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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

Phenprobamate Manufacturer/High quality/Best price/In stock

Cas:673-31-4

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Hangzhou Dingyan Chem Co., Ltd

Items Standard Result Assay (Ursolic acid) 98%min 98.22% ----------------------------------------------------------------

High purity 673-31-4 phenprobamate

Cas:673-31-4

Min.Order:1 Gram

FOB Price: $100.0 / 500.0

Type:Trading Company

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Phenprobamate supplier in China

Cas:673-31-4

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

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Hangzhou JINLAN Pharm-Drugs Technology Co., Ltd

We can provide GMP validation service that complies with SFDA, FDA, WHO and EU EMPA.Excellent registration team could help us easlily to register our products in different countries.If you and your customer are interested in some products or need C

Phenprobamate manufacturer with low price

Cas:673-31-4

Min.Order:1 Gram

Negotiable

Type:Manufacturers

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Xi`an Eastling Biotech Co., Ltd.

Phenprobamate CAS: 673-31-4 Molecular Formula: C10H13NO2 Home Product Category other other 673-31-4 673-31-4 - Names and Identifiers Name Phenprobamate Synonyms MH 532 HG 532 Spantol Extacol Eirenal

Factory Directly Supply Top Quality Phenprobamate

Cas:673-31-4

Min.Order:1 Kilogram

FOB Price: $98.0 / 105.0

Type:Trading Company

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Shanghai Seasonsgreen Chemical Co.,Ltd

Shanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu

lower price High quality Phenprobamate

Cas:673-31-4

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Manufacturers

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Phenprobamate

Cas:673-31-4

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

Phenprobamate Basic information Product Name: Phenprobamate Synonyms: PHENPROBAMATE;1-Carbamoyloxy-3-phenylpropane;1-Propanol, 3-phenyl-, carbamate;3-phenyl-1-propanocarbamate;3-Phenyl-1

Phenprobamate_

Cas:673-31-4

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

Phenprobamate

Cas:673-31-4

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supply CAS 673-31-4 with best quality

Cas:673-31-4

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Name: Phenprobamate Synonyms: 3-Phenyl-1-propanol carbamate CAS: 673-31-4 MF: C10H13NO2 Appearance:White powder Storage:Store in cool and dry place, away from sun light. Package:25kg/drum Application:APIs Transportation:By sea or by air Port:Qing

Phenprobamate

Cas:673-31-4

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Benzenepropanol,1-carbamate 673-31-4

Cas:673-31-4

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Minstar Chemical Co., Ltd

Product Name: Phenprobamate CAS: 673-31-4 MF: C10H13NO2 MW: 179.22 EINECS: 211-606-1 Mol File: 673-31-4.mol Phenprobamate Structure Phenprobamate Chemical Properties Melting point 101-104° Boiling point 311.75°C (r

Phenprobamate

Cas:673-31-4

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present

Phenprobamate with CAS:673-31-4

Cas:673-31-4

Min.Order:1 Kilogram

FOB Price: $86.0 / 120.0

Type:Trading Company

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Qingdao Beluga Import and Export Co., LTD

Phenprobamate CAS:673-31-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates

Phenprobamate CAS:673-31-4

Cas:673-31-4

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

3-Phenylpropyl carbamate

Cas:673-31-4

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Xi'an Yinherb Bio-Tech Co., Ltd.

Xi'an Yinherb Bio-Tech Co., Ltd was founded in 2009, We have more than 10 experienced doctors and scientists and professional managers, specializing in Nootropics, Sarms and Peptides researching and developing, and become the lead

China Factory Supply Top Quality Phenprobamate with Best Price 673-31-4 Stock Supply

Cas:673-31-4

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

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Triumph International Development Limilted

Triumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Business Custom Synthesis: Trading(Raw M

Benzenepropanol,1-carbamate

Cas:673-31-4

Min.Order:0 Metric Ton

FOB Price: $18.0 / 20.0

Type:Lab/Research institutions

inquiry

Hubei Jiutian Bio-medical Technology Co., Ltd

1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie

Phenprobamate CAS 673-31-4

Cas:673-31-4

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

Phenprobamate

Cas:673-31-4

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Phenprobamate

Cas:673-31-4

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Afine Chemicals Limited

Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

PHENPROBAMATE

Cas:673-31-4

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Benzenepropanol,1-carbamate

Cas:673-31-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality Phenprobamate

Cas:673-31-4

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

High Purity Pharmaceutical Powder Phenprobamate For Muscle Relaxation

Cas:673-31-4

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

inquiry

TaiChem Taizhou Limited

Established in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site

Phenprobamate

Cas:673-31-4

Min.Order:10 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

Phenprobamate

Cas:673-31-4

Min.Order:1 Milligram

Negotiable

Type:Trading Company

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

Phenprobamate

Cas:673-31-4

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Hangzhou Huarong Pharm Co., Ltd.

Hangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu

3-Phenylpropyl carbamate

Cas:673-31-4

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

Phenprobamate

Cas:673-31-4

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

3-Phenyl-1-propanol
122-97-4

3-Phenyl-1-propanol

carbamic acid phenyl ester
622-46-8

carbamic acid phenyl ester

phenprobamate
673-31-4

phenprobamate

Conditions
ConditionsYield
With di-n-butyltin maleate In toluene at 90℃; for 4h;99%
3-Phenyl-1-propanol
122-97-4

3-Phenyl-1-propanol

methyl carbamate
598-55-0

methyl carbamate

phenprobamate
673-31-4

phenprobamate

Conditions
ConditionsYield
With di-n-butyltin maleate In toluene for 3h; Reflux;98%
3-Phenyl-1-propanol
122-97-4

3-Phenyl-1-propanol

sodium cyanide
143-33-9

sodium cyanide

phenprobamate
673-31-4

phenprobamate

Conditions
ConditionsYield
With trifluoroacetic acid
C12H12Cl3NO3

C12H12Cl3NO3

phenprobamate
673-31-4

phenprobamate

Conditions
ConditionsYield
With methanol; potassium carbonate In 1,2-dichloro-ethane Inert atmosphere;
3-Phenyl-1-propanol
122-97-4

3-Phenyl-1-propanol

phenprobamate
673-31-4

phenprobamate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1,2-dichloro-ethane / 5 h / 0 °C / Inert atmosphere
2: methanol; potassium carbonate / 1,2-dichloro-ethane / Inert atmosphere
View Scheme
3-phenylpropyl hydroxycarbamate

3-phenylpropyl hydroxycarbamate

phenprobamate
673-31-4

phenprobamate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: potassium carbonate / diethyl ether / 12 h / 0 - 20 °C
2: tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; potassium carbonate / 12 h / 25 °C / Inert atmosphere; Irradiation
View Scheme
3-phenylpropyl [{3,5-bis(trifluoromethyl)benzoyl}oxy]carbamate

3-phenylpropyl [{3,5-bis(trifluoromethyl)benzoyl}oxy]carbamate

phenprobamate
673-31-4

phenprobamate

Conditions
ConditionsYield
With tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; potassium carbonate at 25℃; for 12h; Inert atmosphere; Irradiation;30 %Spectr.
phenprobamate
673-31-4

phenprobamate

pinacol vinylboronate
75927-49-0

pinacol vinylboronate

(3R)-3-(4',4',5',5'-tetramethyl-1',3',2’-dioxaborolanyl)-5-phenylpent-1-ene
1000376-26-0

(3R)-3-(4',4',5',5'-tetramethyl-1',3',2’-dioxaborolanyl)-5-phenylpent-1-ene

Conditions
ConditionsYield
Stage #1: phenprobamate With (2-methylpropyl)lithium In diethyl ether; hexane; cyclohexane at -78℃; for 5h;
Stage #2: pinacol vinylboronate In diethyl ether; hexane; cyclohexane at -78℃; for 1h;
Stage #3: With magnesium dibromide etherate In diethyl ether; hexane; cyclohexane at 20℃; for 16h; Reflux; enantioselective reaction;
79%
phenprobamate
673-31-4

phenprobamate

4,4,5,5-tetramethyl-2-[(1E)-prop-1-en-1-yl]-1,3,2-dioxaborolane
83947-58-4

4,4,5,5-tetramethyl-2-[(1E)-prop-1-en-1-yl]-1,3,2-dioxaborolane

(2E,4R)-4-(4’,4’,5’,5’-tetramethyl-1’,3’,2’-dioxaborolanyl)-6-phenylhex-2-ene
1428538-05-9

(2E,4R)-4-(4’,4’,5’,5’-tetramethyl-1’,3’,2’-dioxaborolanyl)-6-phenylhex-2-ene

Conditions
ConditionsYield
Stage #1: phenprobamate With (2-methylpropyl)lithium In diethyl ether; hexane; cyclohexane at -78℃; for 5h;
Stage #2: 4,4,5,5-tetramethyl-2-[(1E)-prop-1-en-1-yl]-1,3,2-dioxaborolane In diethyl ether; hexane; cyclohexane at -78℃; for 1h;
Stage #3: With magnesium dibromide etherate In diethyl ether; hexane; cyclohexane at 20℃; for 16h; Reflux; enantioselective reaction;
77%
phenprobamate
673-31-4

phenprobamate

(+/-)-4-phenyl-1,3-oxazinan-2-one

(+/-)-4-phenyl-1,3-oxazinan-2-one

Conditions
ConditionsYield
With iodosylbenzene; (±)-trans-N,N′-1,2-cyclohexylenebis(4-nitrobenzylideneamine); tetrakis(acetonitrile)copper(I) hexafluorophosphate In acetonitrile at 45℃; Molecular sieve; Inert atmosphere;54%
phenprobamate
673-31-4

phenprobamate

3-trifluoromethylphenyl sulfinic acid sodium salt
118849-61-9

3-trifluoromethylphenyl sulfinic acid sodium salt

Glyoxilic acid
298-12-4

Glyoxilic acid

(3-Phenyl-propoxycarbonylamino)-(3-trifluoromethyl-benzenesulfonyl)-acetic acid
41142-04-5

(3-Phenyl-propoxycarbonylamino)-(3-trifluoromethyl-benzenesulfonyl)-acetic acid

Conditions
ConditionsYield
(i) aq. HCO2H, (ii) /BRN= 1959273/; Multistep reaction;
phenprobamate
673-31-4

phenprobamate

Sodium; 2-chloro-5-trifluoromethyl-benzenesulfinate

Sodium; 2-chloro-5-trifluoromethyl-benzenesulfinate

Glyoxilic acid
298-12-4

Glyoxilic acid

(2-Chloro-5-trifluoromethyl-benzenesulfonyl)-(3-phenyl-propoxycarbonylamino)-acetic acid
41142-18-1

(2-Chloro-5-trifluoromethyl-benzenesulfonyl)-(3-phenyl-propoxycarbonylamino)-acetic acid

Conditions
ConditionsYield
(i) H2O, (ii) /BRN= 6307616/, HCO2H; Multistep reaction;
(E)-1-propenylboronic acid 2,2-dimethyl-1,3-propanediol ester

(E)-1-propenylboronic acid 2,2-dimethyl-1,3-propanediol ester

phenprobamate
673-31-4

phenprobamate

C17H25BO2

C17H25BO2

Conditions
ConditionsYield
Stage #1: phenprobamate With sec.-butyllithium; (-)-sparteine In diethyl ether; hexane; cyclohexane at -78℃;
Stage #2: (E)-1-propenylboronic acid 2,2-dimethyl-1,3-propanediol ester In diethyl ether; hexane; cyclohexane at -78 - 20℃;
(E)-1-propenylboronic acid 2,2-dimethyl-1,3-propanediol ester

(E)-1-propenylboronic acid 2,2-dimethyl-1,3-propanediol ester

phenprobamate
673-31-4

phenprobamate

C17H25BO2

C17H25BO2

Conditions
ConditionsYield
Stage #1: phenprobamate With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium In diethyl ether; hexane; cyclohexane at -78℃;
Stage #2: (E)-1-propenylboronic acid 2,2-dimethyl-1,3-propanediol ester In diethyl ether; hexane; cyclohexane at -78 - 20℃;
phenprobamate
673-31-4

phenprobamate

9-((E)-prop-1-enyl)-9-borabicyclo[3.3.1]nonane

9-((E)-prop-1-enyl)-9-borabicyclo[3.3.1]nonane

C20H29B

C20H29B

Conditions
ConditionsYield
Stage #1: phenprobamate With sec.-butyllithium; (-)-sparteine In diethyl ether; hexane; cyclohexane at -78℃;
Stage #2: 9-((E)-prop-1-enyl)-9-borabicyclo[3.3.1]nonane In diethyl ether; hexane; cyclohexane at -78℃;
phenprobamate
673-31-4

phenprobamate

9-((E)-prop-1-enyl)-9-borabicyclo[3.3.1]nonane

9-((E)-prop-1-enyl)-9-borabicyclo[3.3.1]nonane

C20H29B

C20H29B

Conditions
ConditionsYield
Stage #1: phenprobamate With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium In diethyl ether; hexane; cyclohexane at -78℃;
Stage #2: 9-((E)-prop-1-enyl)-9-borabicyclo[3.3.1]nonane In diethyl ether; hexane; cyclohexane at -78℃;
phenprobamate
673-31-4

phenprobamate

9-((E)-hex-1-enyl)-9-borabicyclo[3.3.1]nonane

9-((E)-hex-1-enyl)-9-borabicyclo[3.3.1]nonane

C23H35B

C23H35B

Conditions
ConditionsYield
Stage #1: phenprobamate With sec.-butyllithium; (-)-sparteine In diethyl ether; hexane; cyclohexane at -78℃;
Stage #2: 9-((E)-hex-1-enyl)-9-borabicyclo[3.3.1]nonane In diethyl ether; hexane; cyclohexane at -78℃;
phenprobamate
673-31-4

phenprobamate

9-((E)-hex-1-enyl)-9-borabicyclo[3.3.1]nonane

9-((E)-hex-1-enyl)-9-borabicyclo[3.3.1]nonane

C23H35B

C23H35B

Conditions
ConditionsYield
Stage #1: phenprobamate With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium In diethyl ether; hexane; cyclohexane at -78℃;
Stage #2: 9-((E)-hex-1-enyl)-9-borabicyclo[3.3.1]nonane In diethyl ether; hexane; cyclohexane at -78℃;
phenprobamate
673-31-4

phenprobamate

((E)-3-(9-borabicyclo[3.3.1]nonan-9-yl)allyloxy)trimethylsilane

((E)-3-(9-borabicyclo[3.3.1]nonan-9-yl)allyloxy)trimethylsilane

C23H37BOSi

C23H37BOSi

Conditions
ConditionsYield
Stage #1: phenprobamate With sec.-butyllithium; (-)-sparteine In diethyl ether; hexane; cyclohexane at -78℃;
Stage #2: ((E)-3-(9-borabicyclo[3.3.1]nonan-9-yl)allyloxy)trimethylsilane In diethyl ether; hexane; cyclohexane at -78℃;
phenprobamate
673-31-4

phenprobamate

((E)-3-(9-borabicyclo[3.3.1]nonan-9-yl)allyloxy)trimethylsilane

((E)-3-(9-borabicyclo[3.3.1]nonan-9-yl)allyloxy)trimethylsilane

C23H37BOSi

C23H37BOSi

Conditions
ConditionsYield
Stage #1: phenprobamate With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium In diethyl ether; hexane; cyclohexane at -78℃;
Stage #2: ((E)-3-(9-borabicyclo[3.3.1]nonan-9-yl)allyloxy)trimethylsilane In diethyl ether; hexane; cyclohexane at -78℃;
phenprobamate
673-31-4

phenprobamate

B-2-(E)-(hex-1-en-1-yl)-5,5-dimethyl-1,3,2-dioxaborinane
1218988-11-4

B-2-(E)-(hex-1-en-1-yl)-5,5-dimethyl-1,3,2-dioxaborinane

C20H31BO2

C20H31BO2

Conditions
ConditionsYield
Stage #1: phenprobamate With sec.-butyllithium; (-)-sparteine In diethyl ether; hexane; cyclohexane at -78℃;
Stage #2: B-2-(E)-(hex-1-en-1-yl)-5,5-dimethyl-1,3,2-dioxaborinane In diethyl ether; hexane; cyclohexane at -78 - 20℃;
phenprobamate
673-31-4

phenprobamate

B-2-(E)-(hex-1-en-1-yl)-5,5-dimethyl-1,3,2-dioxaborinane
1218988-11-4

B-2-(E)-(hex-1-en-1-yl)-5,5-dimethyl-1,3,2-dioxaborinane

C20H31BO2

C20H31BO2

Conditions
ConditionsYield
Stage #1: phenprobamate With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium In diethyl ether; hexane; cyclohexane at -78℃;
Stage #2: B-2-(E)-(hex-1-en-1-yl)-5,5-dimethyl-1,3,2-dioxaborinane In diethyl ether; hexane; cyclohexane at -78 - 20℃;
phenprobamate
673-31-4

phenprobamate

(Z)-4,4,5,5-tetramethyl-2-(prop-1-en-1-yl)-1,3,2-dioxaborolane
83947-59-5

(Z)-4,4,5,5-tetramethyl-2-(prop-1-en-1-yl)-1,3,2-dioxaborolane

C18H27BO2

C18H27BO2

Conditions
ConditionsYield
Stage #1: phenprobamate With sec.-butyllithium; (-)-sparteine In diethyl ether; hexane; cyclohexane at -78℃;
Stage #2: (Z)-4,4,5,5-tetramethyl-2-(prop-1-en-1-yl)-1,3,2-dioxaborolane In diethyl ether; hexane; cyclohexane at -78 - 20℃;
phenprobamate
673-31-4

phenprobamate

(Z)-4,4,5,5-tetramethyl-2-(prop-1-en-1-yl)-1,3,2-dioxaborolane
83947-59-5

(Z)-4,4,5,5-tetramethyl-2-(prop-1-en-1-yl)-1,3,2-dioxaborolane

C18H27BO2

C18H27BO2

Conditions
ConditionsYield
Stage #1: phenprobamate With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium In diethyl ether; hexane; cyclohexane at -78℃;
Stage #2: (Z)-4,4,5,5-tetramethyl-2-(prop-1-en-1-yl)-1,3,2-dioxaborolane In diethyl ether; hexane; cyclohexane at -78 - 20℃;
phenprobamate
673-31-4

phenprobamate

(Z)-2-(hex-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
91083-23-7

(Z)-2-(hex-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

C21H33BO2

C21H33BO2

Conditions
ConditionsYield
Stage #1: phenprobamate With sec.-butyllithium; (-)-sparteine In diethyl ether; hexane; cyclohexane at -78℃;
Stage #2: (Z)-2-(hex-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane In diethyl ether; hexane; cyclohexane at -78 - 20℃;
phenprobamate
673-31-4

phenprobamate

(Z)-2-(hex-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
91083-23-7

(Z)-2-(hex-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

C21H33BO2

C21H33BO2

Conditions
ConditionsYield
Stage #1: phenprobamate With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium In diethyl ether; hexane; cyclohexane at -78℃;
Stage #2: (Z)-2-(hex-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane In diethyl ether; hexane; cyclohexane at -78 - 20℃;
phenprobamate
673-31-4

phenprobamate

(1S,2S,3E)-2-methyl-1,6-diphenylhex-3-en-1-ol
1218988-28-3

(1S,2S,3E)-2-methyl-1,6-diphenylhex-3-en-1-ol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: (2-methylpropyl)lithium / hexane; cyclohexane; diethyl ether / 5 h / -78 °C
1.2: 1 h / -78 °C
1.3: 16 h / 20 °C / Reflux
2.1: n-butyllithium / hexane; tetrahydrofuran / 0.25 h / -78 °C
2.2: 0.5 h / -78 °C
2.3: 16 h / -78 - 20 °C
View Scheme
phenprobamate
673-31-4

phenprobamate

A

(1R,2R,3Z)-2-methyl-1,6-diphenylhex-3-en-1-ol
1218988-13-6

(1R,2R,3Z)-2-methyl-1,6-diphenylhex-3-en-1-ol

B

(1S,2S,3E)-2-methyl-1,6-diphenylhex-3-en-1-ol
1218988-28-3

(1S,2S,3E)-2-methyl-1,6-diphenylhex-3-en-1-ol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: (2-methylpropyl)lithium / hexane; cyclohexane; diethyl ether / 5 h / -78 °C
1.2: 1 h / -78 °C
1.3: 16 h / 20 °C / Reflux
2.1: tetrahydrofuran / 96 h / 20 °C
View Scheme
phenprobamate
673-31-4

phenprobamate

((3R)-5-phenylpent-1-en-3-yl)trifluoroborate

((3R)-5-phenylpent-1-en-3-yl)trifluoroborate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: (2-methylpropyl)lithium / hexane; cyclohexane; diethyl ether / 5 h / -78 °C
1.2: 1 h / -78 °C
1.3: 16 h / 20 °C / Reflux
2.1: L-Tartaric acid / acetonitrile; water; tetrahydrofuran; methanol / 20 °C
View Scheme
phenprobamate
673-31-4

phenprobamate

A

(1R,3Z)-1,6-diphenylhex-3-en-1-ol
1428537-74-9

(1R,3Z)-1,6-diphenylhex-3-en-1-ol

B

(1S,3E)-1,6-diphenylhex-3-en-1-ol
1428537-73-8

(1S,3E)-1,6-diphenylhex-3-en-1-ol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: (2-methylpropyl)lithium / hexane; cyclohexane; diethyl ether / 5 h / -78 °C
1.2: 1 h / -78 °C
1.3: 16 h / 20 °C / Reflux
2.1: tetrahydrofuran / 96 h / 20 °C
View Scheme
phenprobamate
673-31-4

phenprobamate

(1S,3E)-1,6-diphenylhex-3-en-1-ol
1428537-73-8

(1S,3E)-1,6-diphenylhex-3-en-1-ol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: (2-methylpropyl)lithium / hexane; cyclohexane; diethyl ether / 5 h / -78 °C
1.2: 1 h / -78 °C
1.3: 16 h / 20 °C / Reflux
2.1: n-butyllithium / hexane; tetrahydrofuran / 0.25 h / -78 °C
2.2: 0.5 h / -78 °C
2.3: -78 - 20 °C
View Scheme

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