As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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inquiry3,3,3-TRIFLUOROPROPIONYL CHLORIDE CAS:41463-83-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquirySuperiority We can customize and synthesize products that other suppliers may not be able to provide. Advantage cof, mof ligand manufacturer Product Detail bes
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
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inquirySuperior quality Appearance:Liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used as Pharmaceutical Intermediates Transportation:BY AIR Port
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates
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inquiry1. Product advantages? High purity, all above 98.5%, no impurities after dissolution? We will test each batch to ensure quality? OEM and private brand services designed for free? Various cap colors available? We can also provide MT1 peptide powder2.
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquirybest seller Application:API
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inquiryWe are committed to providing our customers with the best products and services at the most competitive prices.Appearance:off-white powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as prima
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inquiry3,3,3-TRIFLUOROPROPIONYL CHLORIDEAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:pharmaceutical intermediate Transportation:by air, by sea, by express
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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inquiryHangzhou ZeErRui Chemical Co., Ltd. is focused on customization, research and development and production of APIs and advanced intermediates, which can effectively compensate for the deficiencies of traditional CRO and CMO. Priority of high-tech barri
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inquiryWuhan Xinweiye Chemical Co., Ltd. is mainly engaged in the process development and production of customized synthesis and pharmaceutical intermediates. We have professional researchers in organic synthesis, analytical chemistry and production process
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3,3,3-Trifluoropropionic acid
3,3,3-trifluoropropanoyl chloride
Conditions | Yield |
---|---|
With phosphorus pentachloride at 65℃; Cooling with ice; | 99% |
With thionyl chloride; N,N-dimethyl-formamide at 70℃; for 4h; | 72% |
With Phthaloyl dichloride for 3h; Heating; | 69% |
3,3,3-trifluoropropanal
A
3,3,3-trifluoropropanoyl chloride
B
3,3,3-Trifluoropropionic acid
C
3,3,3-trifluoro-2-chloropropionyl chloride
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); chlorine In 2,4-dichloro-benzotrifluoride at 50℃; for 2.5h; Product distribution / selectivity; | A 62.5% B n/a C n/a |
3,3,3-trifluoropropanal
A
3,3,3-trifluoropropanoyl chloride
B
3,3,3-trifluoro-2-chloropropionaldehyde
Conditions | Yield |
---|---|
With trichloroisocyanuric acid In 2,4-dichloro-benzotrifluoride at 50℃; for 2.25h; Product distribution / selectivity; | A 51% B n/a |
3,3,3-trifluoropropanal
3,3,3-trifluoropropanoyl chloride
Conditions | Yield |
---|---|
With chlorine at 20℃; for 4h; Neat (no solvent); UV-irradiation; chemoselective reaction; | 39% |
3,3,3-trifluoropropanal
A
3,3,3-trifluoropropanoyl chloride
B
3,3,3-trifluoro-2-chloropropionaldehyde
C
3,3,3-trifluoro-2-chloropropionyl chloride
Conditions | Yield |
---|---|
With sulfuryl dichloride; dibenzoyl peroxide In water; 1,2-dichloro-benzene at 50℃; for 2.08333h; Product distribution / selectivity; |
3,3,3-trifluoropropanal
A
3,3,3-trifluoropropanoyl chloride
B
3,3,3-Trifluoropropionic acid
C
3,3,3-trifluoro-2-chloropropionaldehyde
D
3,3,3-trifluoro-2-chloropropionyl chloride
E
2,2-dichloro-3,3,3-trifluoro-propionaldehyde
Conditions | Yield |
---|---|
With chlorine at 50℃; for 4h; Product distribution / selectivity; | |
With sulfuryl dichloride; dibenzoyl peroxide In water at 50℃; for 2.08333h; Product distribution / selectivity; | |
With sulfuryl dichloride; 2,2'-azobis(isobutyronitrile) In 2,4-dichloro-benzotrifluoride at 50℃; for 2.08333h; Product distribution / selectivity; |
3,3,3-trifluoropropanal
A
3,3,3-trifluoropropanoyl chloride
B
3,3,3-Trifluoropropionic acid
C
3,3,3-trifluoro-2-chloropropionaldehyde
D
3,3,3-trifluoro-2-chloropropionyl chloride
Conditions | Yield |
---|---|
With sulfuryl dichloride; dibenzoyl peroxide In 2,4-dichloro-benzotrifluoride; water at 50℃; for 2.08333h; Product distribution / selectivity; | |
With sulfuryl dichloride; 2,2'-azobis(isobutyronitrile) In 2,4-dichloro-benzotrifluoride at 50 - 65℃; for 2h; Product distribution / selectivity; | |
With trichloroisocyanuric acid In acetonitrile at 50℃; for 4.08333h; Product distribution / selectivity; |
3,3,3-trifluoropropanal
A
3,3,3-trifluoropropanoyl chloride
B
3,3,3-trifluoro-2-chloropropionaldehyde
C
2,2-dichloro-3,3,3-trifluoro-propionaldehyde
Conditions | Yield |
---|---|
With sulfuryl dichloride; 2,2'-azobis(isobutyronitrile) In acetonitrile at 50℃; for 4.08333h; Product distribution / selectivity; |
3,3,3-trifluoropropanal
A
3,3,3-trifluoropropanoyl chloride
B
3,3,3-Trifluoropropionic acid
C
3,3,3-trifluoro-2-chloropropionaldehyde
D
2,2-dichloro-3,3,3-trifluoro-propionaldehyde
Conditions | Yield |
---|---|
With sulfuryl dichloride; 2,2'-azobis(isobutyronitrile) In acetonitrile at 50℃; for 4.08333h; Product distribution / selectivity; |
3,3,3-trifluoropropanal
A
3,3,3-trifluoropropanoyl chloride
B
3,3,3-Trifluoropropionic acid
C
3,3,3-trifluoro-2-chloropropionaldehyde
Conditions | Yield |
---|---|
With sulfuryl dichloride; 2,2'-azobis(isobutyronitrile) In toluene at 50℃; for 2.08333h; Product distribution / selectivity; |
3,3,3-trifluoropropanoyl chloride
Conditions | Yield |
---|---|
With sulfuric acid In acetonitrile at 50℃; for 2h; |
3,3,3-trifluoropropanoyl chloride
4-[4-(3-fluoro-2-methoxyphenyl)piperidin-1-yl]-2-hydrazinopyridine-3-carbonitrile
N'-{3-cyano-4-[4-(3-fluoro-2-methoxyphenyl)piperidin-1-yl]-pyridin-2-yl}-3,3,3-trifluoropropanehydrazide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; | 100% |
3,3,3-trifluoropropanoyl chloride
Conditions | Yield |
---|---|
With potassium carbonate In tetrahydrofuran at 60℃; for 3h; Reagent/catalyst; Solvent; Temperature; | 100% |
3,3,3-trifluoropropanoyl chloride
(3'-chloro-4-fluoro-4-phenyl-3,4,5,6-tetrahydro-2H-[1,4']bipyridinyl-2'-yl)hydrazine
N'-[3-chloro-4-(4-fluoro-4-phenylpiperidin-1-yl)pyridin-2-yl]-3,3,3-trifluoropropanohydrazide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 1h; | 99% |
3,3,3-trifluoropropanoyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; | 97% |
Conditions | Yield |
---|---|
With dmap In pyridine at 0 - 60℃; | 95.1% |
3,3,3-trifluoropropanoyl chloride
[3-chloro-4-(3,3-dimethyl-4-phenyl-piperazin-1-yl)-pyridin-2-yl]-hydrazine
N'-[3-chloro-4-(3,3-dimethyl-4-phenyl-piperazin-1-yl)pyridin-2-yl]-3,3,3-trifluoropropanohydrazide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 2h; | 92% |
3,3,3-trifluoropropanoyl chloride
4-aminotiophenol
S-4-(3,3,3-trifluoropropanamido)phenyl 3,3,3-trifluoropropanethioate
Conditions | Yield |
---|---|
With potassium carbonate In water; ethyl acetate at 0 - 20℃; | 87.2% |
3,3,3-trifluoropropanoyl chloride
4-chloro-5-(4-(2-fluoro-6-methoxyphenyl)piperidin-1-yl)-3-hydrazinylpyridazine
N-(4-chloro-5-(4-(2-fluoro-6-methoxyphenyl)piperidin-1-yl)pyridazin-3-yl)-3,3,3-trifluoropropanehydrazide
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In tetrahydrofuran; ethyl acetate at 20℃; for 16h; | 87% |
3,3,3-trifluoropropanoyl chloride
{3-chloro-4-[3-chloro-4-(tetrahydro-pyran-4-yloxy)-phenyl]-pyridin-2-yl}-hydrazine
N'-{3-chloro-4-[3-chloro-4-(tetrahydro-2H-pyran-4-yloxy)-phenyl]-pyridin-2-yl}-3,3,3-trifluoropropanohydrazide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 1h; | 86% |
3,3,3-trifluoropropanoyl chloride
N,N-dimethylammonium chloride
N,N-dimethyl-3,3,3-trifluoropropionamide
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In dichloromethane for 4h; | 86% |
Stage #1: N,N-dimethylammonium chloride With sodium hydrogencarbonate In dichloromethane Stage #2: 3,3,3-trifluoropropanoyl chloride In dichloromethane for 4h; | 86% |
N-((pyridin-2-yl)methyl)benzamide
3,3,3-trifluoropropanoyl chloride
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 3h; Green chemistry; | 86% |
3,3,3-trifluoropropanoyl chloride
3,3,3-trifluoro-2-chloropropionyl chloride
A
3,3,3-Trifluoropropionic acid
B
2-chloro-3,3,3-trifluoropropanoic acid
Conditions | Yield |
---|---|
With water at 50℃; for 4h; Product distribution / selectivity; | A 84.5% B n/a |
methanol
3,3,3-trifluoropropanoyl chloride
methyl 3,3,3-trifluoropropionate
Conditions | Yield |
---|---|
at 50℃; for 2h; Inert atmosphere; | 80% |
In N,N-dimethyl-formamide at 50℃; for 1h; | 7.5 g |
3,3,3-trifluoropropanoyl chloride
Conditions | Yield |
---|---|
With pyridine In tetrahydrofuran at 20℃; for 2h; | 80% |
3,3,3-trifluoropropanoyl chloride
5-morpholino-2,4-dinitroaniline
Conditions | Yield |
---|---|
With pyridine at 20℃; for 0.0833333h; | 80% |
2-(acetylamino)ethanethiol
3,3,3-trifluoropropanoyl chloride
S-(3,3,3-trifluoropropionyl)-N-acetylcysteamine
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; Inert atmosphere; | 79.5% |
3,3,3-trifluoropropanoyl chloride
cyanoacetic acid
5,5,5-trifluoro-3-oxopentanenitrile
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; n-butyllithium In tetrahydrofuran; hexane at -78 - -10℃; for 3h; | 77% |
3,3,3-trifluoropropanoyl chloride
tert-butyl alcohol
tert-butyl 3,3,3-trifluoropropanoate
Conditions | Yield |
---|---|
With N,N-diethylaniline In diethyl ether at 50℃; for 8h; Inert atmosphere; | 76% |
5-amino-2,4-bis(benzyloxy)-6-[2,3,4,5-tetrakis-(O-tert-butyldimethylsilanyl)ribitylamino]pyrimidine
3,3,3-trifluoropropanoyl chloride
N-(2,4-bis(benzyloxy)-6-((2S,3S,4R)-2,3,4,5-tetrakis(tert-butyldimethylsilyloxy)pentylamino)pyrimidin-5-yl)-3,3,3-trifluoropropanamide
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 0℃; for 0.5h; | 75% |
3,3,3-trifluoropropanoyl chloride
Conditions | Yield |
---|---|
With pyridine; dmap In tetrahydrofuran at 70℃; for 16h; Inert atmosphere; | 75% |
3,3,3-trifluoropropanoyl chloride
Bis(trimethylsilyl)ethyne
Conditions | Yield |
---|---|
With aluminum (III) chloride In dichloromethane at 0℃; for 1h; | 75% |
With aluminum (III) chloride In dichloromethane at 0℃; for 1h; | 75% |
potassium[manganese(pentacarbonyl)]
3,3,3-trifluoropropanoyl chloride
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 3h; Inert atmosphere; | 75% |
3,3,3-trifluoropropanoyl chloride
4-chloro-5-(4-(2-fluorophenyl)piperidin-1-yl)-3-hydrazinylpyridazine
N'-(4-chloro-5-(4-(2-fluorophenyl)piperidin-1-yl)pyridazin-3-yl)-3,3,3-trifluoropropanehydrazide
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In tetrahydrofuran; ethyl acetate at 20℃; for 16h; | 74% |
cycl-isopropylidene malonate
3,3,3-trifluoropropanoyl chloride
C9H9F3O5
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0℃; for 2h; Inert atmosphere; | 72.5% |
2-(N-methylamino)pyridine
3,3,3-trifluoropropanoyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 2h; | 72% |
3,3,3-trifluoropropanoyl chloride
N-(((1S,2S)-2-(4-fluorophenyl)cyclopropyl)methyl)-2-hydrazinyl-3-(trifluoromethyl)pyridin-4-amine
3,3,3-trifluoro-N'-(4-((((1S,2S)-2-(4-fluorophenyl)cyclopropyl)methyl)amino)-3-(trifluoromethyl)pyridin-2-yl)propanehydrazide
Conditions | Yield |
---|---|
With sodium carbonate In tetrahydrofuran; water; ethyl acetate for 0.166667h; | 71.6% |
3,3,3-trifluoropropanoyl chloride
3,3,3-Trifluoropropionic acid
Conditions | Yield |
---|---|
With water at 50℃; for 5h; Product distribution / selectivity; | 70.5% |
3,3,3-trifluoropropanoyl chloride
5-[4-(azetidin-3-yloxy)-3-methoxyphenyl]-2-(4-chlorophenyl)-6,7-dihydro-5H-thiazolo[5,4-c]pyridin-4-one
Conditions | Yield |
---|---|
With pyridine; dmap | 70% |
3,3,3-trifluoropropanoyl chloride
benzyl alcohol
benzyl 3,3,3-trifluoropropanoate
Conditions | Yield |
---|---|
In dichloromethane at 60℃; for 3h; | 70% |
at 50℃; for 2h; Inert atmosphere; |
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