,3',3',3'-hexafluoro-propanol at 20℃; chemoselective reaction; | 99% |
benzyl azide
1,3-Dimethoxybenzene
N-{[2,4-bis(methyloxy)phenyl]methyl}aniline
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid In dichloromethane at 20℃; for 0.05h; Aube-Schmidt rearrangement; | 99% |
Conditions | Yield |
---|---|
With aluminum (III) chloride In dichloromethane at 0 - 20℃; Friedel-Crafts Acylation; | 99% |
Conditions | Yield |
---|---|
With aluminum (III) chloride In dichloromethane at 0 - 20℃; | 99% |
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