Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:1647-16-1
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1,9-DECADIENE CAS:1647-16-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediat
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Conditions | Yield |
---|---|
at 600℃; under 20 Torr; for 0.0333333h; | A 93% B 31% C 57% |
Conditions | Yield |
---|---|
Mo(NC6H3(CH(CH3)2)2)(CHC(CH3)2C6H5)(NC4H2(CH3)2)(OC10H9BrC10H9BrOSi(CH3)2C(CH3)3) In 1,3,5-trimethyl-benzene under 7600.51 Torr; for 16h; Product distribution / selectivity; Inert atmosphere; Sealed system; | 90% |
Re2O7/B2O3/Al2O3; tetramethylstannane In toluene under 3750.38 - 4500.45 Torr; for 92.5h; Product distribution / selectivity; | |
Re2O7/B2O3/Al2O3; tetramethylstannane In toluene under 3750.38 - 4500.45 Torr; Product distribution / selectivity; | |
With Mo[N(2,6-(i-Pr)2Ph)](CHCMe2Ph)(Me2Pyr)(OBitet) at 20℃; under 15201 Torr; for 20h; Inert atmosphere; | 93 %Chromat. |
Conditions | Yield |
---|---|
With 1-hexadecylcarboxylic acid at 340℃; for 6h; Molecular sieve; | A n/a B 88% |
Conditions | Yield |
---|---|
With methoxy(cyclooctadiene)rhodium(I) dimer; N,N-Dimethylacrylamide; 3-Methoxybenzoic acid; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In toluene at 90℃; for 24h; Inert atmosphere; Glovebox; Sealed tube; chemoselective reaction; | 88% |
Conditions | Yield |
---|---|
With nickel(II) iodide; triphenylphosphine In neat (no solvent) for 16h; Reagent/catalyst; Inert atmosphere; Sealed tube; | 85% |
With bis-triphenylphosphine-palladium(II) chloride; 3,3',5,5'-tetra(tert-butyl)biphenyl-2,2'-diol; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In neat (no solvent) at 132℃; for 3h; Inert atmosphere; | 59% |
Stage #1: 10-undecenoic acid With bis(1,5-cyclooctadiene)diiridium(I) dichloride; triphenylphosphine; potassium iodide at 20℃; for 0.5h; Inert atmosphere; Schlenk technique; Stage #2: With acetic anhydride at 160℃; for 5h; Inert atmosphere; Schlenk technique; regioselective reaction; |
2-(oct-7-en-1-yl)oxirane
1,10-decadiene
Conditions | Yield |
---|---|
With bis(acetylacetonate)nickel(II); diethylzinc In hexane; toluene at 110℃; for 48h; Inert atmosphere; | 85% |
C24H30O4
1,10-decadiene
Conditions | Yield |
---|---|
at 330℃; for 8h; | 82% |
1,10-decanediol diacetate
1,10-decadiene
Conditions | Yield |
---|---|
at 350℃; for 8h; | 80% |
at 565℃; | |
at 600℃; |
tetrabromo-1,1,10,10 decane
1,10-decadiene
Conditions | Yield |
---|---|
With n-butyllithium In diethyl ether at -30 - -25℃; | 78% |
n-Decandiyl-dipropionat
1,10-decadiene
Conditions | Yield |
---|---|
at 340℃; for 8h; | 78% |
Conditions | Yield |
---|---|
Stage #1: bromopentene With magnesium Stage #2: (E)-4-(phenylthio)-3-octene With 1,2-bis(diphenylphosphino)ethane nickel(II) chloride In diethyl ether at 20℃; for 15h; | A n/a B 76% |
1,10-decadiene
Conditions | Yield |
---|---|
at 350℃; for 8h; | 70% |
1,10-decadiene
Conditions | Yield |
---|---|
With C55H46N4O4W; N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 3h; Irradiation; | 41% |
1,4-dibromo-butane
allylmagnesium bromide
A
1,10-decadiene
B
7-bromo-hept-1-ene
Conditions | Yield |
---|---|
With lithium chloride; copper dichloride In tetrahydrofuran at 0℃; for 2.5h; | A n/a B 40% |
Conditions | Yield |
---|---|
With dilithium tetrachlorocuprate In tetrahydrofuran at 25℃; for 20h; | 38% |
Conditions | Yield |
---|---|
With C27H29Cl2FN2ORu at 60℃; under 7757.43 Torr; Pressure; Inert atmosphere; Glovebox; | 34% |
With aluminum oxide; tetramethylstannane; rhenium(VII) oxide at 90℃; under 37503 Torr; | |
With C41H46Cl2F9N2PRu In toluene at 35℃; under 7500.75 Torr; for 5h; Catalytic behavior; Reagent/catalyst; Temperature; Autoclave; Glovebox; | 20 %Chromat. |
Conditions | Yield |
---|---|
With C44H59Cl2F2N2PRu In toluene at 35℃; under 7500.75 Torr; for 0.0833333h; Catalytic behavior; Reagent/catalyst; Time; Temperature; Glovebox; | A 15% B 9% |
With C37H52Cl2F3N2PRu In toluene at 35℃; under 7500.75 Torr; for 5h; Catalytic behavior; Reagent/catalyst; Temperature; Autoclave; Glovebox; | A 50 %Chromat. B 11 %Chromat. |
Conditions | Yield |
---|---|
With diethyl ether; magnesium durch Einw. von Allylbromid auf die entstehende Loesung von Tetramethylen-bismagnesiumjodid; |
Conditions | Yield |
---|---|
With ammonium sulfate; ammonia; sodium | |
With copper(II)-citrate; hexamethylenetetramine; hypophosphorous acid In water; N,N-dimethyl-formamide at 130℃; for 24h; Inert atmosphere; Green chemistry; chemoselective reaction; | 88 %Chromat. |
Conditions | Yield |
---|---|
at 565℃; |
2,13-dioxa-tetradecanedioic acid diethyl ester
A
1,10-decadiene
B
1,10-Decanediol
C
9-Decen-1-ol
D
carbonic acid ethyl ester-(10-hydroxy-decyl ester)
Conditions | Yield |
---|---|
at 500℃; Produkt 5-7:Aethanol,Kohlensaeure-aethylester-dec-9-enylester,Aethylen.Pyrolysis; |
3,3'-(butane-1,4-disulfonyl)-bis-propene
1,10-decadiene
Conditions | Yield |
---|---|
at 195 - 260℃; under 150 - 250 Torr; (pyrolysis); |
Conditions | Yield |
---|---|
With sodium methylate In methanol (electrolysis); |
acetoxycyclodecane
A
1,10-decadiene
B
(Z)-cyclodecene
C
trans-cyclodecene
Conditions | Yield |
---|---|
at 500℃; |
1,4-dibromo-butane
allyl bromide
A
1,10-decadiene
B
1,5-Hexadien
C
7-bromo-hept-1-ene
D
tetradeca-1,13-diene
Conditions | Yield |
---|---|
(i) Mg, THF, (ii) /BRN= 605308/; Multistep reaction. Further byproducts given; |
1,4-dibromo-butane
allyl bromide
3-Chloro-2-methylpropene
A
1,10-decadiene
B
2,9-dimethyl-deca-1,9-diene
C
2-methyl-deca-1,9-diene
Conditions | Yield |
---|---|
(i) Mg, THF, (ii) /BRN= 605308/, /BRN= 878160/; Multistep reaction; |
1,10-dibromodecane
A
1,10-decadiene
B
1,10-difluorodecane
C
1-bromo-10-fluorodecane
Conditions | Yield |
---|---|
With tetrabutylammonium hydrogen bifluoride In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide at 95℃; for 3.5h; | A 2 % Chromat. B 76 % Chromat. C 22 % Chromat. |
Conditions | Yield |
---|---|
With hydrogenchloride; oxygen; copper dichloride; palladium dichloride In tetrahydrofuran under 760 Torr; for 19h; Ambient temperature; | 100% |
1,10-decadiene
2,4,4-trimethyl-1-pentyl hypophosphorous acid
{10-(hydroxy-(2,4,4-trimethylpentyl)phosphinoyl)decyl}(2,4,4-trimethylpentyl)phosphinic acid
Conditions | Yield |
---|---|
With di-tert-amyl peroxide at 140℃; for 6h; Inert atmosphere; | 100% |
1,10-decadiene
poly(6-methyl-1,10-undecadiene-co-1,9-decadiene) copolymer, 7.1 methyl groups/1000 total carbons, Mw=35000, Mw/Mn=1.8; Monomer(s): 6-methyl-1,10-undecadiene; 1,9-decadiene
Conditions | Yield |
---|---|
With bis[1,1-di(trifluoromethyl)ethoxy][(2,6-diisopropylphenyl)imino](2-methyl-2-phenylpropylidene)molybdenum | 98% |
1,10-decadiene
poly(6-methyl-1,10-undecadiene-co-1,9-decadiene) copolymer, 1.5 methyl groups/1000 total carbons, Mw=30100, Mw/Mn=1.9; Monomer(s): 6-methyl-1,10-undecadiene; 1,9-decadiene
Conditions | Yield |
---|---|
With bis[1,1-di(trifluoromethyl)ethoxy][(2,6-diisopropylphenyl)imino](2-methyl-2-phenylpropylidene)molybdenum | 98% |
1,10-decadiene
Conditions | Yield |
---|---|
With bis[1,1-di(trifluoromethyl)ethoxy][(2,6-diisopropylphenyl)imino](2-methyl-2-phenylpropylidene)molybdenum | 98% |
1,10-decadiene
methyl vinyl ketone
(3E,11E)-tetradeca-3,11-diene-2,13-dione
Conditions | Yield |
---|---|
With copper(l) iodide; C39H52Cl2N2O3Ru In diethyl ether at 35℃; for 16h; Cross Metathesis; Inert atmosphere; | 98% |
1,10-decadiene
poly(6-methyl-1,10-undecadiene-co-1,9-decadiene) copolymer, 25.0 methyl groups/1000 total carbons, Mw=60200, Mw/Mn=2.4; Monomer(s): 6-methyl-1,10-undecadiene; 1,9-decadiene
Conditions | Yield |
---|---|
With bis[1,1-di(trifluoromethyl)ethoxy][(2,6-diisopropylphenyl)imino](2-methyl-2-phenylpropylidene)molybdenum | 97% |
1,10-decadiene
poly(6-methyl-1,10-undecadiene-co-1,9-decadiene) copolymer, 13.6 methyl groups/1000 total carbons, Mw=57500, Mw/Mn=2.0; Monomer(s): 6-methyl-1,10-undecadiene; 1,9-decadiene
Conditions | Yield |
---|---|
With bis[1,1-di(trifluoromethyl)ethoxy][(2,6-diisopropylphenyl)imino](2-methyl-2-phenylpropylidene)molybdenum | 97% |
Conditions | Yield |
---|---|
With C69H57N2*C8H18OSi2*Pt In toluene at 95℃; for 3.95h; Inert atmosphere; regioselective reaction; | 97% |
Conditions | Yield |
---|---|
With tert-butyl peroxypivalate In acetonitrile at 75℃; for 2h; | 96% |
Conditions | Yield |
---|---|
With cobalt(II) bromide-[1,2-bis(diphenylphosphino)ethane]; zinc(II) iodide; zinc In dichloromethane for 20h; | 96% |
1,10-decadiene
5,5-dimethyl-2-thiolo-2-thiono-1,3,2-dioxaphosphorinane
2,2'-[decane-2,9-diylbis(thio)]bis(5,5-dimethyl-1,3,2-dioxaphosphorinane)2,2'-disulfide
Conditions | Yield |
---|---|
In toluene at 80℃; for 12h; | 96% |
1,10-decadiene
Conditions | Yield |
---|---|
Grubbs catalyst first generation at 20 - 60℃; under 10 Torr; for 24h; Product distribution; Further Variations:; Reagents; ratio of the input monomer; copolymerization; | 95% |
1,10-decadiene
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid; (η6-p-cymene)Ru(P(cyclohexyl)3)(CCC(phenyl)2)Cl triflate In dichloromethane-d2 at 0℃; for 12h; | 94% |
tetrakis(dimethylsiloxy)octaphenylsilsesquioxane
1,10-decadiene
Conditions | Yield |
---|---|
With platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex In toluene at 65℃; for 20h; Schlenk technique; Inert atmosphere; | 93% |
1,10-decadiene
(E)-1-phenyl-N-(1-phenylethylidene)methanamine
Conditions | Yield |
---|---|
Stage #1: 1,10-decadiene; (E)-1-phenyl-N-(1-phenylethylidene)methanamine With molecular sieve; tris(triphenylphosphine)rhodium(I) chloride In toluene at 150℃; for 2h; Stage #2: With water Acid hydrolysis; Stage #3: With hydrogen; palladium on activated charcoal | 92% |
Stage #1: 1,10-decadiene; (E)-1-phenyl-N-(1-phenylethylidene)methanamine; [RhCl(PPh3)3]Cl In toluene at 150℃; for 2h; Stage #2: With hydrogenchloride Stage #3: With hydrogen; palladium on activated charcoal Further stages.; | 92% |
1,10-decadiene
poly(6-methyl-1,10-undecadiene-co-1,9-decadiene) copolymer, 43.3 methyl groups/1000 total carbons, Mw=69400, Mw/Mn=1.8; Monomer(s): 6-methyl-1,10-undecadiene; 1,9-decadiene
Conditions | Yield |
---|---|
With bis[1,1-di(trifluoromethyl)ethoxy][(2,6-diisopropylphenyl)imino](2-methyl-2-phenylpropylidene)molybdenum | 92% |
Conditions | Yield |
---|---|
With 2,2,4-trimethylpentane; tetradecafluorohexane; bromine at 20℃; for 2h; Irradiation; | 92% |
With HBr gas; sodium hydrogencarbonate; dibenzoyl peroxide In diethyl ether; hexane; water | 58 mol % |
Conditions | Yield |
---|---|
Stage #1: 1,10-decadiene With 9-bora-bicyclo[3.3.1]nonane In tetrahydrofuran at 40℃; for 0.0666667h; Stage #2: With dihydrogen peroxide; sodium hydroxide In ethanol; water at 20℃; for 0.0488333h; | 91% |
Stage #1: 1,10-decadiene With sodium tetrahydroborate; iodine; ethylene dibromide In 1,2-dimethoxyethane at 25℃; for 20h; Stage #2: With dihydrogen peroxide; sodium hydroxide In water at 0 - 25℃; for 0.333333h; | 69% |
1,10-decadiene
rac/meso-1,2,9,10-diepoxydecane
Conditions | Yield |
---|---|
With peracetic acid; manganese(II) perchlorate; ammonium bicarbonate In water; acetic acid; acetonitrile at 20℃; for 0.666667h; | 90% |
With peracetic acid; C8H18N(1+)*MnO4(1-); sodium hydrogencarbonate In water at 20℃; for 0.5h; | 82% |
With Perbenzoic acid; chloroform | |
With peracetic acid; 1-methyl-1-propylpyrrolidinium dodecyl sulfate; manganese(II) acetate; sodium hydrogencarbonate In water; acetic acid at 20℃; for 0.5h; | 88 %Chromat. |
1,10-decadiene
poly(6-methyl-1,10-undecadiene-co-1,9-decadiene) copolymer, 55.6 methyl groups/1000 total carbons, Mw=26100, Mw/Mn=1.7; Monomer(s): 6-methyl-1,10-undecadiene; 1,9-decadiene
Conditions | Yield |
---|---|
With bis[1,1-di(trifluoromethyl)ethoxy][(2,6-diisopropylphenyl)imino](2-methyl-2-phenylpropylidene)molybdenum | 90% |
2,2-dimethyl-3-butyne
1,10-decadiene
1,4-di-tert-butyl-5-(7-octenyl)-1,3-cyclohexadiene
Conditions | Yield |
---|---|
With tris-(trimethylsilyl)silane; niobium pentachloride In 1,2-dichloro-ethane at 40℃; for 3h; Inert atmosphere; chemoselective reaction; | 90% |
With NbCl3(DME) In 1,2-dichloro-ethane at 40℃; for 2h; Inert atmosphere; regioselective reaction; | 81% |
Conditions | Yield |
---|---|
With MeOH In dichloromethane N2-atmosphere; addn. of H2BrB*SMe2 to olefin, then MeOH addn. (pptn.); | 88% |
1,10-decadiene
2-(oct-7-en-1-yl)oxirane
Conditions | Yield |
---|---|
With oxygen In acetonitrile at 60℃; under 760.051 Torr; for 1.5h; Catalytic behavior; chemoselective reaction; | 85% |
With p-chloroperbenzoic acid In dichloromethane | |
With oxygen In acetonitrile under 760.051 Torr; for 1h; Kinetics; | 90 %Chromat. |
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