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inquiryCAS No.: 356560-84-4 Synonyms: 1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione; QC-1211; 1-([1,2,4]triazolo[1,5-a]pyridin
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inquiry1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione CAS: 356560-84-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chem
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inquiryPKA:0.85±0.10(Predicted) PSA:77.22000 Density:1.39±0.1 g/cm3(Predicted) LogP:1.49830 Storage Temp.:Sealed in dry,Room Temperature Purity/Quality: 99% Appearance:white powder Storage:cool and dry environment Package:accordi
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
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inquiry1,2-Ethanedione, 1-(6-Methyl-2-pyridinyl)-2-[1,2,4]triazolo[1,5-a]pyridin-6-yl-;1-(6-Methyl-2 -pyridinyl)-2-[1,2,4]triazolo[1,5-a]pyridine-6-yl-1,2-ethanedione;1-([1,2,4]triazolo[1,5-a ]pyridin-6-yl)-2-(6-methylpyridin-2-yl); 1-([1,2,4]triazolo[1,5
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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inquiryhight degree of purity Application:Fine chemical intermediates, used as the main raw material for he synthesis of various pesticides, medicines, surfactants, polymer monomers, Ond Ontifungal agents
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inquiry1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione Application:1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
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inquirygood quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:25kg,50kg,180kg,200kg,250kg,1000kg,customization Application:Pharma;Industry;Agricultural;chemical reaserch Tran
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inquiry1-([1,2,4]Triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione cas 356560-84-4Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by s
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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inquiry1-(6-methylpyridin-2-yl)-2-([1,2,4]triazolo[1,5-a]pyridin-6-yl)ethanone
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
Conditions | Yield |
---|---|
With hydrogen bromide; dimethyl sulfoxide at 60 - 70℃; for 2h; | 92% |
With water; hydrogen bromide In dimethyl sulfoxide at 60 - 70℃; for 2h; |
6-methyl-2-pyridinecarboxaldehyde
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: ziconium(IV) oxychloride octahydrate / 1 h / 20 °C 2.1: caesium carbonate / isopropyl alcohol; tetrahydrofuran / 20 °C 2.2: 1 h 2.3: pH 7 - 8 3.1: dimethyl sulfoxide; hydrogen bromide / 2 h / 60 - 70 °C View Scheme |
diphenyl (6-methylpyridin-2-yl)(phenylamino)methylphosphonate
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: caesium carbonate / isopropyl alcohol; tetrahydrofuran / 20 °C 1.2: 1 h 1.3: pH 7 - 8 2.1: dimethyl sulfoxide; hydrogen bromide / 2 h / 60 - 70 °C View Scheme |
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
dimethoxyacetaldehyde
6-(2-(dimethoxymethyl)-5-(6-methylpyridin-2-yl)-1H-imidazol-4-yl)-[1,2,4]triazolo[1,5-a]pyridine
Conditions | Yield |
---|---|
With ammonium acetate In methanol; tert-butyl methyl ether; water at 20℃; for 4h; | 83% |
With ammonium acetate In methanol; tert-butyl methyl ether; water at 20℃; for 4h; | 83% |
Stage #1: 1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione; dimethoxyacetaldehyde With ammonium acetate In methanol; tert-butyl methyl ether; water at 20℃; for 3h; Stage #2: With sodium hydrogencarbonate In methanol; tert-butyl methyl ether; water pH=8; | 78% |
N-phthalimidyl-2-aminoacetaldehyde
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
2-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)isoindoline-1,3-dione
Conditions | Yield |
---|---|
With ammonium acetate In methanol; tert-butyl methyl ether at 20 - 50℃; for 10h; | 67% |
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
2-phenoxyethanal
6-(5-(6-methylpyridin-2-yl)-2-(phenoxymethyl)-1H-imidazol-4-yl)-[1,2,4]triazolo[1,5-a]pyridine
Conditions | Yield |
---|---|
With ammonium acetate In methanol; tert-butyl methyl ether at 20℃; for 1.16667h; Inert atmosphere; | 56% |
With ammonium acetate In methanol; tert-butyl methyl ether at 20℃; Inert atmosphere; | 56% |
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
2-(phenylthio)acetaldehyde
6-(5-(6-methylpyridin-2-yl)-2-((phenylthio)methyl)-1H-imidazol-4-yl)-[1,2,4]triazolo[1,5-a]pyridine
Conditions | Yield |
---|---|
With ammonium acetate In methanol; tert-butyl methyl ether at 20℃; for 1.16667h; Inert atmosphere; | 38% |
With ammonium acetate In methanol; tert-butyl methyl ether at 20℃; Inert atmosphere; | 38% |
6,7-dimethoxy-3,4-dihydro-isoquinoline
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
Conditions | Yield |
---|---|
With ammonium acetate; acetic acid In tert-butyl methyl ether Heating / reflux; | 37% |
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
3-cyanophenyl-1-acetaldehyde
3-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)benzonitrile
Conditions | Yield |
---|---|
Stage #1: 1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione; 3-cyanophenyl-1-acetaldehyde With ammonium acetate In methanol; tert-butyl methyl ether at 20℃; for 1.5h; Inert atmosphere; Stage #2: With sodium hydrogencarbonate In methanol; tert-butyl methyl ether; water pH=8; Inert atmosphere; | 33% |
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
2-((2-fluorophenyl)(methyl)amino)acetaldehyde
N-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)-2-fluoro-N-methylaniline
Conditions | Yield |
---|---|
Stage #1: 1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione; 2-((2-fluorophenyl)(methyl)amino)acetaldehyde With ammonium acetate In methanol; tert-butyl methyl ether at 20℃; for 2h; Inert atmosphere; Stage #2: With sodium hydrogencarbonate In methanol; tert-butyl methyl ether; water pH=8; Inert atmosphere; | 32% |
C8H12ClNO2
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
Conditions | Yield |
---|---|
Stage #1: C8H12ClNO2; 1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione With ethanol; ammonium acetate at 70℃; for 10h; Stage #2: With water; sodium carbonate In ethanol; dichloromethane; water |
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
1-oxo-2-oxaspiro[4.5]decane-8-carbaldehyde
8-(5-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-4-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)-2-oxaspiro[4.5]decan-1-one
Conditions | Yield |
---|---|
With ammonium acetate; acetic acid In tert-butyl methyl ether Heating / reflux; |
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
N-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)-3-vinylaniline
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: ammonium acetate / water; tert-butyl methyl ether; methanol / 3 h / 20 °C 1.2: pH 8 2.1: hydrogenchloride; water / 3 h / 70 °C 2.2: 0 °C 3.1: acetic acid / 1,2-dichloro-ethane / 2 h / 80 °C 3.2: 0 - 40 °C View Scheme | |
Multi-step reaction with 4 steps 1: ammonium acetate / methanol; tert-butyl methyl ether; water / 4 h / 20 °C 2: hydrogenchloride / water / 4 h / 70 °C 3: acetic acid / 1,2-dichloro-ethane / 2 h / 120 °C / Inert atmosphere; Sealed tube 4: sodium tetrahydroborate / methanol; tetrahydrofuran / 3 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1.1: ammonium acetate / tert-butyl methyl ether; methanol; water / 4 h / 20 °C 2.1: hydrogenchloride / water / 4 h / 70 °C 3.1: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4.1: sodium tetrahydroborate / methanol; tetrahydrofuran / 3 h / 0 - 20 °C 4.2: 0 °C / pH 7-8 View Scheme |
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
3-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methylamino)-4-((dimethylamino)methyl)benzonitrile
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: ammonium acetate / water; tert-butyl methyl ether; methanol / 3 h / 20 °C 1.2: pH 8 2.1: hydrogenchloride; water / 3 h / 70 °C 2.2: 0 °C 3.1: acetic acid / 1,2-dichloro-ethane / 80 °C 3.2: 0 - 20 °C View Scheme | |
Multi-step reaction with 4 steps 1: ammonium acetate / methanol; tert-butyl methyl ether; water / 4 h / 20 °C 2: hydrogenchloride / water / 4 h / 70 °C 3: acetic acid / 1,2-dichloro-ethane / 2 h / 120 °C / Inert atmosphere; Sealed tube 4: sodium tetrahydroborate / methanol; tetrahydrofuran / 3 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1.1: ammonium acetate / tert-butyl methyl ether; methanol; water / 4 h / 20 °C 2.1: hydrogenchloride / water / 4 h / 70 °C 3.1: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4.1: sodium tetrahydroborate / methanol; tetrahydrofuran / 3 h / 0 - 20 °C 4.2: 0 °C / pH 7-8 View Scheme |
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazole-2-carbaldehyde
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: ammonium acetate / water; tert-butyl methyl ether; methanol / 3 h / 20 °C 1.2: pH 8 2.1: hydrogenchloride; water / 3 h / 70 °C 2.2: 0 °C View Scheme | |
Multi-step reaction with 2 steps 1: ammonium acetate / methanol; tert-butyl methyl ether; water / 4 h / 20 °C 2: hydrogenchloride / water / 4 h / 70 °C View Scheme | |
Multi-step reaction with 2 steps 1: ammonium acetate / tert-butyl methyl ether; methanol; water / 4 h / 20 °C 2: hydrogenchloride / water / 4 h / 70 °C View Scheme |
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
N-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)-3-vinylaniline sulfate
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: ammonium acetate / water; tert-butyl methyl ether; methanol / 3 h / 20 °C 1.2: pH 8 2.1: hydrogenchloride; water / 3 h / 70 °C 2.2: 0 °C 3.1: acetic acid / 1,2-dichloro-ethane / 2 h / 80 °C 3.2: 0 - 40 °C 4.1: sulfuric acid / ethanol / 0 - 20 °C View Scheme |
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
N-((4-([1,2,4]triazolo[1,5-a]pyridine-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)-2-fluoroaniline
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: ammonium acetate / methanol; tert-butyl methyl ether; water / 4 h / 20 °C 2: hydrogenchloride / water / 4 h / 70 °C 3: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4: sodium tetrahydroborate / methanol; tetrahydrofuran / 3 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1.1: ammonium acetate / tert-butyl methyl ether; methanol; water / 4 h / 20 °C 2.1: hydrogenchloride / water / 4 h / 70 °C 3.1: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4.1: sodium tetrahydroborate / methanol; tetrahydrofuran / 3 h / 0 - 20 °C 4.2: 0 °C / pH 7-8 View Scheme |
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
N-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)-2-chloroaniline
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: ammonium acetate / methanol; tert-butyl methyl ether; water / 4 h / 20 °C 2: hydrogenchloride / water / 4 h / 70 °C 3: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4: sodium tris(acetoxy)borohydride / methanol; tetrahydrofuran / 3 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1.1: ammonium acetate / tert-butyl methyl ether; methanol; water / 4 h / 20 °C 2.1: hydrogenchloride / water / 4 h / 70 °C 3.1: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4.1: sodium tris(acetoxy)borohydride / methanol; tetrahydrofuran / 3 h / 0 - 20 °C 4.2: 0 °C / pH 7-8 View Scheme |
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
N-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)-2-bromoaniline
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: ammonium acetate / methanol; tert-butyl methyl ether; water / 4 h / 20 °C 2: hydrogenchloride / water / 4 h / 70 °C 3: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4: sodium tetrahydroborate / methanol; tetrahydrofuran / 3 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1.1: ammonium acetate / tert-butyl methyl ether; methanol; water / 4 h / 20 °C 2.1: hydrogenchloride / water / 4 h / 70 °C 3.1: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4.1: sodium tetrahydroborate / methanol; tetrahydrofuran / 3 h / 0 - 20 °C 4.2: 0 °C / pH 7-8 View Scheme |
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
N-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)-2-methylaniline
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: ammonium acetate / methanol; tert-butyl methyl ether; water / 4 h / 20 °C 2: hydrogenchloride / water / 4 h / 70 °C 3: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4: sodium tris(acetoxy)borohydride / methanol; tetrahydrofuran / 3 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1.1: ammonium acetate / tert-butyl methyl ether; methanol; water / 4 h / 20 °C 2.1: hydrogenchloride / water / 4 h / 70 °C 3.1: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4.1: sodium tris(acetoxy)borohydride / methanol; tetrahydrofuran / 3 h / 0 - 20 °C 4.2: 0 °C / pH 7-8 View Scheme |
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
N-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)-2-ethylaniline
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: ammonium acetate / methanol; tert-butyl methyl ether; water / 4 h / 20 °C 2: hydrogenchloride / water / 4 h / 70 °C 3: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4: sodium tris(acetoxy)borohydride / methanol; tetrahydrofuran / 3 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1.1: ammonium acetate / tert-butyl methyl ether; methanol; water / 4 h / 20 °C 2.1: hydrogenchloride / water / 4 h / 70 °C 3.1: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4.1: sodium tris(acetoxy)borohydride / methanol; tetrahydrofuran / 3 h / 0 - 20 °C 4.2: 0 °C / pH 7-8 View Scheme |
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
N-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)-2-isopropylaniline
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: ammonium acetate / methanol; tert-butyl methyl ether; water / 4 h / 20 °C 2: hydrogenchloride / water / 4 h / 70 °C 3: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4: sodium tris(acetoxy)borohydride / methanol; tetrahydrofuran / 3 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1.1: ammonium acetate / tert-butyl methyl ether; methanol; water / 4 h / 20 °C 2.1: hydrogenchloride / water / 4 h / 70 °C 3.1: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4.1: sodium tris(acetoxy)borohydride / methanol; tetrahydrofuran / 3 h / 0 - 20 °C 4.2: 0 °C / pH 7-8 View Scheme |
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
N-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)-2-methoxyaniline
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: ammonium acetate / methanol; tert-butyl methyl ether; water / 4 h / 20 °C 2: hydrogenchloride / water / 4 h / 70 °C 3: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4: sodium tris(acetoxy)borohydride / methanol; tetrahydrofuran / 3 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1.1: ammonium acetate / tert-butyl methyl ether; methanol; water / 4 h / 20 °C 2.1: hydrogenchloride / water / 4 h / 70 °C 3.1: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4.1: sodium tris(acetoxy)borohydride / methanol; tetrahydrofuran / 3 h / 0 - 20 °C 4.2: 0 °C / pH 7-8 View Scheme |
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
N-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)-2-(trifluoromethoxy)aniline
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: ammonium acetate / methanol; tert-butyl methyl ether; water / 4 h / 20 °C 2: hydrogenchloride / water / 4 h / 70 °C 3: acetic acid / 1,2-dichloro-ethane / 2 h / Inert atmosphere 4: sodium tetrahydroborate / methanol; tetrahydrofuran / 3 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1.1: ammonium acetate / tert-butyl methyl ether; methanol; water / 4 h / 20 °C 2.1: hydrogenchloride / water / 4 h / 70 °C 3.1: 1,2-dichloro-ethane / 2 h / 20 °C / Inert atmosphere 4.1: sodium tetrahydroborate / methanol; tetrahydrofuran / 3 h / 0 - 20 °C 4.2: 0 °C / pH 7-8 View Scheme |
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
N-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)-2-(methylthio)aniline
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: ammonium acetate / methanol; tert-butyl methyl ether; water / 4 h / 20 °C 2: hydrogenchloride / water / 4 h / 70 °C 3: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4: sodium tris(acetoxy)borohydride / methanol; tetrahydrofuran / 3 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1.1: ammonium acetate / tert-butyl methyl ether; methanol; water / 4 h / 20 °C 2.1: hydrogenchloride / water / 4 h / 70 °C 3.1: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4.1: sodium tris(acetoxy)borohydride / methanol; tetrahydrofuran / 3 h / 0 - 20 °C 4.2: 0 °C / pH 7-8 View Scheme |
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
N-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)-2-vinylaniline
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: ammonium acetate / methanol; tert-butyl methyl ether; water / 4 h / 20 °C 2: hydrogenchloride / water / 4 h / 70 °C 3: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4: sodium tris(acetoxy)borohydride / methanol; tetrahydrofuran / 3 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1.1: ammonium acetate / tert-butyl methyl ether; methanol; water / 4 h / 20 °C 2.1: hydrogenchloride / water / 4 h / 70 °C 3.1: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4.1: sodium tris(acetoxy)borohydride / methanol; tetrahydrofuran / 3 h / 0 - 20 °C 4.2: 0 °C / pH 7-8 View Scheme |
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
2-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methylamino)benzonitrile
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: ammonium acetate / methanol; tert-butyl methyl ether; water / 4 h / 20 °C 2: hydrogenchloride / water / 4 h / 70 °C 3: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4: sodium tetrahydroborate / methanol; tetrahydrofuran / 3 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1.1: ammonium acetate / tert-butyl methyl ether; methanol; water / 4 h / 20 °C 2.1: hydrogenchloride / water / 4 h / 70 °C 3.1: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4.1: sodium tetrahydroborate / methanol; tetrahydrofuran / 3 h / 0 - 20 °C 4.2: 0 °C / pH 7-8 View Scheme |
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
2-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methylamino)benzamide
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: ammonium acetate / methanol; tert-butyl methyl ether; water / 4 h / 20 °C 2: hydrogenchloride / water / 4 h / 70 °C 3: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4: sodium tetrahydroborate / methanol; tetrahydrofuran / 3 h / 20 °C / Inert atmosphere 5: sodium hydroxide; dihydrogen peroxide / ethanol / 20 °C View Scheme | |
Multi-step reaction with 5 steps 1.1: ammonium acetate / tert-butyl methyl ether; methanol; water / 4 h / 20 °C 2.1: hydrogenchloride / water / 4 h / 70 °C 3.1: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4.1: sodium tetrahydroborate / methanol; tetrahydrofuran / 3 h / 0 - 20 °C 4.2: 0 °C / pH 7-8 5.1: dihydrogen peroxide; sodium hydroxide / ethanol / 20 °C View Scheme |
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
N-(2-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methylamino)phenyl)methanesulfonamide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: ammonium acetate / methanol; tert-butyl methyl ether; water / 4 h / 20 °C 2: hydrogenchloride / water / 4 h / 70 °C 3: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4: sodium tetrahydroborate / methanol; tetrahydrofuran / 3 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1.1: ammonium acetate / tert-butyl methyl ether; methanol; water / 4 h / 20 °C 2.1: hydrogenchloride / water / 4 h / 70 °C 3.1: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4.1: sodium tetrahydroborate / methanol; tetrahydrofuran / 3 h / 0 - 20 °C 4.2: 0 °C / pH 7-8 View Scheme |
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione
N-(2-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methylamino)phenyl)acetamide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: ammonium acetate / methanol; tert-butyl methyl ether; water / 4 h / 20 °C 2: hydrogenchloride / water / 4 h / 70 °C 3: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4: sodium tetrahydroborate / methanol; tetrahydrofuran / 3 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1.1: ammonium acetate / tert-butyl methyl ether; methanol; water / 4 h / 20 °C 2.1: hydrogenchloride / water / 4 h / 70 °C 3.1: acetic acid / 1,2-dichloro-ethane / 2 h / Reflux; Inert atmosphere 4.1: sodium tetrahydroborate / methanol; tetrahydrofuran / 3 h / 0 - 20 °C 4.2: 0 °C / pH 7-8 View Scheme |
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