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inquiry1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethanone CAS:25892-95-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, speci
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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inquiry1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethanoneAppearance:detailed see specifications Storage:Keep away of light, cool place Package:25kg/drum;200kg/drum Application:It is an important raw material and intermediate used in Organic Synthesis,
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inquiry1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethanone cas 25892-95-9Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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inquirybest seller Application:API
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inquiry1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
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inquiryZhengzhou Kingorgchem Chemical Technology Co., Ltd. was founded on the basis of Organophosphorus Chemistry Lab of Institute of Chemistry Henan Academy of Sciences in 2015. The laboratory covers 600 m2 and the pilot plant covers 2000 m2. Kingorgchem i
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inquiryBetterbiochem is specialized in APIs, pharmaceutical intermediates & fine chemicals. 1. The best quality, competitive price. 2. The best service before or after shipment. 3. Rich experience in export operation. 4. Rich experience in
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inquiryhigh purity,good quality,fast delivery,good service Storage:under dry storage and room temperature Package:fluorinated bottle Application:intermediate Transportation:by fedex
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inquiryAt Capot,We can synthesize and purify your complex molecules from 100 gram to 10 tons.Appearance:Clear colorless to light yellow liquid Storage:Dry,Seal and Cool place Package:1G,5G,10G,25G,100G,250G,500G,1KG,5KG,10KG,25KG,50KG,100KG,150KG,200KG. App
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inquiry1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethanone Application:1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethanone
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inquiry1-(4-(benzyloxy)-3,6-dihydroxy-2-methoxyphenyl)ethan-1-one
dimethyl sulfate
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 60℃; for 5h; | 85% |
With potassium carbonate In acetone Heating; | 59% |
In acetone for 5h; Reflux; |
2-hydroxy-4,6-dimethoxyacetophenone
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 60 percent / aluminium chloride / chlorobenzene / 1 h / Heating 2: 99 percent / K2CO3 / acetone / Heating 3: 29 percent / NaOH; K2S2O8; pyridine / H2O / 24 h / 20 °C 4: 59 percent / K2CO3 / acetone / Heating View Scheme |
2,4,6-trihydroxyacetophenone
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 92 percent / K2CO3 / acetone / 3 h / 65 °C 2: 60 percent / aluminium chloride / chlorobenzene / 1 h / Heating 3: 99 percent / K2CO3 / acetone / Heating 4: 29 percent / NaOH; K2S2O8; pyridine / H2O / 24 h / 20 °C 5: 59 percent / K2CO3 / acetone / Heating View Scheme |
4,6-dihydroxy-2-methoxyacetophenone
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 99 percent / K2CO3 / acetone / Heating 2: 29 percent / NaOH; K2S2O8; pyridine / H2O / 24 h / 20 °C 3: 59 percent / K2CO3 / acetone / Heating View Scheme |
1-(4-(benzyloxy)-2-hydroxy-6-methoxyphenyl)ethan-1-one
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 29 percent / NaOH; K2S2O8; pyridine / H2O / 24 h / 20 °C 2: 59 percent / K2CO3 / acetone / Heating View Scheme | |
Multi-step reaction with 2 steps 1: pyridine; dipotassium peroxodisulfate; tetraethylammonium hydroxide / water / 24 h / 20 °C 2: acetone / 5 h / Reflux View Scheme | |
Multi-step reaction with 2 steps 1.1: pyridine; tetraethylammonium hydroxide / water / 20 °C 1.2: 24 h / 20 °C 1.3: 1 h / 95 °C 2.1: potassium carbonate / acetone / 5 h / 60 °C View Scheme |
1-(4-(benzyloxy)-3,6-dihydroxy-2-methoxyphenyl)ethan-1-one
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
In acetone |
benzyl bromide
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: potassium carbonate / acetone / 60 °C 3: potassium hydroxide; pyridine / diethylene glycol; water / 100 °C 4: pyridine; dipotassium peroxodisulfate; tetraethylammonium hydroxide / water / 24 h / 20 °C 5: acetone / 5 h / Reflux View Scheme | |
Multi-step reaction with 5 steps 1.1: potassium carbonate / acetone / 5 h / 0 - 60 °C 2.1: potassium hydroxide / acetone / 5 h / 60 °C 3.1: sodium hydroxide; pyridine / water; diethylene glycol / 2 h / 100 °C 4.1: pyridine; tetraethylammonium hydroxide / water / 20 °C 4.2: 24 h / 20 °C 4.3: 1 h / 95 °C 5.1: potassium carbonate / acetone / 5 h / 60 °C View Scheme |
5,7-dihydroxy-2-phenyl-chromen-4-one
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: potassium carbonate / acetone / 60 °C 3: potassium hydroxide; pyridine / diethylene glycol; water / 100 °C 4: pyridine; dipotassium peroxodisulfate; tetraethylammonium hydroxide / water / 24 h / 20 °C 5: acetone / 5 h / Reflux View Scheme | |
Multi-step reaction with 5 steps 1.1: potassium carbonate / acetone / 5 h / 0 - 60 °C 2.1: potassium hydroxide / acetone / 5 h / 60 °C 3.1: sodium hydroxide; pyridine / water; diethylene glycol / 2 h / 100 °C 4.1: pyridine; tetraethylammonium hydroxide / water / 20 °C 4.2: 24 h / 20 °C 4.3: 1 h / 95 °C 5.1: potassium carbonate / acetone / 5 h / 60 °C View Scheme |
7-(benzyloxy)-5-hydroxy-2-phenyl-4H-chromen-4-one
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 2: potassium hydroxide; pyridine / diethylene glycol; water / 100 °C 3: pyridine; dipotassium peroxodisulfate; tetraethylammonium hydroxide / water / 24 h / 20 °C 4: acetone / 5 h / Reflux View Scheme | |
Multi-step reaction with 4 steps 1.1: potassium hydroxide / acetone / 5 h / 60 °C 2.1: sodium hydroxide; pyridine / water; diethylene glycol / 2 h / 100 °C 3.1: pyridine; tetraethylammonium hydroxide / water / 20 °C 3.2: 24 h / 20 °C 3.3: 1 h / 95 °C 4.1: potassium carbonate / acetone / 5 h / 60 °C View Scheme |
1-(4-(benzyloxy)-2-hydroxy-6-methoxyphenyl)ethanone
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: potassium hydroxide; pyridine / diethylene glycol; water / 100 °C 2: pyridine; dipotassium peroxodisulfate; tetraethylammonium hydroxide / water / 24 h / 20 °C 3: acetone / 5 h / Reflux View Scheme | |
Multi-step reaction with 3 steps 1.1: sodium hydroxide; pyridine / water; diethylene glycol / 2 h / 100 °C 2.1: pyridine; tetraethylammonium hydroxide / water / 20 °C 2.2: 24 h / 20 °C 2.3: 1 h / 95 °C 3.1: potassium carbonate / acetone / 5 h / 60 °C View Scheme |
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
N,N-dimethyl-formamide dimethyl acetal
7-(benzyloxy)-5,6-dimethoxy-4H-chromen-4-one
Conditions | Yield |
---|---|
Stage #1: 1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one; N,N-dimethyl-formamide dimethyl acetal In toluene at 80℃; for 18h; Stage #2: With hydrogenchloride In toluene at 0 - 50℃; for 1h; | 97% |
In toluene at 80℃; for 18h; | 97% |
Stage #1: 1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one; N,N-dimethyl-formamide dimethyl acetal In 1,2-dimethoxyethane at 80℃; for 20h; Stage #2: With hydrogenchloride In water at 0 - 50℃; for 1h; | 95% |
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
With pyridine at 20℃; for 3h; | 81% |
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
3,4-dimethoxy-benzaldehyde
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol; water | 75% |
isovanillin
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol at 20℃; for 48h; | 53% |
With potassium hydroxide In ethanol at 20℃; for 48h; Aldol Condensation; | 53% |
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
4-benzyloxy-3,5-dimethoxybenzoic acid chloride
2,3-dimethoxy-4-benzyloxy-6-(3,5-dimethoxy-4-benzyloxy)-benzyloxyacetophenone
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 2h; Heating; | 52% |
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
3,4-dimethoxy-benzaldehyde
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol; water at 20℃; for 24h; | 39% |
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
3,4-dibenzyloxybenzoyl chloride
2-(3,4-Dibenzyloxy-benzoyloxy)-4-benzyloxy-5,6-dimethoxyacetophenone
Conditions | Yield |
---|---|
With pyridine for 3h; Heating; | 800 mg |
4-(benzyloxy)benzoic acid chloride
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
With pyridine at 20℃; for 3h; |
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
hispidulin
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: pyridine / 3 h / 20 °C 2: KOH / pyridine / 4 h / 60 °C 3: sulfuric acid / acetic acid / 1.5 h / 60 °C 4: BCl3 / CH2Cl2 / 1.5 h / -65 °C View Scheme |
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: pyridine / 3 h / 20 °C 2: KOH / pyridine / 4 h / 60 °C 3: sulfuric acid / acetic acid / 1.5 h / 60 °C View Scheme |
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: pyridine / 3 h / 20 °C 2: KOH / pyridine / 4 h / 60 °C View Scheme |
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
5,7,4′-trihydroxy-6,3′,5′-trimethoxyflavone
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 52 percent / K2CO3 / acetone / 2 h / Heating 2: 1.) KOH, Py; 2.) HOAc-NaOAc / 1.) 60 deg C, 30 min; 2.) reflux, 2 h 3: 61 percent / HCl / acetic acid / 3 h / Heating View Scheme |
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 52 percent / K2CO3 / acetone / 2 h / Heating 2: 1.) KOH, Py; 2.) HOAc-NaOAc / 1.) 60 deg C, 30 min; 2.) reflux, 2 h 3: 61 percent / HCl / acetic acid / 3 h / Heating 4: 22 mg / Py / 24 h / Ambient temperature View Scheme |
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 52 percent / K2CO3 / acetone / 2 h / Heating 2: 1.) KOH, Py; 2.) HOAc-NaOAc / 1.) 60 deg C, 30 min; 2.) reflux, 2 h View Scheme |
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
2-Hydroxy-3',4',4-tribenzyloxy-5,6-dimethoxydibenzoylmethane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 800 mg / pyridine / 3 h / Heating 2: 450 mg / potassium hydroxide / pyridine / 2 h View Scheme |
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
3',4',7-trihydroxy-5,6-dimethoxyflavone
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 800 mg / pyridine / 3 h / Heating 2: 450 mg / potassium hydroxide / pyridine / 2 h 3: 150 mg / sodium acetate, glacial acetic acid / 3 h / Heating 4: 40 mg / hydrogene / Pd/C (10percent) / ethyl acetate / 5 h View Scheme |
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
7,3',4'-Tribenzyloxy-5,6-dimethoxyflavone
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 800 mg / pyridine / 3 h / Heating 2: 450 mg / potassium hydroxide / pyridine / 2 h 3: 150 mg / sodium acetate, glacial acetic acid / 3 h / Heating View Scheme |
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium hydroxide / ethanol / 48 h / 20 °C 2: palladium 10% on activated carbon; hydrogen / methanol / 1 h View Scheme | |
Multi-step reaction with 2 steps 1: potassium hydroxide / ethanol / 48 h / 20 °C 2: palladium 10% on activated carbon; hydrogen / methanol / 1 h View Scheme |
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: potassium hydroxide / ethanol / 48 h / 20 °C 2: palladium 10% on activated carbon; hydrogen / methanol / 1 h 3: potassium carbonate / acetone / 3 h / Reflux View Scheme | |
Multi-step reaction with 3 steps 1: potassium hydroxide / ethanol / 48 h / 20 °C 2: palladium 10% on activated carbon; hydrogen / methanol / 1 h 3: potassium carbonate / acetone / 3 h / Reflux View Scheme |
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: potassium hydroxide / ethanol / 48 h / 20 °C 2: palladium 10% on activated carbon; hydrogen / methanol / 1 h 3: potassium carbonate / acetone / 3 h / Reflux 4: toluene / 6 h / Reflux View Scheme | |
Multi-step reaction with 4 steps 1: potassium hydroxide / ethanol / 48 h / 20 °C 2: palladium 10% on activated carbon; hydrogen / methanol / 1 h 3: potassium carbonate / acetone / 3 h / Reflux 4: toluene / 6 h / Reflux View Scheme |
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: potassium hydroxide / ethanol / 48 h / 20 °C 2: palladium 10% on activated carbon; hydrogen / methanol / 1 h 3: potassium carbonate / acetone / 3 h / Reflux 4: toluene / 6 h / Reflux 5: palladium 10% on activated carbon; hydrogen / methanol / 1 h View Scheme | |
Multi-step reaction with 5 steps 1: potassium hydroxide / ethanol / 48 h / 20 °C 2: palladium 10% on activated carbon; hydrogen / methanol / 1 h 3: potassium carbonate / acetone / 3 h / Reflux 4: toluene / 6 h / Reflux 5: palladium 10% on activated carbon; hydrogen / methanol / 1 h View Scheme | |
Multi-step reaction with 4 steps 1.1: toluene / 18 h / 80 °C 1.2: 1 h / 0 - 50 °C 2.1: diisobutylaluminium hydride / toluene; tetrahydrofuran / -60 °C 3.1: toluene-4-sulfonic acid / benzene / 12 h / 0 °C / Reflux; Acidic conditions 4.1: hydrogen; palladium 10% on activated carbon / methanol / 1 h / 20 °C View Scheme | |
Multi-step reaction with 4 steps 1.1: toluene / 18 h / 80 °C 1.2: 1 h / 0 - 50 °C 2.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 0.08 h / -60 °C / Inert atmosphere 3.1: toluene-4-sulfonic acid / benzene / 12 h / 0 °C / Reflux; Acidic conditions 4.1: hydrogen; palladium 10% on activated carbon / methanol / 1 h / 20 °C View Scheme | |
Multi-step reaction with 4 steps 1.1: 1,2-dimethoxyethane / 20 h / 80 °C 1.2: 1 h / 0 - 50 °C 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / -60 °C 3.1: toluene-4-sulfonic acid / toluene / 12 h / 0 °C / Reflux 4.1: palladium 10% on activated carbon; hydrogen / methanol / 17 h / 20 °C View Scheme |
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
5,7-dihydroxy-6-methoxy-3-(3'-hydroxy-4'-methoxybenzyl)-4-chromanone
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: potassium hydroxide / ethanol / 48 h / 20 °C 2: palladium 10% on activated carbon; hydrogen / methanol / 1 h 3: potassium carbonate / acetone / 3 h / Reflux 4: toluene / 6 h / Reflux 5: palladium 10% on activated carbon; hydrogen / methanol / 1 h 6: 1-(Trimethylsilyl)imidazole / chloroform / 4 h / 0 - 60 °C View Scheme | |
Multi-step reaction with 6 steps 1: potassium hydroxide / ethanol / 48 h / 20 °C 2: palladium 10% on activated carbon; hydrogen / methanol / 1 h 3: potassium carbonate / acetone / 3 h / Reflux 4: toluene / 6 h / Reflux 5: palladium 10% on activated carbon; hydrogen / methanol / 1 h 6: trimethylsilyl iodide / chloroform / 0.5 h / 0 - 60 °C View Scheme | |
Multi-step reaction with 5 steps 1.1: toluene / 18 h / 80 °C 1.2: 1 h / 0 - 50 °C 2.1: diisobutylaluminium hydride / toluene; tetrahydrofuran / -60 °C 3.1: toluene-4-sulfonic acid / benzene / 12 h / 0 °C / Reflux; Acidic conditions 4.1: hydrogen; palladium 10% on activated carbon / methanol / 1 h / 20 °C 5.1: trimethylsilyl iodide / dichloromethane / 20 °C View Scheme | |
Multi-step reaction with 5 steps 1.1: toluene / 18 h / 80 °C 1.2: 1 h / 0 - 50 °C 2.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 0.08 h / -60 °C / Inert atmosphere 3.1: toluene-4-sulfonic acid / benzene / 12 h / 0 °C / Reflux; Acidic conditions 4.1: hydrogen; palladium 10% on activated carbon / methanol / 1 h / 20 °C 5.1: trimethylsilyl iodide / dichloromethane / 20 °C View Scheme |
1-(4-(benzyloxy)-6-hydroxy-2,3-dimethoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: toluene / 18 h / 80 °C 1.2: 1 h / 0 - 50 °C 2.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 0.08 h / -60 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1.1: 1,2-dimethoxyethane / 20 h / 80 °C 1.2: 1 h / 0 - 50 °C 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / -60 °C View Scheme |
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