DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
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Product Name: ACENAPHTHYLENE Synonyms: cyclopenta(de)naphthalene;Cyclopenta[de]naphthalene;ACENAPHTHYLENE, 99+%;ACENAPHTHYLENE, 100MG, NEAT;ACENAPHTHYLENE, 1X1ML, MEOH, 5000UG/ML;ACENAPHTHYLENE 80+%;ACENAPHTHYLENE 95%;Acenaphthylene, t
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inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
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inquiry1. Product advantages High purity, all above 98.5%, no impurities after dissolution We will test each batch to ensure quality OEM and private brand services designed for free Various cap colors available We can also provide MT1 peptide powd
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inquiryItem Standard Structural data confirmation 1. H-NMR: The data of structure are identical with reference standard 2. HPLC/GC-MS: Ensure the molecul
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Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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Cas:208-96-8
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inquiryProduct name: Acenaphthylene CAS No.: 208-96-8 Molecule Formula:C12H8 Molecule Weight:152.19 Purity: 99.0% Package: 25kg/drum Description:White or yellowish crystalline powder Manufacture Standards:Enterprise Standard TESTING ITE
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inquiryWe product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Product Name:ACENAPHTHYLENE CAS No:208-96-8 Synonym
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ACENAPHTHYLENE Basic information Product Name: ACENAPHTHYLENE Synonyms: cyclopenta(de)naphthalene;Cyclopenta[de]naphthalene;acenaphthylene anion radical;1,2-dihydroacenaphthylene-1,2-diide;ACENAPHTHALENE;ACENAPHTHYLENE;acenaphthylene,industria
factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:208-96-8
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inquiryHangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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inquiryWe are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as:
Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Enterprise standard Package:100g:1kg;10kg;100kg;200kg Application:Pharma Intermediate
1-bromo-1H,3H-naphtho<1,8-cd>thiopyran 2,2-dioxide
acenaphthylene
Conditions | Yield |
---|---|
With sodium methylate In methanol for 16.5h; Ambient temperature; | 97% |
With sodium methylate In methanol for 16.5h; Product distribution; Ambient temperature; var. of base; | 97% |
acenaphthene
7,7',8,8'-tetracyanoquinodimethane
A
9-Acenaphthyl<4-(dicyanomethyl)phenyl>dicyanomethane
B
acenaphthylene
Conditions | Yield |
---|---|
for 0.0833333h; Heating; | A 95.5% B n/a |
Carbonic acid acenaphthen-1-yl ester methyl ester
acenaphthylene
Conditions | Yield |
---|---|
With 1,2-bis-(diphenylphosphino)ethane; bis(dibenzylideneacetone)-palladium(0) In N,N-dimethyl-formamide at 60℃; for 48h; | 95% |
Propynoic acid acenaphthen-1-yl ester
acenaphthylene
Conditions | Yield |
---|---|
at 760℃; under 0.03 Torr; | 95% |
Multi-step reaction with 2 steps 1: 32 percent / deuterium oxide, triethylamine / tetrahydrofuran / 1.25 h / 35 °C 2: 95 percent / 760 °C / 0.03 Torr View Scheme |
acenaphthylene
Conditions | Yield |
---|---|
at 760℃; under 0.03 Torr; | 95% |
trans-1,2-dibromo-1,2-dihydroacenaphthylene
acenaphthylene
Conditions | Yield |
---|---|
With acetic acid; zinc | 94% |
With ethanol; zinc |
1,2-dibromoacenaphthene
acenaphthylene
Conditions | Yield |
---|---|
With sodium sulfide; Aliquat 336 In water; benzene for 1h; Ambient temperature; | 92% |
Conditions | Yield |
---|---|
methyltrioxorhenium(VII) In benzene for 72h; | 89% |
zirconium(IV) chloride In acetonitrile at 20℃; for 0.666667h; | 89% |
With pyridine; thionyl chloride |
Conditions | Yield |
---|---|
at 500℃; under 0.02 Torr; for 0.0833333h; | A 88% B 4% |
Conditions | Yield |
---|---|
at 800℃; under 0.1 Torr; Cyclization; Pyrolysis; | A 81% B 2% |
Conditions | Yield |
---|---|
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In toluene for 24h; Reflux; | 80% |
With oxygen; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium nitrite In toluene at 120℃; under 9750.98 Torr; for 8h; | 77% |
With manganese(IV) oxide In benzene for 30h; Heating; | 41% |
Conditions | Yield |
---|---|
With Lawessons reagent In toluene for 0.5h; Heating; | A 72% B 13% |
With Lawessons reagent In toluene for 0.5h; Heating; | A 72% B 13% |
acenaphthene
chloranil
A
2,3,5,6-tetrachlorobenzene-1,4-diol
B
acenaphthylene
Conditions | Yield |
---|---|
In benzene for 18h; Irradiation; | A 68% B 19% |
Conditions | Yield |
---|---|
With N,N,N,N,-tetramethylethylenediamine; iodine In tetrahydrofuran Kinetics; to a soln. of nucleophile in THF was added soln. of complex in THF at -60°C; after 45 min at -60°C I2 in THF was added and soln. allowed to stir overnight while being warmed to room temp.;; soln. was filtered through Celite, evapd., extd. with ether, extract was washed with other solvents, then chromd. on silica column, eluent CHCl3-hexane;; | A 19% B 20% C 68% |
acenaphthylene
Conditions | Yield |
---|---|
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In toluene for 24h; Schlenk technique; Inert atmosphere; Reflux; | 57% |
Conditions | Yield |
---|---|
With N,N,N,N,-tetramethylethylenediamine; iodine; trifluoroacetic acid In tetrahydrofuran to a soln. of nucleophile in THF at -60°C soln. of complex was added, after 45 min at -60°C CF3COOH was added followed by I2, and soln. was allowed to stir overnight while being warmed to room temp.;; soln. was filtered through Celite, evapd.; residue was extd. was ether and washed with other solvents; then chromd. on silica column, eluent CH2Cl2-hexane;; | A 47% B 8% |
Conditions | Yield |
---|---|
at 780℃; under 1 Torr; for 0.0833333h; | A 43% B 19% C 37% |
dichloromethane
(naphthalene-1,8-diyl)dilithium
A
naphthalene
B
1,1'-cis-ethene-1,2-diyl-bis-naphthalene
C
(E)-1,2-bis(1-naphthyl)ethene
D
1H-Cyclobutanaphthalene
E
1-Chloromethylnaphthalene
F
acenaphthylene
Conditions | Yield |
---|---|
With N,N,N,N,-tetramethylethylenediamine In diethyl ether at -100 - -60℃; Product distribution; Mechanism; var. of temp., further with CD2Cl2; | A 42% B n/a C n/a D 21% E n/a F n/a |
dichloromethane
(naphthalene-1,8-diyl)dilithium
A
naphthalene
B
1,1'-cis-ethene-1,2-diyl-bis-naphthalene
C
1H-Cyclobutanaphthalene
D
acenaphthylene
Conditions | Yield |
---|---|
With N,N,N,N,-tetramethylethylenediamine In diethyl ether at -100 - -60℃; Further byproducts given; | A 42% B n/a C 21% D n/a |
(acenaphthylene)chromium tricarbonyl
A
C40H44N2O2
B
C20H23NO
C
acenaphthylene
Conditions | Yield |
---|---|
With N,N,N,N,-tetramethylethylenediamine; iodine In tetrahydrofuran to a soln. of nucleophile in THF at -60°C soln. of complex was added, after 45 min at -60°C soln. of I2 in THF was added, and soln. was allowed to stir overnight while being warmed to room temp.;; soln. was filtered through Celite, evapd.; residue was extd. was ether and washed with other solvents; then chromd. on silica column, eluent CH2Cl2-hexane;; | A 16% B 42% C 41% |
2-(2-ethynyl-phenyl)-thiophene
A
naphtho[1,2-b]thiophene
B
acenaphthylene
Conditions | Yield |
---|---|
at 1000℃; under 0.1 Torr; Cyclization; rearrangement; Pyrolysis; | A 18% B 41% |
acenaphthene quinone
A
1-acenaphthenol
B
acenaphthene
C
acenaphthylene
Conditions | Yield |
---|---|
With samarium diiodide; water In tetrahydrofuran at 20℃; for 0.00277778h; | A 41% B 26% C 23% |
A
acenaphthene
B
9-Hydroxymethyl-1H-naphtho[1,2-c]furan-3-one
C
acenaphthylene
Conditions | Yield |
---|---|
at 730℃; under 0.03 Torr; for 0.05h; | A 9% B 38% C 12% |
1,3-dibromo-1H,3H-naphtho<1,8-cd>thiopyran 2,2-dioxide
A
decacyclene
B
1-bromoacenaphthylene
C
acenaphthylene
Conditions | Yield |
---|---|
With potassium tert-butylate In tert-butyl alcohol at 27℃; for 18h; Product distribution; other reagents; | A 5% B 33% C 23% |
With potassium tert-butylate In tert-butyl alcohol for 1.5h; Heating; | A 5% B n/a C n/a |
acenaphthene quinone
A
decacyclene
B
1-acenaphthenol
C
acenaphthene
D
acenaphthylene
Conditions | Yield |
---|---|
bis(η6-biphenyl)titanium(0) In toluene at 110℃; for 2h; Further byproducts given; | A 21% B 10% C 11% D 31% |
acenaphthene quinone
A
decacyclene
B
trans-biacenaphthylidene
C
cis-biacenaphthylidene
D
acenaphthylene
Conditions | Yield |
---|---|
bis(η6-biphenyl)titanium(0) In toluene at 110℃; for 2h; Yield given. Further byproducts given; | A 21% B n/a C n/a D 31% |
1,2-dihydroacenaphthylen-1-yl diazoacetate
acenaphthylene
Conditions | Yield |
---|---|
at 340℃; under 0.02 Torr; | 22% |
acenaphthylene
Conditions | Yield |
---|---|
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In toluene for 24h; Schlenk technique; Inert atmosphere; Reflux; | 21% |
(acenaphthylene)chromium tricarbonyl
lithium isobutyronitrile
A
C16H13N
B
acenaphthylene
Conditions | Yield |
---|---|
With N,N,N,N,-tetramethylethylenediamine; iodine; trifluoroacetic acid In tetrahydrofuran to a soln. of nucleophile in THF at -60°C soln. of complex was added, after 45 min at -60°C CF3COOH was added followed by I2, and soln. was allowed to stir overnight while being warmed to room temp.;; soln. was filtered through Celite, evapd.; residue was extd. was ether and washed with other solvents; then chromd. on silica column, eluent CH2Cl2-hexane;; | A 20% B 3% |
Conditions | Yield |
---|---|
With tetraethylammonium bromide In ethanol at 60℃; electrolysis, lead cathode; | 100% |
With benzenetellurol In ethanol; ethyl acetate for 4h; Product distribution; Heating; other reagent, reaction time; | 98% |
With iodine; hypophosphorous acid In acetic acid for 24h; Heating; | 98% |
Conditions | Yield |
---|---|
In acetic acid | 100% |
acenaphthylene
acenaphthylene
Conditions | Yield |
---|---|
With 6-per-deoxy-6-per-(2-sulfoethyl)thio-γ-cyclodextrin, sodium salt for 12h; UV-irradiation; stereoselective reaction; | 100% |
With Rosebengal In methanol Irradiation; | 65% |
In hexane at 25℃; Irradiation; | |
With racemic palladium-ruthenium heterometallic cage with 3-{1H-imidazo[4,5-f]1,10-phenanthrolin-2-yl}pyridine In water; dimethyl sulfoxide at 20℃; Kinetics; Catalytic behavior; Reagent/catalyst; Solvent; Irradiation; |
acenaphthylene
7,8,9,10-Tetrachloro-6b,10a-dihydro-fluoranthene
Conditions | Yield |
---|---|
at 20℃; for 1h; | 100% |
acenaphthylene
trans-1,2-dibromo-1,2-dihydroacenaphthylene
Conditions | Yield |
---|---|
With tri(decyl)(methyl)phosphonium tribromide In Hexadecane for 240h; | 100% |
With hydrogen bromide; oxygen; sodium nitrite In water; acetonitrile at 22℃; for 8h; diastereoselective reaction; | 96% |
With pyridinium hydrobromide perbromide In tetrahydrofuran at -78 - 20℃; | 93% |
Conditions | Yield |
---|---|
Stage #1: methanol; 4-allylguaiacol With [bis(acetoxy)iodo]benzene; sodium hydrogencarbonate In benzene at 0℃; for 0.166667h; Stage #2: acenaphthylene In benzene at 20℃; for 22h; Diels-Alder reaction; stereoselective reaction; | 100% |
1,3-diphenyl-2H-cyclopenta<1>phenanthren-2-one
acenaphthylene
C40H26
Conditions | Yield |
---|---|
In xylene Reflux; | 100% |
Conditions | Yield |
---|---|
In diethyl ether; dichloromethane; o-xylene at 100 - 140℃; for 2h; | 100% |
acenaphthylene
6b,7a-dihydroacenaphtho [1,2-b]oxirene
Conditions | Yield |
---|---|
Stage #1: acenaphthylene With N-Bromosuccinimide In water; dimethyl sulfoxide at 20℃; for 2h; Stage #2: With sodium hydroxide In diethyl ether at 20℃; | 99% |
With 3,3-dimethyldioxirane In acetone at 20℃; for 1h; | 97% |
With 2-Nitrobenzenesulfonyl chloride In acetonitrile at -30℃; for 10h; Product distribution; various arenes, solvents + times; | 95% |
Conditions | Yield |
---|---|
With 5,5’-bis(diphenylphosphino)-2,2,2’,2’-tetrafluoro-4,4’-bi-1,3-benzodioxole; [Rh(OH)(cod)]2 In 1,4-dioxane at 60℃; for 6h; Catalytic behavior; Reagent/catalyst; Inert atmosphere; Schlenk technique; enantioselective reaction; | 99% |
Conditions | Yield |
---|---|
With oxygen; isobutyraldehyde In acetonitrile at 60℃; for 3h; | 98% |
With dinitrogen monoxide; dioxo(tetramesitylporphyrinato)ruthenium(VI) In fluorobenzene at 100℃; under 7500.6 Torr; | 87% |
With iodosylbenzene; iron(III) tetraphenylporphyrin In dichloromethane for 1h; | 58% |
With iodosylbenzene; μ-oxo dimer of iron(III)porphyrinate In methanol at 21.9℃; for 3h; Product distribution; Mechanism; catalysts also Fe(III)porphyrinate, Fe(III)tetraphenylporphyrinate; protic and aprotic solvents; inhibition effect by phenanthrene; by-products; | 28% |
With dinitrogen monoxide at 300℃; under 367754 Torr; |
Conditions | Yield |
---|---|
In diethyl ether at 0℃; | 98% |
N-ethoxycarbonyl-(2,3,4,5-tetrachloro-1-thiophenio)amide
acenaphthylene
(6bS,10aR)-7,8,9,10-Tetrachloro-6b,10a-dihydro-fluoranthene
Conditions | Yield |
---|---|
at 20℃; for 0.166667h; | 98% |
Conditions | Yield |
---|---|
With 5,5’-bis(diphenylphosphino)-2,2,2’,2’-tetrafluoro-4,4’-bi-1,3-benzodioxole; [Rh(OH)(cod)]2 In 1,4-dioxane at 60℃; for 6h; Inert atmosphere; Schlenk technique; enantioselective reaction; | 98% |
Conditions | Yield |
---|---|
In acetic acid | 97% |
Conditions | Yield |
---|---|
With 5,5’-bis(diphenylphosphino)-2,2,2’,2’-tetrafluoro-4,4’-bi-1,3-benzodioxole; tert-Amyl alcohol; [Rh(OH)(cod)]2 In 1,4-dioxane at 60℃; for 6h; Inert atmosphere; Schlenk technique; enantioselective reaction; | 97% |
N-(ethoxycarbonyl)-(2,3,4,5-tetrachloro-1-thiophenio)amide S-oxide
acenaphthylene
A
sulfinylcarbamic acid ethyl ester
B
(6bS,10aR)-7,8,9,10-Tetrachloro-6b,10a-dihydro-fluoranthene
Conditions | Yield |
---|---|
In dichloromethane for 1h; | A 89% B 96% |
Conditions | Yield |
---|---|
In acetic acid | 96% |
acenaphthylene
Conditions | Yield |
---|---|
With pyridine In chloroform at 70℃; for 24h; | 96% |
Conditions | Yield |
---|---|
With Br2Co*C27H26P2; zinc(II) iodide; zinc In dichloromethane at 25℃; for 48h; | 95% |
bis(pinacol)diborane
acenaphthylene
2-(1,2-dihydroacenaphthylen-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
Conditions | Yield |
---|---|
With methanol; (2-mesityl-5-methyl-2,3-dihydroimidazo[1,5-a]pyridin-3-yl)copper(I) chloride; sodium t-butanolate In diethyl ether at 20℃; for 0.5h; Inert atmosphere; Schlenk technique; | 95% |
1,3-diphenylisobenzofuran
acenaphthylene
10.13-Diphenyl-10.13-endoxy-11:12-benzo-9.10.13.14-tetrahydrofluoranthen
Conditions | Yield |
---|---|
In 5,5-dimethyl-1,3-cyclohexadiene Reflux; | 94.85% |
In benzonitrile at 140℃; for 7h; | 60% |
Conditions | Yield |
---|---|
With Raney Ni-Al In potassium hydroxide; water at 90℃; for 6.5h; Reduction; | 94% |
With hydrogen; nickel at 250℃; |
Conditions | Yield |
---|---|
With benzeneseleninic anhydride In chlorobenzene at 120℃; for 2h; | 94% |
With N-Bromosuccinimide; water; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In dimethyl sulfoxide at 60 - 70℃; for 3h; | 79% |
With sodium dichromate; cerous nitrate In acetic acid for 19h; Ambient temperature; | 36% |
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