Name: 2-Amino-5-chlorobenzonitrile Application:2-Amino-5-chlorobenzonitrile
Cas:5922-60-1
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inquiryDayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:5922-60-1
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryItems Standard Result Assay 98%min ----------------------------------------------------------------------------------------------
Cas:5922-60-1
Min.Order:1 Gram
FOB Price: $100.0 / 500.0
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inquiryhe company has advanced technology, as well as a large number of excellent R & D team, to provide customers from the grams to one hundred kilograms and tons of high-quality products, competitive prices and quality se T rvice Appearance:White or
Cas:5922-60-1
Min.Order:1 Kilogram
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inquiryHigh quality. Factory supply. In stock. Best price.1.Quick response within 24 hours;2.Best quality in your requirement;?3.We pay more attention on delivery time, and usually ship on time;4.Under the premise of safety and effectiveness, we can produce
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Cas:5922-60-1
Min.Order:5 Kiloliter
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Type:Manufacturers
inquiry2-Amino-5-chlorobenzonitrile Basic information Product Name: 2-Amino-5-chlorobenzonitrile Synonyms: 5-CHLOROANTHRANILONITRILE;AMINO(2-) 5-CHLORO-BENZONITRILE;ACBN;2-AMINO-5-CHLOROBENZONI
WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:5922-60-1
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryWe are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED
Cas:5922-60-1
Min.Order:1 Gram
FOB Price: $3.0
Type:Lab/Research institutions
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:5922-60-1
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryEnglish name: 2-Amino-5-chlorobenzonitrile CAS: 5922-60-1 EINECS: 227-651-5 Assay,% ≥98.0% Appearance: white to light beige crystalline needles
Cas:5922-60-1
Min.Order:1 Gram
FOB Price: $1.0 / 10.0
Type:Trading Company
inquiry2-Amino-5-chlorobenzonitrile CAS:5922-60-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organ
Cas:5922-60-1
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
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Cas:5922-60-1
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:5922-60-1
Min.Order:0 Metric Ton
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Type:Other
inquiryChemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff
Cas:5922-60-1
Min.Order:100 Gram
Negotiable
Type:Other
inquirylow price high quality high purity good sevice stock Appearance:white Storage:Preserve In Well-Closed, Light-Resistant and Tight Containers. Store In Cool & Dry Place Package:1g,5g,10g...1kg,5kg...more Application:Pharmaceutical interme
Cas:5922-60-1
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:5922-60-1
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquirySuperior quality, moderate price & quick delivery. Appearance:white crystals Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:For medicine , pesticide intermed
Cas:5922-60-1
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiry2-Amino-5-chlorobenzonitrile Chemical Properties Melting point 96-99 °C (lit.) Boiling point 132-135 °C/0.5 mmHg (lit.) density 1.2763 (rough estimate) refractive index 1.5500 (estimate) Fp >230 °F pka 1.18&plusm
Cas:5922-60-1
Min.Order:1 Gram
FOB Price: $66.0
Type:Lab/Research institutions
inquiry2-Amino-5-Chlorobenzonitrile CAS 5922-60-1 High Quality Prompt Delivery Free Sample Production Information CAS Number: 5922-60-1 Name: Benzonitrile, …Appearance:white to light beige crystalline needles Storage:Room Temperature Package:25kg/Bag Appli
1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:5922-60-1
Min.Order:1 Metric Ton
FOB Price: $7.0 / 8.0
Type:Trading Company
inquiryGOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api
Cas:5922-60-1
Min.Order:1 Kilogram
FOB Price: $10.0
Type:Lab/Research institutions
inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:5922-60-1
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiry2-Amino-5-chlorobenzonitrileAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
Cas:5922-60-1
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryJinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Cas:5922-60-1
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryOur clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Conditions | Yield |
---|---|
With N-chloro-succinimide; isopropyl alcohol for 0.25h; Chlorination; Heating; | 89% |
With N-chloro-succinimide In acetonitrile for 1.5h; Heating; | 71% |
Conditions | Yield |
---|---|
In 1-methyl-pyrrolidin-2-one at 140℃; for 5h; | 80% |
2-amino-5-chlorobenzonitrile
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride In ethanol; water at 120℃; for 0.5h; Microwave irradiation; | 76% |
Conditions | Yield |
---|---|
With phosphorus pentaoxide for 0.5h; | 63% |
5-chloro-2-(4-chloro-5H-1,2,3-dithiazol-5-ylideneamino)benzonitrile
A
3-amino-5-chloroindole-2-carbonitrile
B
2-amino-5-chlorobenzonitrile
Conditions | Yield |
---|---|
With water; triphenylphosphine In dichloromethane at 20℃; | A 32% B 27% |
methylmagnesium bromide
2-azido-5-chlorobenzonitrile
A
6-chloro-3,4-dihydro-4-imino-3-methyl-1,2,3-benzotriazine
B
2-amino-5-chlorobenzonitrile
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 1h; | A 31% B 29% |
5-Chloroisatin 3-oxime
2-amino-5-chlorobenzonitrile
Conditions | Yield |
---|---|
at 250℃; |
3-chloro-6-nitrobenzonitrile
2-amino-5-chlorobenzonitrile
Conditions | Yield |
---|---|
With tin(ll) chloride Yield given; | |
With titanium(III) chloride In water; acetone for 0.5h; | |
With hydrogen In neat (no solvent) at 110℃; under 15001.5 Torr; for 15h; chemoselective reaction; |
Conditions | Yield |
---|---|
With boron trichloride; tin(IV) chloride; potassium carbonate 1.) C6H6, reflux, 6 h, 2.) CH3OH, reflux, 2.5 h,; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With pyridine |
N-(4-Chloro-2-cyanophenyl)-2,2,2-trifluoroacetamide
2-amino-5-chlorobenzonitrile
Conditions | Yield |
---|---|
With potassium carbonate In methanol at 20℃; for 12h; |
p-chloro-o-iodoaniline
2-amino-5-chlorobenzonitrile
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: dimethylformamide / 0.5 h / 20 °C 2: dimethylformamide / 0.5 h / 100 °C 3: aq. K2CO3 / methanol / 12 h / 20 °C View Scheme |
2,2,2-trifluoro-N-(2-iodo-4-chlorophenyl)acetamide
2-amino-5-chlorobenzonitrile
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dimethylformamide / 0.5 h / 100 °C 2: aq. K2CO3 / methanol / 12 h / 20 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 35 percent / sulfuryl chloride; hydrochloric acid / diethyl ether / 1.5 h / 60 - 70 °C 2: 37 percent / thionyl chloride / 0.5 h / Heating 3: 68 percent / liq. ammonia / 0.5 h / 0 °C 4: 63 percent / phosphorus pentoxide / 0.5 h View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 37 percent / thionyl chloride / 0.5 h / Heating 2: 68 percent / liq. ammonia / 0.5 h / 0 °C 3: 63 percent / phosphorus pentoxide / 0.5 h View Scheme |
2-amino-5-chlorobenzoic chloride
2-amino-5-chlorobenzonitrile
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 68 percent / liq. ammonia / 0.5 h / 0 °C 2: 63 percent / phosphorus pentoxide / 0.5 h View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 1.) SOCl2; 2.) NH4OH / 1.) PhMe, reflux 2: SOCl2 / Heating 3: 15 percent TiCl3 / acetone; H2O / 0.5 h View Scheme |
2-nitro-5-chlorobenzamide
2-amino-5-chlorobenzonitrile
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: SOCl2 / Heating 2: 15 percent TiCl3 / acetone; H2O / 0.5 h View Scheme |
5-chloro-2-nitrobenzaldehyde oxime
2-amino-5-chlorobenzonitrile
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 80 percent / PCl5 2: SnCl2 View Scheme |
Conditions | Yield |
---|---|
With N-chloro-succinimide In acetonitrile |
carbon dioxide
2-amino-5-chlorobenzonitrile
6-chloro-1,2,3,4-tetrahydroquinazoline-2,4-dione
Conditions | Yield |
---|---|
With bicarbonate salt of 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide at 80℃; under 750.075 Torr; for 4h; Inert atmosphere; | 100% |
With potassium carbonate; 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride In dimethyl sulfoxide at 120℃; under 750.075 Torr; for 8h; High pressure; Autoclave; | 99% |
With tetrabutyl ammonium fluoride In dimethyl sulfoxide at 110℃; under 15001.5 Torr; for 24h; Autoclave; | 99% |
2-amino-5-chlorobenzonitrile
4-Methoxybenzyl alcohol
5-chloro-2-(4-methoxy-benzylamino)-benzonitrile
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In acetonitrile at 70℃; for 12h; | 99% |
2-amino-5-chlorobenzonitrile
2,4-diamino-6-chloroquinazoline
Conditions | Yield |
---|---|
Stage #1: chloro-formamidine hydrochloride; 2-amino-5-chlorobenzonitrile In sulfolane; dimethylsulfone at 165℃; for 0.5h; Stage #2: With ammonia; water In sulfolane; dimethylsulfone pH=7 - 8; | 99% |
Stage #1: chloro-formamidine hydrochloride; 2-amino-5-chlorobenzonitrile In sulfolane; dimethylsulfone at 165℃; for 0.5h; Stage #2: With ammonia; water In sulfolane; dimethylsulfone pH=7 - 8; | 99% |
2-amino-5-chlorobenzonitrile
2-azido-5-chlorobenzonitrile
Conditions | Yield |
---|---|
With tert.-butylnitrite; trimethylsilylazide In acetonitrile at 20℃; for 2h; | 97% |
Stage #1: 2-amino-5-chlorobenzonitrile With hydrogenchloride; sodium nitrite In water at 0 - 5℃; for 0.5h; Stage #2: With sodium azide; sodium acetate In water at 0 - 5℃; for 0.5h; | 72% |
With hydrogenchloride; sodium azide; sodium acetate; sodium nitrite 1.) water, 0-5 deg C, 10 min; 2.) water, 0-5 deg C, 0.5 h; Multistep reaction; |
2-amino-5-chlorobenzonitrile
methyl chloroformate
5-chloro-2-<(methoxycarbonyl)amino>benzonitrile
Conditions | Yield |
---|---|
With sodium hydrogencarbonate Reflux; | 97% |
With sodium hydrogencarbonate In butanone Reflux; | 97% |
With sodium hydrogencarbonate In butanone Reflux; | 97% |
With sodium hydrogencarbonate In butanone at 80℃; for 18h; | 76% |
With dmap In N,N-dimethyl acetamide at 10 - 90℃; |
Conditions | Yield |
---|---|
With silica-gel-supported sulfuric acid In toluene for 2.5h; Inert atmosphere; Reflux; | 97% |
With water; potassium carbonate In water at 150℃; for 0.5h; Microwave irradiation; | 89% |
With potassium hydroxide; ethanol Heating / reflux; |
2-amino-5-chlorobenzonitrile
Triethyl orthopropionate
ethyl N-(4-chloro-2-cyanophenyl)propanimidate
Conditions | Yield |
---|---|
With trifluoroacetic acid | 97% |
2-amino-5-chlorobenzonitrile
2-(aminomethyl)-4-chloroaniline
Conditions | Yield |
---|---|
With borane-THF In tetrahydrofuran at 0 - 20℃; for 24.17h; Inert atmosphere; | 96% |
With borane-THF In tetrahydrofuran at 0 - 20℃; for 24.1667h; Inert atmosphere; | 50% |
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃; for 18h; |
2-amino-5-chlorobenzonitrile
phenylboronic acid
2-Amino-5-chlorobenzophenone
Conditions | Yield |
---|---|
With 5,5'-dimethyl-2,2'-bipyridine; methanesulfonic acid; palladium(II) trifluoroacetate; water In 2-methyltetrahydrofuran at 80℃; for 36h; Schlenk technique; | 96% |
With [2,2]bipyridinyl; methanesulfonic acid; palladium(II) trifluoroacetate In tetrahydrofuran; water at 80℃; for 36h; |
2-amino-5-chlorobenzonitrile
2-amino-5-chlorobenzothioamide
Conditions | Yield |
---|---|
With sodium hydrogen sulfide monohydrate; magnesium chloride In N,N-dimethyl-formamide at 20℃; for 72h; Sealed tube; | 96% |
Conditions | Yield |
---|---|
With 5,5'-dimethyl-2,2'-bipyridine; methanesulfonic acid; palladium(II) trifluoroacetate In 2-methyltetrahydrofuran; water at 80℃; for 12h; Reagent/catalyst; Temperature; Sealed tube; Inert atmosphere; Cooling with ice; | 96% |
2-amino-5-chlorobenzonitrile
N,N-dimethyl-formamide
6-chloro-1,2,3,4-tetrahydroquinazoline-2,4-dione
Conditions | Yield |
---|---|
With carbon dioxide In water at 150℃; under 37503.8 Torr; for 5h; | 95.6% |
2-amino-5-chlorobenzonitrile
formamide
4-amino-6-chloroquinazoline
Conditions | Yield |
---|---|
Stage #1: 2-amino-5-chlorobenzonitrile; formamide at 180℃; for 6h; Stage #2: With water | 95% |
at 180℃; for 6h; | 95% |
2-amino-5-chlorobenzonitrile
benzoyl chloride
N-(4-chloro-2-cyanophenyl)benzonitrile
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 20℃; for 3h; | 94% |
Conditions | Yield |
---|---|
With C7H14OS2*C9H16N2 In neat (no solvent) at 40℃; for 18h; Green chemistry; | 94% |
ortho-bromophenylacetic acid
2-amino-5-chlorobenzonitrile
Conditions | Yield |
---|---|
Stage #1: ortho-bromophenylacetic acid With thionyl chloride In dichloromethane for 4h; Reflux; Stage #2: 2-amino-5-chlorobenzonitrile In toluene for 16h; Reflux; | 94% |
Conditions | Yield |
---|---|
Stage #1: 2-amino-5-chlorobenzonitrile; cycloheptanone With aluminum (III) chloride at 150℃; for 0.166667h; Microwave irradiation; Stage #2: With hydrogenchloride In methanol; water at 20℃; | 94% |
2-amino-5-chlorobenzonitrile
chloroformic acid ethyl ester
(2-cyano-4-chloro-phenyl)-carbamic acid ethyl ester
Conditions | Yield |
---|---|
for 6h; Reflux; | 93% |
at 93℃; for 18h; | 85% |
for 6h; Reflux; | 68% |
for 6h; Heating; | |
Reflux; |
2-amino-5-chlorobenzonitrile
Benzyldithiophosphonsaeureanhydrid
Conditions | Yield |
---|---|
In toluene at 90℃; for 3h; | 92% |
2-amino-5-chlorobenzonitrile
A
(2-amino-5-chlorophenyl)-phenyl-methane-imine
B
phenylmagnesium bromide
Conditions | Yield |
---|---|
A 92% B n/a |
1,1,1-trimethoxybutane
2-amino-5-chlorobenzonitrile
methyl N-(4-chloro-2-cyanophenyl)butanimidate
Conditions | Yield |
---|---|
With trifluoroacetic acid | 92% |
2-amino-5-chlorobenzonitrile
2-amino-3-bromo-5-chlorobenzonitrile
Conditions | Yield |
---|---|
With bromine; sodium bromide In water at 25℃; for 0.5h; | 92% |
With bromine In acetic acid at 50℃; |
2-amino-5-chlorobenzonitrile
sodium benzenesulfonate
2-Amino-5-chlorobenzophenone
Conditions | Yield |
---|---|
With p-nitrobenzenesulfonic acid; palladium diacetate In tetrahydrofuran; water at 80℃; for 48h; Inert atmosphere; Schlenk technique; | 92% |
2-amino-5-chlorobenzonitrile
4-methylphenylboronic acid
Triethyl orthoacetate
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; palladium diacetate; acetic acid In N,N-dimethyl-formamide at 100℃; for 12h; | 91% |
2-amino-5-chlorobenzonitrile
5-<4-(trifluoromethyl)phenyl>-1,3-cyclohexanedione
5-chloro-2-<<5-<4-(trifluoromethyl)phenyl>-3-oxo-1-cyclohexenyl>amino>benzonitrile
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene for 8h; Heating; | 90.58% |
bis(trichloromethyl) carbonate
2-amino-5-chlorobenzonitrile
2,4,6-trichloroquinazoline
Conditions | Yield |
---|---|
Stage #1: bis(trichloromethyl) carbonate With triethylamine; Triphenylphosphine oxide In chlorobenzene at 20℃; for 0.5h; Cooling with ice; Stage #2: 2-amino-5-chlorobenzonitrile In chlorobenzene at 120℃; for 8h; | 90.3% |
Conditions | Yield |
---|---|
at 70 - 75℃; for 2h; | 90% |
In methanol for 6h; Reflux; |
N,4-dimethyl-N-(phenylethynyl)benzenesulfonamide
2-amino-5-chlorobenzonitrile
Conditions | Yield |
---|---|
With [bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold(I) In 1,4-dioxane at 80℃; for 7h; Schlenk technique; regioselective reaction; | 90% |
Ethyldithioxo-λ5-phosphoran
2-amino-5-chlorobenzonitrile
Conditions | Yield |
---|---|
In toluene at 90℃; for 3h; | 89% |
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