DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:1535-75-7
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inquiry2-(Trifluoromethoxy)aniline Basic information Product Name: 2-(Trifluoromethoxy)aniline Synonyms: 2-(TrifloroMethoxy)aniline;2-(TrifluoroMethoxy)aniline, 97.5%;2-(Trifluoromethoxy)aniline,o-Aminotrifluoromethoxybenzene;2-(TRIFLUOROMETHOXY)ANILI
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Min.Order:1 Gram
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryAppearance:white or yellowish white flaky crystal Storage:Keep the sun from direct sunlight ;prevention against high temperature Package:As customer request Application:Used for research and industrial manufacture. Transportatio
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inquiry2-(Trifluoromethoxy)aniline Chemical Properties Boiling point 61-63 °C (15 mmHg) density 1,301 g/cm3 refractive index 1.4614-1.4634 Fp 54°C pka 2.45±0.10(Predicted) form Liquid color Clear colorless to yellow
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
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inquiry1-bromo-2-(trifluoromethoxy)benzene
2-trifluoromethoxy aniline
Conditions | Yield |
---|---|
With ammonium hydroxide; L-2-O-methyl-chiro-inositol; copper(II) acetate monohydrate In 1-methyl-pyrrolidin-2-one at 110℃; for 12h; | 82% |
1-chloro-4-(trifluoromethoxy)benzene
A
2-trifluoromethoxy aniline
B
m-trifluoromethoxyaniline
Conditions | Yield |
---|---|
Stage #1: 1-chloro-4-(trifluoromethoxy)benzene With sulfuric acid; nitric acid at 0 - 45℃; Stage #2: With palladium on activated charcoal; hydrogen; triethylamine In methanol at 80℃; under 15001.5 Torr; Temperature; Pressure; Autoclave; Overall yield = 98 percent; Overall yield = 177.12 g; |
2-trifluoromethoxy aniline
2-(trifluoromethoxy)benzenesulfonyl chloride
2-trifluoromethoxy-benzenesulphonic acid amide
Conditions | Yield |
---|---|
99.4% |
di-tert-butyl dicarbonate
2-trifluoromethoxy aniline
tert-butyl N-[2-(trifluoromethoxy)phenyl]carbamate
Conditions | Yield |
---|---|
In toluene at 100℃; for 2h; | 98% |
In toluene Heating; | 76% |
2-trifluoromethoxy aniline
ethyl acetoacetate
3-oxo-2-(2-(2-(trifluoromethoxy)phenyl)hydrazono)butanoic acid ethyl ester
Conditions | Yield |
---|---|
Stage #1: 2-trifluoromethoxy aniline With hydrogenchloride; sodium nitrite In water at 0℃; for 0.5h; Stage #2: ethyl acetoacetate With sodium acetate In ethanol; water at 0℃; | 92.3% |
Stage #1: 2-trifluoromethoxy aniline With hydrogenchloride; sodium nitrite In water at 0℃; for 0.0833333h; Stage #2: ethyl acetoacetate With ammonium acetate In ethanol; water | |
Stage #1: 2-trifluoromethoxy aniline With hydrogenchloride; sodium nitrite In water at 0℃; for 0.0833333h; Stage #2: ethyl acetoacetate With ammonium acetate In ethanol; water at 0℃; for 0.5h; |
2-trifluoromethoxy aniline
t-butyl 2-diazopropanoate
Conditions | Yield |
---|---|
With C32H30N4O4; copper(l) chloride In dichloromethane at 0℃; for 18h; Inert atmosphere; Molecular sieve; optical yield given as %ee; enantioselective reaction; | 92% |
Conditions | Yield |
---|---|
With formic acid for 12h; Reflux; | 90.56% |
Conditions | Yield |
---|---|
Stage #1: 2-trifluoromethoxy aniline With hydrogenchloride; sodium nitrite In ethanol; water at 0 - 5℃; for 0.5h; Stage #2: ethyl 2-chloro-3-oxo-butyrate With sodium acetate In ethanol; water at 0 - 25℃; | 90% |
2-trifluoromethoxy aniline
Conditions | Yield |
---|---|
With sodium nitrite In hydrogenchloride; water | 88% |
ortho-nitrobenzoic acid
2-trifluoromethoxy aniline
2-nitro-N-(2-(trifluoromethoxy)phenyl)benzamide
Conditions | Yield |
---|---|
Stage #1: ortho-nitrobenzoic acid With thionyl chloride In N,N-dimethyl-formamide; benzene Reflux; Stage #2: 2-trifluoromethoxy aniline With triethylamine In dichloromethane; N,N-dimethyl-formamide at 0 - 20℃; | 88% |
Conditions | Yield |
---|---|
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 1h; Inert atmosphere; | 87% |
Conditions | Yield |
---|---|
Stage #1: 3-bromo-3-methyl-2-indolinone With nickel(II) tetrafluoroborate hexahydrate; C42H66N4O8 In ethyl acetate at 35℃; for 0.583333h; Stage #2: With N-ethyl-N,N-diisopropylamine In ethyl acetate at 0℃; for 0.166667h; Stage #3: 2-trifluoromethoxy aniline In ethyl acetate at 0℃; for 24h; enantioselective reaction; | 86% |
Conditions | Yield |
---|---|
With hydrogenchloride; hydroxylamine hydrochloride; sodium sulfate at 55℃; Sandmeyer reaction; | 85% |
With hydrogenchloride; hydroxylamine hydrochloride; sodium sulfate at 55℃; Sandmeyer reaction; | 85% |
Conditions | Yield |
---|---|
With dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 12h; | 85% |
Conditions | Yield |
---|---|
With dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 12h; Inert atmosphere; | 85% |
2-trifluoromethoxy aniline
tetra(n-butyl)ammonium hydrogensulfate
Conditions | Yield |
---|---|
Stage #1: 2-trifluoromethoxy aniline With chlorosulfonic acid; triethylamine In dichloromethane at 0 - 20℃; Inert atmosphere; Stage #2: With sodium hydroxide In dichloromethane; water Stage #3: tetra(n-butyl)ammonium hydrogensulfate In dichloromethane; water | 85% |
Conditions | Yield |
---|---|
With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); N,N,N′,N′-tetramethyl-N″-tert-butylguanidine; 4,4'-di-tert-butyl-2,2'-bipyridine; zinc In dimethyl sulfoxide at 80℃; for 8h; Reagent/catalyst; Inert atmosphere; | 85% |
(4-bromo-3-methylphenyl)(morpholino)methanone
2-trifluoromethoxy aniline
Conditions | Yield |
---|---|
With potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); C37H43N2O4P In 1,4-dioxane at 90℃; for 18h; | 82% |
Conditions | Yield |
---|---|
With tert.-butylnitrite; C29H23N6Ru2(2+)*2Cl(1-)*6H2O; toluene-4-sulfonic acid In acetonitrile at 20℃; for 5h; Irradiation; | 81% |
Conditions | Yield |
---|---|
Stage #1: cycl-isopropylidene malonate; 2-trifluoromethoxy aniline Heating; Stage #2: With Eaton’s reagent Heating; | 81% |
2-trifluoromethoxy aniline
p-cyanophenyl isocyanate
1-(4-cyanophenyl)-3-(2-trifluoromethoxyphenyl)urea
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; | 80.4% |
Conditions | Yield |
---|---|
With iodine; oxygen; dimethyl sulfoxide; salicylic acid at 90℃; under 760.051 Torr; for 16h; Schlenk technique; regioselective reaction; | 80% |
Conditions | Yield |
---|---|
With oxygen; palladium diacetate In dimethyl sulfoxide at 130℃; under 760.051 Torr; for 12h; | 78% |
2-trifluoromethoxy aniline
Conditions | Yield |
---|---|
In methanol for 48h; Reflux; | 77% |
N-vinyl-2-oxazolidone
2-trifluoromethoxy aniline
Diethyl 2-bromomalonate
Conditions | Yield |
---|---|
With (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; triethylamine In acetonitrile at 20℃; for 3h; Inert atmosphere; Sealed tube; Irradiation; | 77% |
Conditions | Yield |
---|---|
With sodium tris(acetoxy)borohydride In dichloromethane at 20℃; for 2h; | 75% |
Conditions | Yield |
---|---|
With copper(l) iodide; boron trifluoride diethyl etherate; oxygen In dimethyl sulfoxide at 105℃; for 14h; regioselective reaction; | 75% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 30 - 35℃; for 12h; | 72.3% |
(Z)-2,2'-dibromostilbene
2-trifluoromethoxy aniline
5-(2-(trifluoromethoxy)phenyl)-5H-dibenzo[b,f]azepine
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate; bis[2-(diphenylphosphino)phenyl] ether In toluene at 120℃; for 10h; Schlenk technique; Inert atmosphere; | 72% |
2-trifluoromethoxy aniline
1,4-dinitro-1H-imidazole
4-nitro-1-{2-(trifluoromethoxy)phenyl}-1H-imidazole
Conditions | Yield |
---|---|
In methanol; water at 20℃; Darkness; | 71% |
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