As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:2094-74-8
Min.Order:1 Kilogram
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Min.Order:1 Kilogram
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Min.Order:1 Kilogram
FOB Price: $9.0 / 99.0
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:2094-74-8
Min.Order:4 Kilogram
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryProduct name: 1-Adamantylcarboxaldehyde CAS No.:2094-74-8 Molecule Formula:C11H16O Molecule Weight:164.24 Purity: 95.0% Package: 25kg/drum Description:White or off-white powder Manufacture Standards:Enterprise Standard TESTING IT
Cas:2094-74-8
Min.Order:1 Kilogram
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Cas:2094-74-8
Min.Order:1 Kilogram
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Cas:2094-74-8
Min.Order:1 Gram
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:2094-74-8
Min.Order:1 Metric Ton
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inquirySuperior quality, moderate price & quick delivery. Appearance:white crystalline powder Storage:stored in a cool, dry and ventilated place to provent sun and rain Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical
Cas:2094-74-8
Min.Order:1 Kilogram
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Type:Trading Company
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Cas:2094-74-8
Min.Order:1 Metric Ton
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
Cas:2094-74-8
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
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Cas:2094-74-8
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inquiryHunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
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Cas:2094-74-8
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inquiryAmoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi
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1-ADAMANTANE CARBOXALDEHYDEAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:pharmaceutical intermediate Transportation:by air, by sea, by express
Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
home-produced Application:medicine
Cas:2094-74-8
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inquiryConditions | Yield |
---|---|
With pyridinium chlorochromate In dichloromethane for 1.75h; Ambient temperature; | 100% |
With oxalyl dichloride; dimethyl sulfoxide; triethylamine In dichloromethane at -78℃; for 1h; Swern oxidation; | 98% |
Stage #1: 1-adamantanemethanol With oxalyl dichloride; dimethyl sulfoxide In dichloromethane at -78℃; for 1h; Inert atmosphere; Stage #2: With triethylamine In dichloromethane at -78℃; for 0.5h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With thexylchloroborane-Me2SO4 In dichloromethane for 0.25h; Ambient temperature; | 99% |
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃; for 2h; | 64% |
Stage #1: 1-Adamantanecarboxylic acid With lithium aluminium tetrahydride Stage #2: Swern Oxidation; | 62% |
Conditions | Yield |
---|---|
In dichloromethane for 1h; | 98% |
1-adamantanecarbonitrile
1-Adamantanecarbaldehyde
Conditions | Yield |
---|---|
Stage #1: 1-adamantanecarbonitrile With hydrogenchloride; tin(ll) chloride In diethyl ether at 0 - 25℃; for 22h; Stephen reduction; Stage #2: With water In diethyl ether at 20 - 60℃; | 95% |
With sodium hydride; zinc(II) chloride In tetrahydrofuran; mineral oil at 40℃; for 1h; Inert atmosphere; Sealed tube; | 77% |
Multi-step reaction with 2 steps 1: CH2Cl2 / 120 h / Heating 2: 1) Et3SiH, 2) H2O / 1) CH2Cl2, 1 h room temperature; 4 h reflux, 2) heating View Scheme |
Conditions | Yield |
---|---|
With sodium hydride; sodium iodide In tetrahydrofuran at 40℃; chemoselective reaction; | 87% |
α-Azido-1-adamantylmethyl phenyl sulfide
A
1-Adamantanecarbaldehyde
B
diphenyldisulfane
Conditions | Yield |
---|---|
In chlorobenzene at 120℃; for 8h; | A 82% B 80.5 mg |
1,1,1,3',3',3'-hexafluoro-propanol
1-adamantanemethanol
1-Adamantanecarbaldehyde
Conditions | Yield |
---|---|
Stage #1: 1-adamantanemethanol With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trichloroisocyanuric acid In dichloromethane at 0℃; Stage #2: 1,1,1,3',3',3'-hexafluoro-propanol With pyridine In dichloromethane at 0 - 20℃; for 24h; | 81% |
carbon monoxide
adamantane
A
1-adamanthanol
B
1-Adamantanecarboxylic acid
C
1-Adamantanecarbaldehyde
Conditions | Yield |
---|---|
trifluorormethanesulfonic acid In various solvent(s) under 62057.8 Torr; for 10h; Ambient temperature; | A 6% B 75% C n/a |
trifluorormethanesulfonic acid In various solvent(s) under 62057.8 Torr; for 10h; Product distribution; Ambient temperature; variation of superacid catalyst systems, in absence of solvent; | A n/a B n/a C 0.2% |
1-Adamantyl bromide
N,N-dimethyl-formamide
1-Adamantanecarbaldehyde
Conditions | Yield |
---|---|
With lithium sodium In tetrahydrofuran at 20℃; for 0.0833333h; Substitution; Bouveault reaction; ultrasonic irradiation; | 75% |
With sodium; lithium In tetrahydrofuran at 20℃; for 0.0833333h; Bouveault reaction; | 75% |
With lithium In diethyl ether for 5h; | 36% |
Conditions | Yield |
---|---|
With aluminum tri-bromide; carbon tetrabromide; methyl-cyclopentane In various solvent(s) at 20℃; for 1h; | A 72% B n/a |
N-cyclohexyl-1-adamantanecarboxamide
1-Adamantanecarbaldehyde
Conditions | Yield |
---|---|
Stage #1: N-cyclohexyladamantane-1-carboxamide With 2-fluoropyridine; trifluoromethylsulfonic anhydride In dichloromethane at -78 - 0℃; Inert atmosphere; Stage #2: With triethylsilane In dichloromethane at 0 - 25℃; Inert atmosphere; Stage #3: With citric acid In tetrahydrofuran; dichloromethane; water at 45℃; for 2h; chemoselective reaction; | 70% |
1-Adamantanecarboxylic acid
A
1-adamantanemethanol
B
1-Adamantanecarbaldehyde
Conditions | Yield |
---|---|
With lithium; ethylamine at 17℃; for 6h; | A 9% B 51% |
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride In benzene at 100℃; under 60800 Torr; for 3h; | 46% |
With 2,2'-azobis-(2,4-dimethylvaleronitrile); tri-n-butyl-tin hydride In decane; toluene at 80℃; under 64604.3 Torr; for 0.2h; Continuous microflow reactor; | 86 %Chromat. |
1-adamantanemethanol
A
1-Adamantanecarbaldehyde
B
(1-adamantanyl)methyl 1-adamantanecarboxylate
Conditions | Yield |
---|---|
With iodine; potassium carbonate In tert-butyl alcohol at 20℃; for 26h; | A 41% B 32% |
1,3-dibromobenzene
adamantylmethylamine
A
1-Adamantanecarbaldehyde
C
N-(1-adamantylmethyl)-3-bromoaniline
D
N,N'-bis(1-adamantylmethyl)benzene-1,3-diamine
Conditions | Yield |
---|---|
With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate In 1,4-dioxane for 7h; Inert atmosphere; Reflux; | A 12% B 7% C 39% D 4% |
1-adamantanecarbonitrile
A
1-Adamantanecarbaldehyde
B
adamantylmethylamine
Conditions | Yield |
---|---|
With sodium hydride; sodium iodide In tetrahydrofuran; mineral oil at 85℃; for 20h; Inert atmosphere; | A 29% B 7% |
A
S-Phenyl benzenethiosulfonate
B
1-Adamantanecarbaldehyde
C
1-adamantanecarbonitrile
D
diphenyldisulfane
Conditions | Yield |
---|---|
In chlorobenzene at 120℃; for 1h; | A 45 mg B 4.1% C 28.5% D 20 mg |
Conditions | Yield |
---|---|
With aluminium trichloride In dichloromethane for 10h; Ambient temperature; | 21% |
With gallium(III) trichloride In 1,2-dichloro-ethane at 20℃; under 760 Torr; for 0.666667h; Product distribution; Further Variations:; Pressures; Temperatures; Solvents; Reagents; | 84 % Chromat. |
1-adamantanemethanol
A
1-Adamantanecarboxylic acid
B
1-Adamantanecarbaldehyde
Conditions | Yield |
---|---|
With silica gel; 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium perchlorate In dichloromethane | A 5% B n/a |
Adamantan-1-carbonsaeure-N2-p-tosylhydrazid
1-Adamantanecarbaldehyde
Conditions | Yield |
---|---|
With sodium carbonate at 160 - 165℃; |
Conditions | Yield |
---|---|
With dimethylsulfide borane complex; pyridinium chlorochromate 1) THF, reflux, 1 h, 2.) CH2Cl2, reflux, 1 h; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
trifluorormethanesulfonic acid; antimony pentafluoride In various solvent(s) for 6h; Ambient temperature; |
Conditions | Yield |
---|---|
With triethylsilane; water 1) CH2Cl2, 1 h room temperature; 4 h reflux, 2) heating; Yield given. Multistep reaction; | A 4 % Spectr. B n/a |
Conditions | Yield |
---|---|
In various solvent(s) at 170 - 220℃; Thermodynamic data; Quantum yield; activation energy at unimolecular thermolysis, solvent effects, effect of oxygen; |
Conditions | Yield |
---|---|
With sodium bis(2-methoxyethoxy)aluminium dihydride | |
Multi-step reaction with 2 steps 1: 96 percent / LiAlH4 / tetrahydrofuran / 1.5 h / 0 - 20 °C 2: 98 percent / oxalyl chloride; DMSO; Et3N / CH2Cl2 / 1 h / -78 °C View Scheme | |
Multi-step reaction with 2 steps 1: lithium aluminium tetrahydride / tetrahydrofuran / 1.25 h / 0 - 20 °C 2: pyridinium chlorochromate / dichloromethane / 1 h / 20 °C View Scheme |
3-adamantan-1-yl-1-tert-butyl-aziridin-2-one
1-Adamantanecarbaldehyde
Conditions | Yield |
---|---|
With methanesulfonic acid |
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