As a leading and professional manufacturer of APIs and API intermediates in China,Anhui Dexinjia Biopharm Co., Ltd founded in 2006, Except for the R&D center, our company has built a close cooperation relation with Chinese Academy of Sciences, T
Cas:626-05-1
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inquiryProduct Description Product website: http://www.finerchem.com Product Name 2,6-Dibromopyridine CAS No. 626-0
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inquiryHigh quality 2,6-Dibromopyridine CAS 626-05-1 with factory price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed addi
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Cas:626-05-1
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inquiryName: 2,6-Dibromo pyridine Molecular Formula:C5H3Br2N Molecular Weight:236.9 CAS No.:626-05-1 Appearance:Similar White To Slight Yellow Crystal Appearance:Similar White To Slight Yellow Crystal Storage:Store in cool and dry place, away from sun l
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Min.Order:1 Gram
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2,6-dibromopyridin N-oxide
2,6-Dibromopyridine
Conditions | Yield |
---|---|
With carbon tetrabromide; lithium tert-butoxide In m-xylene at 100℃; for 1h; Inert atmosphere; | 30% |
Conditions | Yield |
---|---|
With bromine at 500℃; Leiten ueber Bimsstein; | |
With bromine at 500℃; Leiten ueber Glas; |
Conditions | Yield |
---|---|
With acetic acid |
Conditions | Yield |
---|---|
With bromine at 300℃; Leiten ueber mit Kupfer(I)-bromid impraegnierten Bimsstein; |
2,6-Dibromopyridine
Conditions | Yield |
---|---|
at 226℃; |
2,6-dibromo-3-aminopyridine
2,6-Dibromopyridine
Conditions | Yield |
---|---|
With ethanol; sulfuric acid anschliessend Behandeln mit wss. Natriumnitrit-Loesung; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: methanol; bromine 2: ethanol; concentrated sulfuric acid / anschliessend Behandeln mit wss. Natriumnitrit-Loesung View Scheme |
Conditions | Yield |
---|---|
at 500℃; |
6-bromo-1-methyl-1,2-dihydropyridin-2-one
phosphorus tribromide
phosphorus pentabromide
2,6-Dibromopyridine
Conditions | Yield |
---|---|
at 190℃; |
2-bromo-pyridine
bromine
A
2,6-Dibromopyridine
B
pentabromopyridine
Conditions | Yield |
---|---|
at 300℃; |
2,6-Dibromopyridine
carbon monoxide
4-chloro-aniline
N,N'-bis(4'-chlorophenyl)pyridine-2,6-dicarboxamide
Conditions | Yield |
---|---|
With triethylamine; tetrakis(triphenylphosphine) palladium(0) In toluene at 100℃; under 2574.3 Torr; for 8h; | 100% |
2,6-Dibromopyridine
trimethylsilylacetylene
2,6-bis(2-(trimethylsilyl)ethynyl)pyridine
Conditions | Yield |
---|---|
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); diisopropylamine In toluene at 20℃; Sonogashira Cross-Coupling; | 100% |
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); diisopropylamine In tetrahydrofuran at 50℃; for 6h; Inert atmosphere; | 98% |
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); N-ethyl-N,N-diisopropylamine In toluene for 90h; Sonogashira Cross-Coupling; Inert atmosphere; Darkness; | 98% |
Conditions | Yield |
---|---|
With n-butyllithium; butyl magnesium bromide In toluene at -10℃; | 100% |
With n-butyllithium; isopropyl alcohol In hexane; dichloromethane 1.) -78 deg C, 1 h, 2.) -78 deg C, 30, min; warm to room temperature; | 90% |
With n-butyllithium; formaldehyd In tetrahydrofuran at -70 - -40℃; | 90% |
Conditions | Yield |
---|---|
at 150℃; for 0.5h; Microwave irradiation; | 100% |
With potassium fluoride on basic alumina; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl at 90 - 100℃; for 8h; | 90% |
at 150℃; for 5h; Autoclave; | 48% |
2,6-Dibromopyridine
4-chlorobenzylamine
(6-bromopyridin-2-yl)(4-chlorobenzyl)amine
Conditions | Yield |
---|---|
at 150℃; for 0.5h; Neat (no solvent); Microwave irradiation; | 100% |
2,6-Dibromopyridine
pentanal
1-(6-bromo-2-pyridinyl)-1-pentanol
Conditions | Yield |
---|---|
Stage #1: 2,6-Dibromopyridine With n-butyllithium In tetrahydrofuran; hexanes at -78℃; for 1h; Stage #2: pentanal In tetrahydrofuran; hexanes at -78℃; for 0.266667h; | 100% |
2,6-Dibromopyridine
2,6-di(naphthalen-1-yl)pyridine
Conditions | Yield |
---|---|
With dichloro{bis[1-(dicyclohexylphosphanyl)piperidine]}palladium(II) In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 100℃; for 0.5h; Negishi cross-coupling reaction; In air; | 100% |
Conditions | Yield |
---|---|
With potassium hydroxide; 18-crown-6 ether In toluene for 1h; Heating; | 99.9% |
Stage #1: benzyl alcohol With sodium hydride In tetrahydrofuran for 0.5h; Stage #2: 2,6-Dibromopyridine In tetrahydrofuran at 20℃; for 18h; | 90% |
With sodium hydride In N,N-dimethyl-formamide at 0 - 100℃; for 18h; | 79% |
Conditions | Yield |
---|---|
Stage #1: acetonitrile With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Stage #2: 2,6-Dibromopyridine In tetrahydrofuran; hexane at -78 - 20℃; for 1.25h; | 99% |
Stage #1: acetonitrile With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.75h; Metallation; Stage #2: 2,6-Dibromopyridine In tetrahydrofuran; hexane at -78 - 20℃; for 2.5h; Alkylation; | 91% |
With n-butyllithium 1.) hexane, THF,-70 deg C, 1 h, 2.) -70 deg C,1 h; Yield given. Multistep reaction; | |
Stage #1: acetonitrile With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Stage #2: 2,6-Dibromopyridine In tetrahydrofuran; hexane at -78 - 20℃; for 1.5h; | |
Stage #1: acetonitrile With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Stage #2: 2,6-Dibromopyridine In tetrahydrofuran; hexane at -78℃; for 0.75h; |
2,6-Dibromopyridine
2-bromo-6-deuteropyridine
Conditions | Yield |
---|---|
Stage #1: 2,6-Dibromopyridine With n-butyllithium In tetrahydrofuran; hexane at -75℃; for 0.25h; Inert atmosphere; Stage #2: With deuteromethanol In tetrahydrofuran; hexane at -75℃; for 1.01667h; | 99% |
Stage #1: 2,6-Dibromopyridine With isopropylmagnesium chloride In tetrahydrofuran at 20℃; for 2h; Substitution; Stage #2: With water-d2 In tetrahydrofuran at 20℃; for 18h; Substitution; | 95% |
With n-butyllithium; Isopropanol-d1 In hexane; dichloromethane 1.) -78 deg C, 1 h, 2.) -78 deg C, 30, min; warm to room temperature; | 86% |
Stage #1: 2,6-Dibromopyridine In tetrahydrofuran at 20℃; for 1h; Stage #2: With water-d2 In tetrahydrofuran for 0.5h; |
2,6-Dibromopyridine
tris((2-phenyl)ethynyl)indium
2,6-bis(2-phenylethynyl)pyridine
Conditions | Yield |
---|---|
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride In tetrahydrofuran Heating; | 99% |
Conditions | Yield |
---|---|
With C37H28N8O*2Cl(1-)*Pd(2+); potassium carbonate In ethanol at 70℃; for 2h; Suzuki-Miyaura Coupling; | 99% |
With potassium phosphate tribasic trihydrate; trans-[(2-mesitylpy)2PdCl2] In methanol; water at 80℃; for 1h; Suzuki-Miyaura Coupling; | 99% |
With {2,6-bis[(di-1-piperidinylphosphino)amino]phenyl}palladium(II) chloride; potassium carbonate In 1,4-dioxane; water; butan-1-ol at 100℃; for 2h; Suzuki-Miyaura reaction; | 96% |
Conditions | Yield |
---|---|
With potassium phosphate tribasic trihydrate; trans-[(2-mesitylpy)2PdCl2] In methanol; water at 80℃; for 1h; Catalytic behavior; Solvent; Time; Reagent/catalyst; Suzuki-Miyaura Coupling; | 99% |
With tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine In tetrahydrofuran for 16h; Heating; | 65% |
With tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium(0) In tetrahydrofuran | 65% |
With potassium phosphate; dichloro{bis[1-(dicyclohexylphosphanyl)piperidine]}palladium(II) In toluene at 80℃; for 4h; Suzuki-Miyaura cross-coupling reaction; Air; | 64% |
Conditions | Yield |
---|---|
With C19H16ClNPdS; potassium carbonate In N,N-dimethyl-formamide at 110℃; for 24h; Reagent/catalyst; Sonogashira Cross-Coupling; | 99% |
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine In N,N-dimethyl-formamide at 80℃; Inert atmosphere; | 96% |
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine In N,N-dimethyl-formamide at 80℃; Inert atmosphere; | 96% |
2,6-Dibromopyridine
3,4,5-Trimethoxyaniline
6-bromo-N-(3,4,5-trimethoxyphenyl)pyridin-2-amine
Conditions | Yield |
---|---|
With potassium hexamethylsilazane In 1,4-dioxane at 20℃; for 1h; | 99% |
With potassium phosphate In 1,4-dioxane at 25℃; for 0.333333h; metal-free Buchwald-Hartwig amination; Inert atmosphere; | 98% |
2,6-Dibromopyridine
N-methylaniline
N,N'-dimethyl-N,N'-diphenylpyridine-2,6-diamine
Conditions | Yield |
---|---|
With potassium hexamethylsilazane In 1,4-dioxane at 100℃; for 0.5h; metal-free Buchwald-Hartwig amination; Inert atmosphere; | 99% |
2,6-Dibromopyridine
4-(ethoxycarbonyl)phenylzinc iodide
diethyl 4,4'-pyridine-2,6-diyldibenzoate
Conditions | Yield |
---|---|
With dichloro{bis[1-(dicyclohexylphosphanyl)piperidine]}palladium(II) In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 100℃; for 0.5h; Negishi cross-coupling reaction; In air; | 99% |
2,6-Dibromopyridine
N-ethyl-N-phenylamine
6-bromo-N-ethyl-N-phenylpyridin-2-amine
Conditions | Yield |
---|---|
With potassium hexamethylsilazane In 1,4-dioxane at 20℃; for 0.25h; | 99% |
Conditions | Yield |
---|---|
With potassium phosphate tribasic trihydrate; trans-[(2-mesitylpy)2PdCl2] In methanol; water at 80℃; for 1h; Suzuki-Miyaura Coupling; | 99% |
With [Pd(Cl)κ2-S,N-C6H4CS=N-(4-Py)(PPh3)]; potassium carbonate In toluene at 80℃; for 5h; Suzuki coupling; | 82% |
2,6-Dibromopyridine
Conditions | Yield |
---|---|
Stage #1: 4-((tert-butyldimethylsilyl)oxy)-N,N,2,2-tetramethylbutanamide With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Stage #2: 2,6-Dibromopyridine In tetrahydrofuran; hexane at -78 - 20℃; for 1h; | 99% |
Conditions | Yield |
---|---|
With potassium phosphate In 1,4-dioxane at 100℃; for 7h; | 98% |
With copper(l) iodide; potassium carbonate at 50℃; for 1h; | 88% |
With potassium phosphate In 1,4-dioxane at 105℃; for 10h; Inert atmosphere; | 88% |
2,6-Dibromopyridine
N,N-dimethyl-formamide
2-bromo-6-(hydroxymethyl)pyridine
Conditions | Yield |
---|---|
Stage #1: 2,6-Dibromopyridine; N,N-dimethyl-formamide With n-butyllithium Stage #2: With sodium tetrahydroborate | 98% |
Stage #1: 2,6-Dibromopyridine With n-butyllithium In tetrahydrofuran; hexane at -70℃; for 0.25h; Inert atmosphere; Stage #2: N,N-dimethyl-formamide In tetrahydrofuran; hexane at -78℃; for 0.25h; Further stages; | 92% |
Stage #1: 2,6-Dibromopyridine With n-butyllithium In tetrahydrofuran; light petroleum at -78℃; for 3.16667h; Inert atmosphere; Stage #2: N,N-dimethyl-formamide In tetrahydrofuran; light petroleum at -78℃; Inert atmosphere; Stage #3: With sodium tetrahydroborate In tetrahydrofuran; methanol; light petroleum; acetic acid at 20℃; Inert atmosphere; | 82% |
2,6-Dibromopyridine
(1R)-fenchone
(1R,2R,4S)-2-(6-bromopyridine-2-yl)-1,3,3-trimethylbicyclo[2.2.1]heptan-2-ol
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran; hexane at -78℃; diastereoselective reaction; | 98% |
Stage #1: 2,6-Dibromopyridine With n-butyllithium In diethyl ether; hexane at -78℃; for 0.5h; Stage #2: (1R)-fenchone In diethyl ether; hexane Further stages.; | 90% |
Stage #1: 2,6-Dibromopyridine With n-butyllithium In diethyl ether; hexane at -78 - -45℃; for 0.25h; Metallation; Stage #2: (1R)-fenchone In diethyl ether; hexane at -78 - 20℃; for 3.5h; Addition; | 48% |
2,6-Dibromopyridine
4-methoxy-2,6-dimethylphenylboronic acid
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium(0) In tetrahydrofuran | 98% |
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In DMF (N,N-dimethyl-formamide) at 100℃; for 9h; | 98% |
Conditions | Yield |
---|---|
Stage #1: 2,6-Dibromopyridine With n-butyllithium In tetrahydrofuran; hexane at -76 - -60℃; Stage #2: acetone In tetrahydrofuran; hexane at 20℃; Cooling with dry ice; Stage #3: With ammonium chloride In tetrahydrofuran; hexane; water | 98% |
With n-butyllithium In tetrahydrofuran; hexane at -76 - 20℃; for 1.25h; Cooling with ice; | 94.3% |
Stage #1: 2,6-Dibromopyridine With n-butyllithium In tetrahydrofuran; hexane at -76℃; for 0.75h; Cooling with acetone-dry ice; Stage #2: acetone In tetrahydrofuran; hexane at 20℃; for 1.25h; Cooling with acetone-dry ice; | 94% |
2,6-Dibromopyridine
2,6-diisopropylbenzenamine
N-[2,6-bis(1-methylethyl)phenyl]-6-bromopyridin-2-amine
Conditions | Yield |
---|---|
With potassium phosphate In 1,4-dioxane at 25℃; for 0.333333h; metal-free Buchwald-Hartwig amination; Inert atmosphere; | 98% |
With potassium hexamethylsilazane In 1,4-dioxane at 20℃; for 1h; | 78% |
With 2,2,6,6-tetramethyl-piperidine at 230℃; for 6h; Sealed tube; | 20% |
2,6-Dibromopyridine
N-methylaniline
6-bromo-N-methyl-N-phenylpyridin-2-amine
Conditions | Yield |
---|---|
With potassium phosphate In 1,4-dioxane at 25℃; for 0.333333h; metal-free Buchwald-Hartwig amination; Inert atmosphere; | 98% |
With potassium hexamethylsilazane In 1,4-dioxane at 20℃; for 0.5h; | 98% |
2,6-Dibromopyridine
2-(methylamino)-6-bromopyridine
N-methyl-bis(6-bromopyridin-2-yl)amine
Conditions | Yield |
---|---|
Stage #1: 2-bromo-6-(methylamino)pyridine With sodium hydride In tetrahydrofuran at 20℃; Reflux; Stage #2: 2,6-Dibromopyridine In tetrahydrofuran for 6h; Reflux; | 98% |
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