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Cas:42245-42-1
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inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
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inquiryMethyl 3-(4-methoxyphenyl)oxirane-2-carboxylate cas 42245-42-1Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
Cas:42245-42-1
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Cas:42245-42-1
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inquiryFINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the Methyl 3-(4-methoxyphenyl)oxirane-2-carboxylate, CAS:42245-42-1 with the most competi
Cas:42245-42-1
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inquiry2-Oxiranecarboxylicacid, 3-(4-methoxyphenyl)-, methyl ester Storage:keep in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/pharma intermediate Transportation:By Sea,by Air,By courier like DHL or Fed
Cas:42245-42-1
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inquiry4-methoxy-benzaldehyde
methyl chloroacetate
methyl 3-(4-methoxyphenyl)glycidate
Conditions | Yield |
---|---|
With sodium methylate In ethanol at 5 - 35℃; for 2h; | 88.4% |
With sodium methylate In methanol 1) -10 deg C, 1.5 h; 2) -5 deg C, 1 h; 3) room temperature, 3 h; | 70% |
Stage #1: methyl chloroacetate With sodium methylate In methanol for 0.0833333h; Cooling with ice; Stage #2: 4-methoxy-benzaldehyde In methanol at 0℃; | 41% |
3-(4-methoxy-phenyl)acrylic acid methyl ester
A
methyl 3-(4-methoxyphenyl)glycidate
Conditions | Yield |
---|---|
With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid In dichloromethane; water for 1.5h; Ambient temperature; |
3-(4-methoxy-phenyl)acrylic acid methyl ester
3-chloro-benzenecarboperoxoic acid
A
methyl 3-(4-methoxyphenyl)glycidate
Conditions | Yield |
---|---|
In dichloromethane for 1.5h; Ambient temperature; |
(E)-3-(4-methoxyphenyl)acrylic acid
methyl 3-(4-methoxyphenyl)glycidate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: H2SO4 2: m-chloroperbenzoic acid, sodium bicarbonate / CH2Cl2; H2O / 1.5 h / Ambient temperature View Scheme | |
Multi-step reaction with 2 steps 1: H2SO4 2: CH2Cl2 / 1.5 h / Ambient temperature View Scheme |
4-methoxy-benzaldehyde
methyl 3-(4-methoxyphenyl)glycidate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 2: H2SO4 3: m-chloroperbenzoic acid, sodium bicarbonate / CH2Cl2; H2O / 1.5 h / Ambient temperature View Scheme | |
Multi-step reaction with 3 steps 2: H2SO4 3: CH2Cl2 / 1.5 h / Ambient temperature View Scheme |
methyl 3-(4-methoxyphenyl)glycidate
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol for 3h; Ambient temperature; | 95.4% |
methyl 3-(4-methoxyphenyl)glycidate
N-methyl-2-(2-(2-(4-phenyl-1-piperidyl)ethoxy)phenyl)thiazolidine-3-carbothioamide oxalate
N-methyl-2-{2-[2-(4-phenylpiperidine-1-yl)ethyloxy]phenyl}thiazolidine-3-carboxamide
Conditions | Yield |
---|---|
In ethanol | 82.3% |
methyl 3-(4-methoxyphenyl)glycidate
Conditions | Yield |
---|---|
Stage #1: methyl 3-(4-methoxyphenyl)glycidate With samarium diiodide In tetrahydrofuran at 20℃; for 2h; Stage #2: With water-d2 In tetrahydrofuran at 20℃; for 12h; Further stages.; | 81% |
methyl 3-(4-methoxyphenyl)glycidate
3-(4-methoxy-phenyl)acrylic acid methyl ester
Conditions | Yield |
---|---|
With samarium diiodide In tetrahydrofuran at 20℃; for 1.5h; | 79% |
methyl 3-(4-methoxyphenyl)glycidate
(N)-methyl-2-(2-(2-(4-phenylpiperazino)ethoxy)phenyl)thiazolidine-3-thiocarboxamide
N-methyl-2-{2-[2-(4-phenylpiperazin-1-yl)ethyloxy]phenyl}thiazolidine-3-carboxamide
Conditions | Yield |
---|---|
In ethanol | 75.7% |
2-amino-5-chlorobenzenethiol
methyl 3-(4-methoxyphenyl)glycidate
Conditions | Yield |
---|---|
In di-isopropyl ether; toluene | 68% |
In di-isopropyl ether; toluene | 68% |
In toluene |
methyl 3-(4-methoxyphenyl)glycidate
2-amino-5-methoxy-thiophenol
threo-2-hydroxy-3-<(2-amino-5-methoxyphenyl)thio>-3-(4-methoxyphenyl)propionic acid methyl ester
Conditions | Yield |
---|---|
In toluene for 6h; Heating; | 63% |
methyl 3-(4-methoxyphenyl)glycidate
4-methoxy-phenol
2-hydroxy-3-(4-methoxy-phenoxy)-3-(4-methoxy-phenyl)propionic acid methyl ester
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride; silver nitrate In isopropyl alcohol at 60 - 80℃; for 8.5h; | 61% |
methyl 3-(4-methoxyphenyl)glycidate
2-(4-methoxy-benzyl)-3,4-dimethyl-piperidin-4-ol
Conditions | Yield |
---|---|
With hydrogenchloride In water at 85 - 90℃; for 36h; | 57.1% |
2-butyl ethyl ether
methyl 3-(4-methoxyphenyl)glycidate
2-nitrothiophenol
methyl 2-hydroxy-3-(4-methoxyphenyl)-3-(2-nitrophenylthio)propionate
Conditions | Yield |
---|---|
With trifluoroborane diethyl ether | 51.3% |
methyl 3-(4-methoxyphenyl)glycidate
methyl 2-hydroxy-3-(4-methoxyphenyl)-3-(2-nitrophenylthio)propionate
Conditions | Yield |
---|---|
In ethyl acetate; benzene | 47.1% |
methyl 3-(4-methoxyphenyl)glycidate
2-(4-methoxy-benzyl)-3,4-dimethyl-piperidin-4-ol
Conditions | Yield |
---|---|
With water; sodium hydroxide at 90 - 95℃; for 48h; pH=6 - 7; | 45% |
Conditions | Yield |
---|---|
With aluminum (III) chloride In chloroform at 20℃; for 0.5h; Reagent/catalyst; | A 38% B 32% |
With tris(p-bromophenylammoniumyl) hexachloroantimonate In dichloromethane at 20℃; for 0.5h; Reagent/catalyst; Solvent; chemoselective reaction; | A 20 %Spectr. B 72 %Spectr. |
methyl 3-(4-methoxyphenyl)glycidate
triphenylborane
Conditions | Yield |
---|---|
In tetrahydrofuran; N,N-dimethyl-formamide at 20℃; for 2h; | A n/a B 20% |
methyl 3-(4-methoxyphenyl)glycidate
2-(cyclopent-1-en-1-yl) ethan-1-amine
1-(4-methoxy-benzyl)-octahydro-[2]pyrindin-4a-ol
Conditions | Yield |
---|---|
With hydrogenchloride |
methyl 3-(4-methoxyphenyl)glycidate
2-(cyclohept-1-en-1-yl)ethan-1-amine
1-(4-methoxy-benzyl)-decahydro-cyclohepta[c]pyridin-4a-ol
Conditions | Yield |
---|---|
With hydrogenchloride |
methyl 3-(4-methoxyphenyl)glycidate
2-(1-cyclohexenyl)ethylamine
1-(4-methoxy-benzyl)-octahydro-isoquinolin-4a-ol
Conditions | Yield |
---|---|
With hydrogenchloride |
methyl 3-(4-methoxyphenyl)glycidate
2-(methylamino)benzenethiol
2-Hydroxy-3-(4-methoxy-phenyl)-3-(2-methylamino-phenylsulfanyl)-propionic acid methyl ester
methyl 3-(4-methoxyphenyl)glycidate
2-(2-diethylamino-ethylamino)-benzenethiol
4-(2-diethylamino-ethyl)-4H-benzo[1,4]thiazin-3-one
Conditions | Yield |
---|---|
at 130 - 140℃; for 3h; |
methyl 3-(4-methoxyphenyl)glycidate
2-(2-diethylamino-ethylamino)-benzenethiol
3-[2-(2-Diethylamino-ethylamino)-phenylsulfanyl]-2-hydroxy-3-(4-methoxy-phenyl)-propionic acid methyl ester
methyl 3-(4-methoxyphenyl)glycidate
4-Methoxyphenylacetaldehyde
Conditions | Yield |
---|---|
With sodium methylate; acetic acid 1.) CH3OH, benzene, 0-5 deg C, 2.) reflux, 3 h; Multistep reaction; | |
With sodium methylate; acetic acid 1) methanol, ether, water, 5 deg C, 3 h; 2) benzene, reflux, 3 h; Yield given. Multistep reaction; | |
Multi-step reaction with 2 steps 1: potassium hydroxide / water / 5 h / 15 - 20 °C 2: potassium dihydrogenphosphate / water; dichloromethane / 5 h View Scheme | |
Multi-step reaction with 2 steps 1: potassium hydroxide / ethanol / 8 h / 0 - 15 °C 2: potassium dihydrogenphosphate / dichloromethane; water / 4 h / 20 °C View Scheme |
methyl 3-(4-methoxyphenyl)glycidate
A
methyl (2R,3S)-3-(4-methoxyphenyl)glycidate
B
(2S,3R)-trans-(4-methoxyphenyl)glycidic acid
Conditions | Yield |
---|---|
With water In acetone at 25℃; Rhizopus arrhizus mycelium lipase, pH 7; |
methyl 3-(4-methoxyphenyl)glycidate
methyl (2R,3S)-3-(4-methoxyphenyl)glycidate
methyl 3-(4-methoxyphenyl)glycidate
2-nitrothiophenol
methyl 2-hydroxy-3-(4-methoxyphenyl)-3-(2-nitrophenylthio)propionate
Conditions | Yield |
---|---|
In acetonitrile |
methyl 3-(4-methoxyphenyl)glycidate
4-chloro-2-nitro-thiophenol
3-(4-Chloro-2-nitro-phenylsulfanyl)-2-hydroxy-3-(4-methoxy-phenyl)-propionic acid methyl ester
Conditions | Yield |
---|---|
In acetonitrile |
methyl 3-(4-methoxyphenyl)glycidate
2-amino-benzenethiol
(2RS,3RS)-3-(2'-aminophenylthio)-2-hydroxy-3-(4''-methoxyphenyl)-propionic acid methyl ester
methyl 3-(4-methoxyphenyl)glycidate
methyl 2-hydroxy-3-(4-methoxyphenyl)acrylate
Conditions | Yield |
---|---|
zinc(II) perchlorate In toluene Heating; |
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