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inquiryName Methoxyfenozide CAS No. 161050-58-4 Chemical name Methoxyfenozide Specification(COA) 10%SC,20%SC,24%SC,98%TC Use categ
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inquiryProduct Name: METHOXYFENOZIDE Synonyms: METHOXYFENOZIDE;Benzoic acid, 3-methoxy-2-methyl-, 2-(3,5-dimethylbenzoyl)-2-(1,1-dimethylethyl)hydrazide;methoxyfenozide (bsi, pa iso, ansi);rh-2485;N-tert-butyl-N'-(3-methoxy-2-methylbenzoly)-3,5-dimet
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Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquiry★.Best quality according to requirement ★.Competitive price in China market ★.Mature Technical support ★.Professional logistic support
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3-methoxy-2-methylbenzoyl chloride
N-(3,5-Dimethylbenzoyl)-N-tert-Butyl-Hydrazine
methoxyfenoside
Conditions | Yield |
---|---|
With triethylamine for 4h; Acylation; | 61.6% |
In 1,2-dichloro-ethane at 20℃; for 15h; |
N-(3-methoxy-2-methylbenzoyl)-N'-tert-butylhydrazine
3,5-dimethylbenzoyl chloride
methoxyfenoside
Conditions | Yield |
---|---|
With sodium hydroxide In dichloromethane |
3-methoxy-2-methylbenzoic acid
N-(3,5-Dimethylbenzoyl)-N-tert-Butyl-Hydrazine
methoxyfenoside
Conditions | Yield |
---|---|
In thionyl chloride; dichloromethane |
tert-butylhydrazine
3-methoxy-2-methylbenzoyl chloride
3,5-dimethylbenzoyl chloride
methoxyfenoside
Conditions | Yield |
---|---|
Stage #1: tert-butylhydrazine With di-tert-butyl dicarbonate; sodium hydroxide In toluene at 0 - 5℃; for 10h; Stage #2: 3,5-dimethylbenzoyl chloride With sodium hydroxide In water; toluene at 0 - 5℃; for 4h; Stage #3: 3-methoxy-2-methylbenzoyl chloride Further stages; |
3,5-dimethylbenzoic acid
methoxyfenoside
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: thionyl chloride / toluene / 6.7 h / 55 °C 2.1: di-tert-butyl dicarbonate; sodium hydroxide / toluene / 10 h / 0 °C 2.2: 5 h / 0 °C 3.1: 1,2-dichloro-ethane / 15 h / 20 °C View Scheme |
phosgene
methoxyfenoside
Conditions | Yield |
---|---|
Stage #1: methoxyfenoside With potassium tert-butylate In tetrahydrofuran at 20℃; Stage #2: phosgene In tetrahydrofuran; ethyl acetate at -78℃; | 95% |
thiophosgene
methoxyfenoside
Conditions | Yield |
---|---|
Stage #1: methoxyfenoside With potassium tert-butylate In tetrahydrofuran at 20℃; Stage #2: thiophosgene In tetrahydrofuran; ethyl acetate at -78℃; | 75% |
α-chlorobenzyl chloroformate
methoxyfenoside
N'-tert-butyl-N'-(3,5-dimethyl-benzoyl)-N-(3-methoxy-2-methyl-benzoyl)-hydrazinecarboxylic acid chloro-phenyl-methyl ester
Conditions | Yield |
---|---|
Stage #1: methoxyfenoside With potassium tert-butylate In tetrahydrofuran at 20℃; Stage #2: α-chlorobenzyl chloroformate In tetrahydrofuran at 20℃; |
methoxyfenoside
C9H8Cl2O2
N'-tert-butyl-N'-(3,5-dimethyl-benzoyl)-N-(3-methoxy-2-methyl-benzoyl)-hydrazinecarboxylic acid chloro-p-tolyl-methyl ester
Conditions | Yield |
---|---|
Stage #1: methoxyfenoside With potassium tert-butylate In tetrahydrofuran at 20℃; Stage #2: C9H8Cl2O2 In tetrahydrofuran at 20℃; |
methoxyfenoside
C9H8Cl2O2
N'-tert-butyl-N'-(3,5-dimethyl-benzoyl)-N-(3-methoxy-2-methyl-benzoyl)-hydrazinecarboxylic acid chloro-o-tolyl-methyl ester
Conditions | Yield |
---|---|
Stage #1: methoxyfenoside With potassium tert-butylate In tetrahydrofuran at 20℃; Stage #2: C9H8Cl2O2 In tetrahydrofuran at 20℃; for 4h; |
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