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Yantai Xianhua Technology Group Co., Ltd

Sales: 1.24hours to reply your E-mail 2.Market information trend share with customers Suggestion for purchase decision Reputation: 1.Implementing contract terms strictly 2.Timely solve any discrepancy Research and development strength 1.

4'-Pentyl-[1,1'-Biphenyl]-4-carbonitrile

Cas:40817-08-1

Min.Order:0 Metric Ton

FOB Price: $1.0

Type:Other

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Henan Wentao Chemical Product Co., Ltd.

We are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED

4-Cyano-4'-pentylbiphenylCAS NO.: 40817-08-1

Cas:40817-08-1

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

4-Cyano-4'-pentylbiphenyl

Cas:40817-08-1

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 4-Cyano-4'-Pentylbiphenyl with high purity

Cas:40817-08-1

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Hangzhou Dingyan Chem Co., Ltd

Items Standard Result Appearance Milky white liquid Milky white liquid Purity ≥99.5%

Top purity 4-Cyano-4'-n-pentylbiphenyl with high quality and best price cas:40817-08-1

Cas:40817-08-1

Min.Order:1 Kilogram

FOB Price: $3.0 / 10.0

Type:Manufacturers

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Ality Chemical Corporation

ProName:4-Cyano-4'-pentylbiphenyl CAS NO.40817... CasNo:40817-08-1 Molecular Formula:C18H19N Appearance:Lyophilized White Powder Application:he preparation of vanilla.Used in pest... DeliveryTime:within 5-7 days after rec

Factory Supply 4-Cyano-4'-pentylbiphenyl

Cas:40817-08-1

Min.Order:1 Kilogram

FOB Price: $0.5 / 1.0

Type:Other

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Hebei yanxi chemical co.,LTD.

hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm

4-Cyano-4'-pentylbiphenyl CAS NO.40817-08-1

Cas:40817-08-1

Min.Order:1 Metric Ton

FOB Price: $1.0 / 3.0

Type:Manufacturers

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Henan Allgreen Chemical Co.,Ltd

high quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai

4-Cyano-4'-pentylbiphenyl

Cas:40817-08-1

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

inquiry

Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

High Quality 99% [1,1'-Biphenyl]-4-carbonitrile,4'-pentyl- 40817-08-1 ISO Manufacturer

Cas:40817-08-1

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

4-Cyano-4'-pentylbiphenyl

Cas:40817-08-1

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

Factory price Potassium hydrogen 4-Cyano-4'-pentylbiphenyl CAS 40817-08-1 in stock Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.O

Factory price 4-Cyano-4'-pentylbiphenyl CAS 40817-08-1 in stock

Cas:40817-08-1

Min.Order:1 Gram

FOB Price: $50.0

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu

4-Cyano-4′ -Pentylbiphenyl 5CB CAS: 40817-08-1

Cas:40817-08-1

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Manufacturer supply CAS 40817-08-1 with best quality

Cas:40817-08-1

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

High purity 4-Cyano-4’-Penylbihpenyl TOP supplier CAS NO.40817-08-1

Cas:40817-08-1

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Henan Sinotech Import&Export Corporation

Product Name: 4-Cyano-4'-pentylbiphenyl CAS No.: 40817-08-1 Molecular Formula:C18H19N Molecular Weight:249.35 Appearance: White crystal Specification: GC>99.7% Impurity max:<0.2% Packaging:5kg/drum Ca

4-Cyano-4'-pentylbiphenyl

Cas:40817-08-1

Min.Order:10 Kilogram

FOB Price: $1.0

Type:Other

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Jinan Finer Chemical Co., Ltd

Product Description Product website: http://www.finerchem.com/pro01en/id/2045.html Product Name 4-Cyano-4'-pentylbiphenyl

4-Cyano-4'-pentylbiphenyl

Cas:40817-08-1

Min.Order:1 Gram

FOB Price: $11.0

Type:Lab/Research institutions

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Hangzhou Sartort Biopharma Co., Ltd

Appearance:white to light yellow crystal Storage:R.T Package:25kg/drum Application:Liquid crystal monomer Transportation:Express/Sea/Air Port:Any port in China

4-Cyano-4'-pentylbiphenyl cas 40817-08-1

Cas:40817-08-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

[1,1'-Biphenyl]-4-carbonitrile,4'-pentyl- 40817-08-1

Cas:40817-08-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese

4-Cyano-4'-pentylbiphenyl

Cas:40817-08-1

Min.Order:1 Kilogram

FOB Price: $300.0 / 325.0

Type:Trading Company

inquiry

Qingdao Beluga Import and Export Co., LTD

4-Cyano-4'-pentylbiphenyl CAS: 40817-08-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality or

4-Cyano-4'-pentylbiphenyl CAS: 40817-08-1

Cas:40817-08-1

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

[1,1'-Biphenyl]-4-carbonitrile,4'-pentyl-

Cas:40817-08-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Lonwin Chemical Group Limited

4-Cyano-4'-pentylbiphenyl CAS: 40817-08-1 Specification Item Standard Identification A.H-NMR:Comply with the structure B.LC-MS:Comply with the structure C.The

Factory supply 4-Cyano-4'-pentylbiphenyl

Cas:40817-08-1

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

4-Cyano-4'-Pentylbiphenyl

Cas:40817-08-1

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Triumph International Development Limilted

Triumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Business Custom Synthesis: Trading(Raw Mater

4-Cyano-4'-pentylbiphenyl

Cas:40817-08-1

Min.Order:0 Metric Ton

FOB Price: $18.0 / 20.0

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

4-Cyano-4'-pentylbiphenyl

Cas:40817-08-1

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Afine Chemicals Limited

Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

4-CYANO-4'-PENTYLBIPHENYL

Cas:40817-08-1

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

4-Cyano-4'-pentylbiphenyl

Cas:40817-08-1

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

[1,1'-Biphenyl]-4-carbonitrile,4'-pentyl-

Cas:40817-08-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

4-Cyano-4’-pentylbiphenyl

Cas:40817-08-1

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

4-PENTYL-4-BIPHENYLCARBONITRILE

Cas:40817-08-1

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Synthetic route

copper(I) cyanide
544-92-3

copper(I) cyanide

4-iodoo-4'-n-pentylbiphenyl
69971-79-5

4-iodoo-4'-n-pentylbiphenyl

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

Conditions
ConditionsYield
In N,N-dimethyl-formamide for 6h; Heating;90.5%
4-(4-pentylphenyl)bromobenzene
63619-59-0

4-(4-pentylphenyl)bromobenzene

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

Conditions
ConditionsYield
Stage #1: 4-(4-pentylphenyl)bromobenzene With iodine; magnesium In tetrahydrofuran at 70℃;
Stage #2: With N,N-dimethyl-formamide In tetrahydrofuran at 0℃; for 2h;
Stage #3: With ammonia; iodine In tetrahydrofuran; water at 20℃; for 2h;
80%
4-bromobenzenecarbonitrile
623-00-7

4-bromobenzenecarbonitrile

(dichloro)(ethyl)<4-(pentyl)phenyl>silane
159259-35-5

(dichloro)(ethyl)<4-(pentyl)phenyl>silane

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

Conditions
ConditionsYield
With potassium fluoride; palladium diacetate; tris-(o-tolyl)phosphine In N,N-dimethyl-formamide at 120℃;73%
4-formyl-4'-n-pentylbiphenyl oxime
80563-32-2

4-formyl-4'-n-pentylbiphenyl oxime

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

Conditions
ConditionsYield
With acetic anhydride for 2h; Heating;73%
tert-butyl isocyanide
630-18-2

tert-butyl isocyanide

4-(4-pentylphenyl)bromobenzene
63619-59-0

4-(4-pentylphenyl)bromobenzene

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

Conditions
ConditionsYield
Stage #1: 4-(4-pentylphenyl)bromobenzene With n-butyllithium In tetrahydrofuran; hexane at -50℃; for 0.5h; Inert atmosphere;
Stage #2: tert-butyl isocyanide In tetrahydrofuran; hexane at -50 - 20℃; for 0.5h; Inert atmosphere; Further stages;
73%
4-(4-pentylphenyl)bromobenzene
63619-59-0

4-(4-pentylphenyl)bromobenzene

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

Conditions
ConditionsYield
Stage #1: 4-(4-pentylphenyl)bromobenzene With n-butyllithium In tetrahydrofuran; hexane at -70℃; for 2h;
Stage #2: N,N-dimethyl-formamide In tetrahydrofuran at 0℃; for 2h;
Stage #3: With 1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione; ammonia In tetrahydrofuran; water at 20℃; for 2h;
72%
4-morpholinoacetonitrile
5807-02-3

4-morpholinoacetonitrile

4'-pentyl-[1,1'-biphenyl]-4-yl dimethylcarbamate

4'-pentyl-[1,1'-biphenyl]-4-yl dimethylcarbamate

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

Conditions
ConditionsYield
With potassium phosphate; nickel dibromide; zinc; 1,2-bis-(dicyclohexylphosphino)ethane In toluene at 150℃; for 18h; Inert atmosphere; Glovebox; Sealed tube;68%
4-bromobenzenecarbonitrile
623-00-7

4-bromobenzenecarbonitrile

(4-pentylphenyl)boronic acid
121219-12-3

(4-pentylphenyl)boronic acid

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

Conditions
ConditionsYield
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; potassium carbonate In 1,4-dioxane; water at 100℃; for 1h; Suzuki-Miyaura Coupling; Inert atmosphere;26%
biphenyl
92-52-4

biphenyl

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: AlCl3 / CH2Cl2 / 5 h / Ambient temperature
2: 1) hydrazine hydrate, 2) KOH / 1) diethylene glycol, 130 deg C, 1 h, 2) diethylene glycol, 130 deg C, 2 h, then 160 deg C, 3 h
3: 1) TiCl4, 2) hydroxylamine hydrochloride, pyridine / 1) CH2Cl2, 0 deg C, 30 min, 2) ethanol, reflux, 2 h
4: 73 percent / acetic anhydride / 2 h / Heating
View Scheme
1-[1,1'-biphenyl]-4-yl-1-pentanone
42916-73-4

1-[1,1'-biphenyl]-4-yl-1-pentanone

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1) hydrazine hydrate, 2) KOH / 1) diethylene glycol, 130 deg C, 1 h, 2) diethylene glycol, 130 deg C, 2 h, then 160 deg C, 3 h
2: 1) TiCl4, 2) hydroxylamine hydrochloride, pyridine / 1) CH2Cl2, 0 deg C, 30 min, 2) ethanol, reflux, 2 h
3: 73 percent / acetic anhydride / 2 h / Heating
View Scheme
Multi-step reaction with 3 steps
1: 145.6 g / 80percent hydrazine hydrate, KOH / bis-(2-hydroxy-ethyl) ether / 3 h / 130 °C
2: 71.9 percent / 98percent H2SO4, HIO3, I2 / acetic acid; H2O; CCl4 / 10 h / 80 °C
3: 90.5 percent / dimethylformamide / 6 h / Heating
View Scheme
1-pentyl-4-phenylbenzene
7116-96-3

1-pentyl-4-phenylbenzene

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1) TiCl4, 2) hydroxylamine hydrochloride, pyridine / 1) CH2Cl2, 0 deg C, 30 min, 2) ethanol, reflux, 2 h
2: 73 percent / acetic anhydride / 2 h / Heating
View Scheme
Multi-step reaction with 2 steps
1: 71.9 percent / 98percent H2SO4, HIO3, I2 / acetic acid; H2O; CCl4 / 10 h / 80 °C
2: 90.5 percent / dimethylformamide / 6 h / Heating
View Scheme
n-valeryl chloride
638-29-9

n-valeryl chloride

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: AlCl3 / CH2Cl2 / 5 h / Ambient temperature
2: 1) hydrazine hydrate, 2) KOH / 1) diethylene glycol, 130 deg C, 1 h, 2) diethylene glycol, 130 deg C, 2 h, then 160 deg C, 3 h
3: 1) TiCl4, 2) hydroxylamine hydrochloride, pyridine / 1) CH2Cl2, 0 deg C, 30 min, 2) ethanol, reflux, 2 h
4: 73 percent / acetic anhydride / 2 h / Heating
View Scheme
4-pentylbromobenzene
51554-95-1

4-pentylbromobenzene

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 96 percent / Mg / tetrahydrofuran / 12 h / Ambient temperature
2: 73 percent / KF / Pd(OAc)2, P(o-Tol)3 / dimethylformamide / 120 °C
View Scheme
biphenyl
92-52-4

biphenyl

sulfur

sulfur

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: AlCl3 / hexane / 2 h / 45 °C
2: 145.6 g / 80percent hydrazine hydrate, KOH / bis-(2-hydroxy-ethyl) ether / 3 h / 130 °C
3: 71.9 percent / 98percent H2SO4, HIO3, I2 / acetic acid; H2O; CCl4 / 10 h / 80 °C
4: 90.5 percent / dimethylformamide / 6 h / Heating
View Scheme
n-valeryl chloride
638-29-9

n-valeryl chloride

petroleum ether

petroleum ether

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: AlCl3 / hexane / 2 h / 45 °C
2: 145.6 g / 80percent hydrazine hydrate, KOH / bis-(2-hydroxy-ethyl) ether / 3 h / 130 °C
3: 71.9 percent / 98percent H2SO4, HIO3, I2 / acetic acid; H2O; CCl4 / 10 h / 80 °C
4: 90.5 percent / dimethylformamide / 6 h / Heating
View Scheme
4-iodobenzonitrile
3058-39-7

4-iodobenzonitrile

(4-pentylphenyl)boronic acid
121219-12-3

(4-pentylphenyl)boronic acid

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

Conditions
ConditionsYield
With sodium carbonate In water; ethyl acetate; isopropyl alcohol at 50℃; for 0.00138889h; Suzuki-Miyaura coupling; Microchannel flow reactor;99 %Chromat.
4-pentylaniline
33228-44-3

4-pentylaniline

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: hydrogenchloride; sodium nitrite / water / 0.25 h / 0 °C
1.2: 0.33 h / 20 °C
2.1: potassium carbonate; palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / water; 1,4-dioxane / 1 h / 100 °C / Inert atmosphere
View Scheme
4-bromophenyl dimethylcarbamate
7308-55-6

4-bromophenyl dimethylcarbamate

(4-pentylphenyl)boronic acid

(4-pentylphenyl)boronic acid

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: potassium phosphate; tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane / 18 h / 90 °C / Schlenk technique; Inert atmosphere
2: nickel dibromide; 1,2-bis-(dicyclohexylphosphino)ethane; zinc; potassium phosphate / toluene / 18 h / 150 °C / Inert atmosphere; Glovebox; Sealed tube
View Scheme
carbon dioxide
124-38-9

carbon dioxide

4-(4-pentylphenyl)bromobenzene
63619-59-0

4-(4-pentylphenyl)bromobenzene

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

Conditions
ConditionsYield
Stage #1: 4-(4-pentylphenyl)bromobenzene With copper(l) iodide; sodium iodide; N,N`-dimethylethylenediamine In 1,4-dioxane at 120℃; for 24h; Inert atmosphere; Sealed tube;
Stage #2: carbon dioxide With 1,4-diaza-bicyclo[2.2.2]octane; copper(I) oxide; phenylsilane; ammonia In 1,4-dioxane; 1-methyl-pyrrolidin-2-one at 130℃; under 2280.15 Torr; for 24h; Sealed tube;
56 %Chromat.
4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

4'-pentyl-1,1'-biphenyl-4-carbaldehyde
56741-21-0

4'-pentyl-1,1'-biphenyl-4-carbaldehyde

Conditions
ConditionsYield
With sulfuric acid; diisobutylaluminium hydride In water; ethyl acetate; toluene99.7%
With hydrogenchloride; diisobutylaluminium hydride In dichloromethane; water; ethyl acetate; toluene98%
With formic acid; aluminum nickel for 8h; Heating;2.5 g
With hydrogenchloride; water; tin(ll) chloride 1) Et2O, 24 h, RT; Yield given. Multistep reaction;
4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

4-(4-n-pentylphenyl)benzoic acid
59662-47-4

4-(4-n-pentylphenyl)benzoic acid

Conditions
ConditionsYield
With sulfuric acid In acetic acid at 120℃;88%
With potassium hydroxide In diethylene glycol at 100℃; for 12h; Saponification;66%
With sodium hydroxide In ethylene glycol
4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

platinum(II) chloride

platinum(II) chloride

trans-{PtCl2(4-pentyl-4'-cyanobiphenyl)2}
103517-45-9

trans-{PtCl2(4-pentyl-4'-cyanobiphenyl)2}

Conditions
ConditionsYield
In melt addn. of PtCl2 to melt of ligand (stirring, 30 min); cooling to room temp., dissolution in CHCl3, filtration (Celite), pptn. on Et2O addn., sepn. (centrifugation);75%
4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

trichloroacetonitrile
545-06-2

trichloroacetonitrile

2,4-bis(trichloromethyl)-6-(4'-pentylbiphenyl)-s-triazine

2,4-bis(trichloromethyl)-6-(4'-pentylbiphenyl)-s-triazine

Conditions
ConditionsYield
With hydrogenchloride; aluminum tri-bromide at 0 - 23℃; for 15h; Inert atmosphere;68%
4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

1-pentyl-4-phenylbenzene
7116-96-3

1-pentyl-4-phenylbenzene

Conditions
ConditionsYield
With tetraethylammonium perchlorate; triethylamine In dimethyl sulfoxide at 20℃; for 8h; Electrolysis; Green chemistry;62%
2-((trifluoromethyl)thio)isoindoline-1,3-dione
719-98-2

2-((trifluoromethyl)thio)isoindoline-1,3-dione

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

C19H18F3NS

C19H18F3NS

Conditions
ConditionsYield
With (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile; potassium carbonate In acetonitrile at 20℃; for 12h; Inert atmosphere; Irradiation;50%
1-bromo-butane
109-65-9

1-bromo-butane

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

1-(4'-Pentyl-biphenyl-4-yl)-pentan-1-one
80563-44-6

1-(4'-Pentyl-biphenyl-4-yl)-pentan-1-one

Conditions
ConditionsYield
With magnesium In tetrahydrofuran; diethyl ether for 5h; Heating; Yield given;
4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

dimethyl methane phosphonate
756-79-6

dimethyl methane phosphonate

A

2-(4'-n-pentyl-<1,1'-biphenyl>-4-yl)-1-(dimethoxyphosphinyl)-2-ethanone
94110-77-7

2-(4'-n-pentyl-<1,1'-biphenyl>-4-yl)-1-(dimethoxyphosphinyl)-2-ethanone

B

[2-Imino-2-(4'-pentyl-biphenyl-4-yl)-ethyl]-phosphonic acid dimethyl ester

[2-Imino-2-(4'-pentyl-biphenyl-4-yl)-ethyl]-phosphonic acid dimethyl ester

Conditions
ConditionsYield
With n-butyllithium; acetic acid Yield given. Multistep reaction. Yields of byproduct given;
4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

dimethyl methane phosphonate
756-79-6

dimethyl methane phosphonate

[2-Imino-2-(4'-pentyl-biphenyl-4-yl)-ethyl]-phosphonic acid dimethyl ester

[2-Imino-2-(4'-pentyl-biphenyl-4-yl)-ethyl]-phosphonic acid dimethyl ester

Conditions
ConditionsYield
With n-butyllithium 1.) THF, -78 deg C, 10 min, 2.) THF, a) -78 deg C, 10 min, b) RT, 1 h; Yield given. Multistep reaction;
2-Ethylhexyl acrylate
103-11-7

2-Ethylhexyl acrylate

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

polymer, Mw ca. 9.4E4 Da, Mn ca. 3.8E4 Da, Mw/Mn ca. 2.5; monomer(s): 2-ethylhexyl acrylate; 4-cyano-4\-n-pentylbiphenyl, 10 wt percent

polymer, Mw ca. 9.4E4 Da, Mn ca. 3.8E4 Da, Mw/Mn ca. 2.5; monomer(s): 2-ethylhexyl acrylate; 4-cyano-4\-n-pentylbiphenyl, 10 wt percent

Conditions
ConditionsYield
at 20℃; for 0.05h; UV-irradiation;
2-Ethylhexyl acrylate
103-11-7

2-Ethylhexyl acrylate

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

polymer, Mw ca. 9.2E4 Da, Mn ca. 3.5E4 Da, Mw/Mn ca. 2.7; monomer(s): 2-ethylhexyl acrylate; 4-cyano-4\-n-pentylbiphenyl, 20 wt percent

polymer, Mw ca. 9.2E4 Da, Mn ca. 3.5E4 Da, Mw/Mn ca. 2.7; monomer(s): 2-ethylhexyl acrylate; 4-cyano-4\-n-pentylbiphenyl, 20 wt percent

Conditions
ConditionsYield
at 20℃; for 0.05h; UV-irradiation;
2-Ethylhexyl acrylate
103-11-7

2-Ethylhexyl acrylate

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

polymer, Mw ca. 8.2E4 Da, Mn ca. 3.2E4 Da, Mw/Mn ca. 2.7; monomer(s): 2-ethylhexyl acrylate; 4-cyano-4\-n-pentylbiphenyl, 20 wt percent

polymer, Mw ca. 8.2E4 Da, Mn ca. 3.2E4 Da, Mw/Mn ca. 2.7; monomer(s): 2-ethylhexyl acrylate; 4-cyano-4\-n-pentylbiphenyl, 20 wt percent

Conditions
ConditionsYield
at 20℃; for 0.05h; UV-irradiation;
2-Ethylhexyl acrylate
103-11-7

2-Ethylhexyl acrylate

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

polymer, Mw ca. 8.8E4 Da, Mn ca. 3.3E4 Da, Mw/Mn ca. 2.8; monomer(s): 2-ethylhexyl acrylate; 4-cyano-4\-n-pentylbiphenyl, 30 wt percent

polymer, Mw ca. 8.8E4 Da, Mn ca. 3.3E4 Da, Mw/Mn ca. 2.8; monomer(s): 2-ethylhexyl acrylate; 4-cyano-4\-n-pentylbiphenyl, 30 wt percent

Conditions
ConditionsYield
at 20℃; for 0.05h; UV-irradiation;
2-Ethylhexyl acrylate
103-11-7

2-Ethylhexyl acrylate

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

polymer, Mw ca. 8.7E4 Da, Mn ca. 3.2E4 Da; monomer(s): 2-ethylhexyl acrylate; 4-cyano-4\-n-pentylbiphenyl, 40 wt percent

polymer, Mw ca. 8.7E4 Da, Mn ca. 3.2E4 Da; monomer(s): 2-ethylhexyl acrylate; 4-cyano-4\-n-pentylbiphenyl, 40 wt percent

Conditions
ConditionsYield
at 20℃; for 0.05h; UV-irradiation;
2-Ethylhexyl acrylate
103-11-7

2-Ethylhexyl acrylate

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

polymer, Mw ca. 8.2E4 Da, Mn ca. 3.5E4 Da, Mw/Mn ca. 2.4; monomer(s): 2-ethylhexyl acrylate; 4-cyano-4\-n-pentylbiphenyl, 40 wt percent

polymer, Mw ca. 8.2E4 Da, Mn ca. 3.5E4 Da, Mw/Mn ca. 2.4; monomer(s): 2-ethylhexyl acrylate; 4-cyano-4\-n-pentylbiphenyl, 40 wt percent

Conditions
ConditionsYield
at 20℃; for 0.05h; UV-irradiation;
2-Ethylhexyl acrylate
103-11-7

2-Ethylhexyl acrylate

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

polymer, Mw ca. 8.0E4 Da, Mn ca. 3.4E4 Da, Mw/Mn ca. 2.4; monomer(s): 2-ethylhexyl acrylate; 4-cyano-4\-n-pentylbiphenyl, 50 wt percent

polymer, Mw ca. 8.0E4 Da, Mn ca. 3.4E4 Da, Mw/Mn ca. 2.4; monomer(s): 2-ethylhexyl acrylate; 4-cyano-4\-n-pentylbiphenyl, 50 wt percent

Conditions
ConditionsYield
at 20℃; for 0.05h; UV-irradiation;
2-Ethylhexyl acrylate
103-11-7

2-Ethylhexyl acrylate

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

polymer, Mw ca. 7.8E4 Da, Mn ca. 3.3E4 Da; monomer(s): 2-ethylhexyl acrylate; 4-cyano-4\-n-pentylbiphenyl, 50 wt percent

polymer, Mw ca. 7.8E4 Da, Mn ca. 3.3E4 Da; monomer(s): 2-ethylhexyl acrylate; 4-cyano-4\-n-pentylbiphenyl, 50 wt percent

Conditions
ConditionsYield
at 20℃; for 0.05h; UV-irradiation;
2-Ethylhexyl acrylate
103-11-7

2-Ethylhexyl acrylate

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

polymer, Mw ca. 7.1E4 Da, Mn ca. 3.1E4 Da; monomer(s): 2-ethylhexyl acrylate; 4-cyano-4\-n-pentylbiphenyl, 60 wt percent

polymer, Mw ca. 7.1E4 Da, Mn ca. 3.1E4 Da; monomer(s): 2-ethylhexyl acrylate; 4-cyano-4\-n-pentylbiphenyl, 60 wt percent

Conditions
ConditionsYield
at 20℃; for 0.05h; UV-irradiation;
2-Ethylhexyl acrylate
103-11-7

2-Ethylhexyl acrylate

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

polymer, Mw ca. 6.5E4 Da, Mn ca. 2.8E4 Da, Mw/Mn ca. 2.35; monomer(s): 2-ethylhexyl acrylate; 4-cyano-4\-n-pentylbiphenyl, 60 wt percent

polymer, Mw ca. 6.5E4 Da, Mn ca. 2.8E4 Da, Mw/Mn ca. 2.35; monomer(s): 2-ethylhexyl acrylate; 4-cyano-4\-n-pentylbiphenyl, 60 wt percent

Conditions
ConditionsYield
at 20℃; for 0.05h; UV-irradiation;
2-Ethylhexyl acrylate
103-11-7

2-Ethylhexyl acrylate

4-cyano-4'-pentyl-1,1'-biphenyl
40817-08-1

4-cyano-4'-pentyl-1,1'-biphenyl

polymer, Mw ca. 6.1E4 Da, Mn ca. 2.5E4 Da, Mw/Mn ca. 2.4; monomer(s): 2-ethylhexyl acrylate; 4-cyano-4\-n-pentylbiphenyl, 70 wt percent

polymer, Mw ca. 6.1E4 Da, Mn ca. 2.5E4 Da, Mw/Mn ca. 2.4; monomer(s): 2-ethylhexyl acrylate; 4-cyano-4\-n-pentylbiphenyl, 70 wt percent

Conditions
ConditionsYield
at 20℃; for 0.05h; UV-irradiation;

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