GL Biochem (Shanghai) Ltd. founded in 1998, has become an internationally recognized biochemical manufacturing company that specializes in producing/synthesizing and providing peptide reagents, custom peptides and antibodies. GL Biochem is
Cas:29022-11-5
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inquiryItems Standard Result Assay 98%min ----------------------------------------------------------------------------------------------
Cas:29022-11-5
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inquiryDayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
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inquiryUnique advantages of FMOC-Glycine Cas 29022-11-5 Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White powder Storage:cool dry place Package:1kg/foil bag;25kg/drum Application:pharm
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inquiryhigh quality Appearance:white powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
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inquiryName:FMOC-Glycine CAS NO: 29022-11-5 Grade:Medical scientific research and export Molecular formula:C17H15NO4 Molecular weight:297.31 Product Quality 12 years of chemical raw materials Mature operation of the industry System stability Dat
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inquiryCompetitive Price High Quality Fast Delivery custom-made Welcome to Henan Tianfu Chemical Co., Ltd. website. Our company engages in Sodium Tripolyphosphate (STPP) and Sodium Hexametabphosphate (SHMP) production; development of noble me
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inquiryDensity: 1.1671 (rough estimate) Melting point: 174-175 ° C (lit.) Boiling point: 438.82 ° C (rough estimate) Flash point: 283.8 ° C Steam pressure: 9.69E-13mmHg at 25 ° C Solubility: most transparency in Methanol Refractive index: 1.
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inquiryProduct Name Fmoc-Gly-OH CAS No. 29022-11-5 Synonyms Fmoc-glycine Purity 98.0% min Molecular Formula C17H15NO4 Molecular Weight 297.3 Appearance: white powder Storage:Stor
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inquiryAbout Product Details Items Specifications Test Results Appearance White to white crystalline powde
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
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inquiryFMOC-Glycine CAS:29022-11-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediate
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inquiryProduct Name Fmoc-Gly-OH Molecular Formula C17H15NO4 CAS Number 29022-11-5 Molecular Weight 297.3 Appearance White to off-white microcrystalline powder
Cas:29022-11-5
Min.Order:1 Gram
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N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
With trifluoroacetic acid In dichloromethane at 20℃; for 0.0833333h; Reagent/catalyst; | 97% |
glycine
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 20℃; for 24h; | 96% |
9-fluorenylmethyl 4,6-dimethoxy-1,3,5-triazinyl carbonate
glycine
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
With sodium carbonate In acetonitrile at 20℃; for 0.333333h; | 96% |
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide
glycine
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In acetone Ambient temperature; | 95% |
Stage #1: glycine With N-cyclohexyl-cyclohexanamine In acetone at 20℃; Stage #2: N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide With sodium carbonate In water; acetonitrile at 0 - 20℃; pH=8; Stage #3: With potassium hydrogensulfate In water; acetonitrile pH=2 - 3; | 86% |
With pyridine In methanol | |
With sodium carbonate In 1,4-dioxane; water at 20℃; for 18h; |
glycine
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
With triethylamine In water Ambient temperature; | 94% |
1-[(9-fluorenylmethyloxycarbonyl)]benzotriazole
glycine
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
With triethylamine In water; acetonitrile at 20℃; for 2h; | 94% |
N-(((9H-fluoren-9-yl)methoxy)carbonyloxy)-2-morpholino-2-oxoacetimidoyl cyanide
glycine
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water; acetone | 93.5% |
N-(((9H-fluoren-9-yl)methoxy)carbonyloxy)-2-amino-2-oxoacetimidoyl cyanide
glycine
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
With sodium carbonate In water; acetone at 20℃; for 4h; pH=9 - 10; | 93% |
With sodium hydrogencarbonate In water; acetone | 90.8% |
(9H-fluoren-9-yl)methyl 2-oxopyridin-1(2H)-yl carbonate
glycine
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water; acetone | 92.8% |
diethyl 2-{[(9H-fluoren-9-yl)methoxy]carbonyloxyimino}-2-cyanoacetate
glycine
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water; acetone | 92.1% |
N-(((9H-fluoren-9-yl)methoxy)carbonyloxy)-2-oxo-2-(piperidin-1-yl)acetimidoyl cyanide
glycine
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water; acetone | 92.1% |
N-(((9H-fluoren-9-yl)methoxy)carbonyloxy)-2-(ethylamino)-2-oxoacetimidoyl cyanide
glycine
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water; acetone | 91.8% |
N-{[(9H-fluoren-9-yl)methoxy]carbonyloxy}picolinimidoyl cyanide
glycine
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water; acetone | 91.6% |
Fmoc-Gly-N3
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
With sodium tetrahydroborate In tetrahydrofuran; water cooling; | 90% |
3-(9-Fluorenylmethoxycarbonyl)-benzothiazoline-2-thione
glycine
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
With sodium hydroxide In 1,4-dioxane for 12h; Ambient temperature; | 88% |
glycine
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 20℃; for 2h; | 88% |
(fluorenylmethoxy)carbonyl chloride
glycine
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
In ethanol; water at 60℃; for 4h; chemoselective reaction; | 85% |
Stage #1: (fluorenylmethoxy)carbonyl chloride; glycine With sodium carbonate In 1,4-dioxane; water at 0 - 20℃; for 4h; Stage #2: With hydrogenchloride In water pH=2; | 85% |
With sodium carbonate; N-ethyl-N,N-diisopropylamine In water; N,N-dimethyl-formamide 1.) 0 deg C, 30 min; 2.) up to RT, 1 h; | 62% |
(9-fluorenyl)methyl pentafluorophenyl carbonate
glycine
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water; acetone Ambient temperature; | 84% |
methyl (((9H-fluoren-9-yl)methoxy)carbonyl)glycinate
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
With water; sodium hydroxide In isopropyl alcohol at 20℃; for 1h; chemoselective reaction; | 84% |
diethyl 2-{[(9H-fluoren-9-yl)methoxy]carbonyloxyimino}malonate
glycine
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water; acetone | 82.9% |
Carbonic acid 3,5-dioxo-4-aza-tricyclo[5.2.1.02,6]dec-8-en-4-yl ester 9H-fluoren-9-ylmethyl ester
glycine
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
With tertiary amine In 1,4-dioxane; water for 3h; | 81% |
N-Fmoc-glycine 2-(2-acetylphenyl)-1-methylethyl ester
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
In acetonitrile for 4h; Photolysis; | 56% |
{[(9H-fluoren-9-yl)methoxy]carbonyloxy}carbonimidoyl dicyanide
glycine
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water; acetone | 48.5% |
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
With methanol In dichloromethane for 0.5h; Ambient temperature; Yield given; |
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
With chymotrypsin In phosphate buffer for 16h; pH=8; |
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
With chymotrypsin In phosphate buffer for 16h; pH=8; |
Conditions | Yield |
---|---|
With ethylenediaminetetraacetic acid; DL-dithiothreitol; cathepsin B In phosphate buffer at 37℃; pH=6.7; Enzyme kinetics; |
(fluorenylmethoxy)carbonyl chloride
A
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 95 percent / Et3N / CH2Cl2 / 1 h / 20 °C 2: 96 percent / aq. Na2CO3 / acetonitrile / 0.33 h / 20 °C View Scheme |
N-(fluoren-9-ylmethoxycarbonyl)glycine
N,O-dimethylhydroxylamine*hydrochloride
(9H-fluoren-9-yl)methyl (2-(methoxy(methyl)amino)-2-oxoethyl)carbamate
Conditions | Yield |
---|---|
With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 4h; Inert atmosphere; | 100% |
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; | 98% |
Stage #1: N-(fluoren-9-ylmethoxycarbonyl)glycine With trichloroacetonitrile; triphenylphosphine In tetrahydrofuran at 20℃; for 1h; Inert atmosphere; Stage #2: N,O-dimethylhydroxylamine*hydrochloride With triethylamine In tetrahydrofuran at 20℃; for 1h; Inert atmosphere; | 89% |
Conditions | Yield |
---|---|
Multistep reaction; | A n/a B 100% |
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
Stage #1: Fmoc-Lys(Dde)-Rink-PS-resin With 1H-imidazole; 1-methyl-pyrrolidin-2-one; hydroxylamine hydrochloride In dichloromethane for 3h; Stage #2: N-(fluoren-9-ylmethoxycarbonyl)glycine With benzotriazol-1-ol; dacarbazine In N,N-dimethyl-formamide Stage #3: With chlorotriisopropylsilane; trifluoroacetic acid In dichloromethane | 100% |
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
Stage #1: Pro-Val-Leu-Cys(Trt)-Ala-Wang resin; N-(fluoren-9-ylmethoxycarbonyl)glycine With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine In dichloromethane; N,N-dimethyl-formamide at 20℃; for 3h; Stage #2: With piperidine In N,N-dimethyl-formamide at 20℃; for 0.25h; | 100% |
N-(fluoren-9-ylmethoxycarbonyl)glycine
Fmoc-Gly-NH2
Conditions | Yield |
---|---|
With N-hydroxybenzotriazole ammonium salt; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 0 - 20℃; | 100% |
Stage #1: N-(fluoren-9-ylmethoxycarbonyl)glycine With Rink amide resin after treatment with piperidine in DMF; benzotriazol-1-ol; dacarbazine In N,N-dimethyl-formamide at 120℃; for 0.0833333h; microwave irradiation; Stage #2: With trifluoroacetic acid In dichloromethane at 20℃; for 1h; | 93% |
Stage #1: N-(fluoren-9-ylmethoxycarbonyl)glycine With 1,3,5-trichloro-2,4,6-triazine; potassium carbonate In tetrahydrofuran for 0.0166667h; Milling; Stage #2: With ammonium thiocyanate In tetrahydrofuran for 0.0833333h; Milling; | 86% |
N-(fluoren-9-ylmethoxycarbonyl)glycine
Conditions | Yield |
---|---|
With benzotriazol-1-ol; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 24h; | 100% |
Conditions | Yield |
---|---|
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In tetrahydrofuran | 100% |
N-(fluoren-9-ylmethoxycarbonyl)glycine
N-Fmoc L-Phe
Fmoc-(tBu)Asp-OH
Fmoc-Arg(Pbf)-OH
(S)-6-allyloxycarbonylamino-2-(9H-fluoren-9-ylmethoxycarbonylamino)-hexanoic acid
Conditions | Yield |
---|---|
Stage #1: N-(fluoren-9-ylmethoxycarbonyl)glycine With N-ethyl-N,N-diisopropylamine In methanol; dichloromethane for 0.25h; solid phase reaction; Stage #2: With piperidine In N,N-dimethyl-formamide for 0.166667h; Automated synthesizer; solid phase reaction; Stage #3: N-Fmoc L-Phe; Fmoc-(tBu)Asp-OH; Fmoc-Arg(Pbf)-OH; (S)-6-allyloxycarbonylamino-2-(9H-fluoren-9-ylmethoxycarbonylamino)-hexanoic acid Further stages; | 100% |
Conditions | Yield |
---|---|
With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 20℃; | 100% |
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