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Cas:68524-30-1
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inquiryProduct informations Product Name 2-[(Diphenylmethyl)thio]acetamide CAS No. 68524-30-1 Appear
Cas:68524-30-1
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryShanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
Cas:68524-30-1
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inquiryDayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:68524-30-1
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:68524-30-1
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:68524-30-1
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:68524-30-1
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inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W
Cas:68524-30-1
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inquiry2-[(Diphenylmethyl)thio]acetamide Basic information Product Name: 2-[(Diphenylmethyl)thio]acetamide Synonyms: 2-[(DIPHENYLMETHYL)THIO]-ACETAMIDE;DIPHENYL METHYL THIO ACETAMIDE;2-[(Diphenylmethyl) Thio] Acetylamine;2-[(Diphenylmethyl)thio
Cas:68524-30-1
Min.Order:25 Kilogram
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Cas:68524-30-1
Min.Order:1 Kilogram
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inquiry2-[(Diphenylmethyl)thio]acetamide Basic information Product Name: 2-[(Diphenylmethyl)thio]acetamide Synonyms: Armodafinil Impurity E (USP RC C);2-[(DIPHENYLMETHYL)THIO]-ACETAMIDE;2-[(Diphenylmethyl) Thio] Acetylamine;2-[(Diphenylmethyl)thio] ac
Cas:68524-30-1
Min.Order:1 Kilogram
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:68524-30-1
Min.Order:1 Kilogram
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inquiry2-[(Diphenylmethyl)thio]acetamide CAS:68524-30-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality
Cas:68524-30-1
Min.Order:1 Gram
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Cas:68524-30-1
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:68524-30-1
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inquiryOverview Quick Details CAS No.: 68524-30-1 Other Names: 2-[(Diphenylmethyl)thio]acetamide CAS 68524-30-1 MF: C15H15NOS, C15H15NOS EINECS No.: 68524-30-1 Place of Origin: Shandong, China (Mainland) Type: Pharmaceutical Intermediates Puri
Cas:68524-30-1
Min.Order:1 Kilogram
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:68524-30-1
Min.Order:0 Metric Ton
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
Cas:68524-30-1
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:68524-30-1
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:68524-30-1
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiry2-[(Diphenylmethyl)thio]acetamideAppearance:White Crystalline Solid Storage:Protected from light, stored hermetically and in a dry place Package:according to customers' requirements Application:Pharmaceutical Intermediate Transportation:By air(EMS or
Superior quality, moderate price & quick delivery. Appearance:white powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:10g/bag,or as your request Application:Used as Pharmaceutical Intermediates Transp
Cas:68524-30-1
Min.Order:1 Gram
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Type:Trading Company
inquiryProduct name: 2-[(Diphenylmethyl)Thio]Acetamide CAS No.:68524-30-1 Molecule Formula:C15H15NOS Molecule Weight:257.35 Purity: 99% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard TE
Cas:68524-30-1
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:68524-30-1
Min.Order:1 Kilogram
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inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
Cas:68524-30-1
Min.Order:1 Milligram
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:68524-30-1
Min.Order:1 Kilogram
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Type:Trading Company
inquiryConditions | Yield |
---|---|
Stage #1: diphenylchloromethane With thiourea; potassium iodide In water at 70 - 75℃; for 1.5h; Stage #2: With sodium hydroxide In water at 15 - 24℃; Stage #3: Chloroacetamide With triethylamine more than 3 stages; | 97.9% |
Stage #1: diphenylchloromethane With thiourea In isopropyl alcohol at 100℃; for 2h; Sealed tube; Stage #2: Chloroacetamide With potassium hydroxide In methanol; isopropyl alcohol at 60℃; for 2h; Sonication; |
benzhydrylsulfanyl acetyl chloride
2-(diphenylmethylthio)acetamide
Conditions | Yield |
---|---|
With ammonium hydroxide In tetrahydrofuran; dichloromethane at 0℃; for 1h; | 96% |
With ammonium hydroxide In dichloromethane for 2h; | 17.0 g |
With ammonium hydroxide In dichloromethane at 2℃; for 20h; | |
With ammonium hydroxide In dichloromethane; water at 0℃; for 1h; | 14.39 g |
With ammonium hydroxide In water at 0 - 20℃; for 20h; Alkaline conditions; |
1,1-Diphenylmethanol
sodium S-(carbamoylmethyl)thiosulfate
2-(diphenylmethylthio)acetamide
Conditions | Yield |
---|---|
With formic acid In water at 60℃; for 0.333333h; | 92% |
(benzhydrylthio)acetic acid
2-(diphenylmethylthio)acetamide
Conditions | Yield |
---|---|
With ammonium carbamate; novozyme-435 In tert-butyl alcohol at 60℃; for 168h; | 90% |
Stage #1: (benzhydrylthio)acetic acid With thionyl chloride In benzene for 2h; Reflux; Stage #2: With ammonia In dichloromethane at 20℃; for 2h; Cooling with ice; | 69% |
Stage #1: (benzhydrylthio)acetic acid With thionyl chloride In benzene at 20℃; for 1h; Inert atmosphere; Reflux; Stage #2: With ammonium hydroxide In dichloromethane at 0℃; for 1h; | 54% |
bromo-acetic acid amide
diphenylmethylisothiouronium bromide
2-(diphenylmethylthio)acetamide
Conditions | Yield |
---|---|
Stage #1: diphenylmethylisothiouronium bromide With sodium hydroxide In water at 40 - 80℃; Stage #2: bromo-acetic acid amide at 60 - 70℃; for 5 - 6h; | 90% |
diphenylmethylisothiouronium bromide
Chloroacetamide
2-(diphenylmethylthio)acetamide
Conditions | Yield |
---|---|
Stage #1: diphenylmethylisothiouronium bromide With sodium hydroxide In water at 40 - 85℃; Stage #2: Chloroacetamide at 30 - 70℃; for 5 - 6h; | 88% |
Stage #1: diphenylmethylisothiouronium bromide With sodium hydroxide In methanol; water at 40 - 60℃; for 0.5h; Stage #2: Chloroacetamide for 3.16667 - 4.16667h; Heating / reflux; | 71% |
Conditions | Yield |
---|---|
With Nafion-H In 2-methyltetrahydrofuran at 20℃; for 12h; Catalytic behavior; Reagent/catalyst; Solvent; Green chemistry; | 88% |
With trifluoroacetic acid at 20℃; for 4h; | 17% |
With ammonia; trifluoroacetic acid In methanol at 20℃; for 4h; | 17% |
2-(diphenylmethylthio)acetamide
Conditions | Yield |
---|---|
With acetyl chloride; potassium iodide In acetic acid at 20℃; for 0.5h; | 87% |
triethylamine
diphenylchloromethane
Chloroacetamide
2-(diphenylmethylthio)acetamide
Conditions | Yield |
---|---|
Stage #1: diphenylchloromethane With thiourea; potassium iodide In water at 70 - 95℃; for 2h; Stage #2: With sodium hydroxide In water at 15 - 24℃; Stage #3: triethylamine; Chloroacetamide more than 3 stages; | 81.4% |
2-benzhydrylsulfanylacetonitrile
2-(diphenylmethylthio)acetamide
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol for 6h; Reflux; | 75% |
(diphenylmethyl)(ethyl acetate)sulfide
2-(diphenylmethylthio)acetamide
Conditions | Yield |
---|---|
With ammonia at 100℃; |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 99.9 percent / SOCl2 / benzene / 1 h / Heating 2: 96 percent / NH4OH / CH2Cl2; tetrahydrofuran / 1 h / 0 °C View Scheme | |
Multi-step reaction with 2 steps 1: 90 percent / ammonium carbamate; Novozyme-435 / 2-methyl-propan-2-ol / 168 h / 60 °C View Scheme | |
Multi-step reaction with 3 steps 1: 99 percent / trifluoroacetic acid / 3 h / 20 °C 2: thionyl chloride / benzene / 1.5 h / Heating 3: 17.0 g / aq. NH4OH / CH2Cl2 / 2 h View Scheme |
1,1-Diphenylmethanol
2-(diphenylmethylthio)acetamide
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: concentrated aqueous HCl 2: concentrated sulfuric acid 3: ethanolic NH3 / 100 °C View Scheme | |
Multi-step reaction with 3 steps 1: trifluoroacetic acid / 20 °C 2: potassium carbonate / acetone / 4 h / Reflux 3: ammonium hydroxide; ammonium chloride / methanol / 72 h / 50 °C View Scheme | |
Multi-step reaction with 3 steps 1: Lawessons reagent / toluene / 3 h / Reflux; Inert atmosphere 2: potassium carbonate / acetone / 6 h 3: potassium hydroxide / ethanol / 6 h / Reflux View Scheme | |
Multi-step reaction with 3 steps 1: trifluoroacetic acid / 3 h 2: thionyl chloride / benzene / 2 h / Reflux 3: ammonium hydroxide / dichloromethane / 20 h / 2 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: trifluoroacetic acid / 3 h / 20 °C 2.1: thionyl chloride / benzene / 2 h / Reflux 2.2: 2 h / 20 °C / Cooling with ice View Scheme |
Conditions | Yield |
---|---|
In tetrahydrofuran; water at 70℃; for 1.25h; | |
In water; chlorobenzene at 70℃; for 0.75h; |
methyl diphenylmethylmercaptoacetate
2-(diphenylmethylthio)acetamide
Conditions | Yield |
---|---|
With ammonia In methanol at 15℃; for 1h; | |
With ammonium hydroxide; ammonium chloride In methanol at 50℃; for 72h; |
(benzhydrylthio)acetic acid
benzhydrylsulfanyl acetyl chloride
2-(diphenylmethylthio)acetamide
Conditions | Yield |
---|---|
With thionyl chloride In dichloromethane; water; tert-butyl alcohol; benzene |
2-(diphenylmethylthio)acetamide
diphenylmethanethiol
2-(diphenylmethylthio)acetamide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium carbonate / acetone / 6 h 2: potassium hydroxide / ethanol / 6 h / Reflux View Scheme |
Bromodiphenylmethane
2-(diphenylmethylthio)acetamide
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: water; acetone / 3 h / 20 - 70 °C / Inert atmosphere 2: thionyl chloride / benzene / 1 h / Inert atmosphere; Reflux 3: ammonium hydroxide / water; dichloromethane / 1 h / 0 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: water; acetone / 3 h / 20 - 70 °C / Inert atmosphere 2.1: thionyl chloride / benzene / 1 h / 20 °C / Inert atmosphere; Reflux 2.2: 1 h / 0 °C View Scheme |
2-(diphenylmethylthio)acetamide
Conditions | Yield |
---|---|
With phthaloyl peroxide In dichloromethane at 25℃; for 8h; Schlenk technique; chemoselective reaction; | 99% |
With 1-methyl-3,5-dinitropyridinium trifluoromethanesulfonate; dihydrogen peroxide In methanol; water at 25℃; for 21.5h; Reagent/catalyst; | 98% |
With 1-octyl-3,5-dinitropyridinium triflate; dihydrogen peroxide In aq. phosphate buffer; chloroform at 25℃; for 4h; pH=2; Reagent/catalyst; Green chemistry; chemoselective reaction; | 98% |
2-(diphenylmethylthio)acetamide
Conditions | Yield |
---|---|
Stage #1: 2-(diphenylmethylthio)acetamide; titanium(IV) isopropylate; diethyl (2R,3R)-tartrate In water; toluene at 55℃; for 0.833333h; Stage #2: With Cumene hydroperoxide; N-ethyl-N,N-diisopropylamine In water; toluene at 25℃; for 1h; Product distribution / selectivity; | 98.5% |
Stage #1: 2-(diphenylmethylthio)acetamide; titanium(IV) isopropylate; diethyl (2S,3S)-tartrate In water; toluene at 55℃; for 0.833333h; Stage #2: With Cumene hydroperoxide; triethylamine In water; toluene at 25℃; for 1h; Product distribution / selectivity; | 90.3% |
Stage #1: 2-(diphenylmethylthio)acetamide; titanium(IV) isopropylate; diethyl (2S,3S)-tartrate In toluene at 55℃; for 0.833333h; Stage #2: With Cumene hydroperoxide; N-ethyl-N,N-diisopropylamine In toluene at 25℃; for 1h; Product distribution / selectivity; | 90.3% |
2-(diphenylmethylthio)acetamide
Conditions | Yield |
---|---|
With dihydrogen peroxide In acetic acid at 40℃; for 6h; | A 95.73% B 0.083% |
With dihydrogen peroxide; acetic acid In methanol; water at 40 - 65℃; for 1 - 28.75h; Product distribution / selectivity; |
2-(diphenylmethylthio)acetamide
2-benzhydrylsulfanylacetonitrile
Conditions | Yield |
---|---|
With (dimethoxy)methylsilane; copper diacetate; 1,2-bis-(dicyclohexylphosphino)ethane In tetrahydrofuran at 20℃; for 12h; Sealed tube; | 77% |
2-(diphenylmethylthio)acetamide
Conditions | Yield |
---|---|
With ε-phthalimido-peroxy-hexanoic acid In dichloromethane at 20℃; for 6h; | 72% |
2-(diphenylmethylthio)acetamide
Conditions | Yield |
---|---|
With Lawessons reagent In 1,4-dioxane for 2h; Reflux; | 62% |
With tetraphosphorus decasulfide; potassium sulfide; toluene | |
With Lawessons reagent |
Conditions | Yield |
---|---|
Stage #1: 2-(diphenylmethylthio)acetamide; titanium(IV) isopropylate; diethyl (2R,3R)-tartrate In dichloromethane; water at -30 - 20℃; for 0.833333h; Stage #2: With Cumene hydroperoxide In dichloromethane; water at -30 - -25℃; for 1.75h; Conversion of starting material; | A 42% B n/a |
Stage #1: 2-(diphenylmethylthio)acetamide; titanium(IV) isopropylate; diethyl (2S,3S)-tartrate In water; ethyl acetate at 25 - 55℃; for 0.166667 - 0.833333h; Stage #2: With Cumene hydroperoxide; triethylamine In water; ethyl acetate at 25 - 55℃; for 0.0833333 - 1h; Product distribution / selectivity; | A n/a B n/a |
Stage #1: 2-(diphenylmethylthio)acetamide; titanium(IV) isopropylate; diethyl (2S,3S)-tartrate In water; ethyl acetate at 55℃; for 0.833333h; Stage #2: With Cumene hydroperoxide In water; ethyl acetate at 25℃; for 1h; Product distribution / selectivity; | A n/a B n/a |
Stage #1: 2-(diphenylmethylthio)acetamide; titanium(IV) isopropylate; diethyl (2S,3S)-tartrate In water; toluene at 55℃; for 0.833333h; Stage #2: With Cumene hydroperoxide In water; toluene at 25℃; for 1h; Product distribution / selectivity; | A n/a B n/a |
2-(diphenylmethylthio)acetamide
2,4,6-tribenzhydrylphenol
Conditions | Yield |
---|---|
With trifluoroacetyl peroxide In trifluoroacetic acid at 10℃; for 0.166667h; Mechanism; | 34% |
2-(diphenylmethylthio)acetamide
Conditions | Yield |
---|---|
With tetraphosphorus decasulfide; potassium sulfide; toluene at 100℃; Erhitzen des Reaktionsprodukts mit Aethylendiamin in Toluol; |
2-(diphenylmethylthio)acetamide
B
modafinil acid
Conditions | Yield |
---|---|
Stage #1: 2-(diphenylmethylthio)acetamide With acetic acid In methanol at 30 - 40℃; for 0.25h; Stage #2: With dihydrogen peroxide In methanol; water at 38 - 43℃; for 24h; Product distribution / selectivity; |
2-(diphenylmethylthio)acetamide
B
modafinil acid
Conditions | Yield |
---|---|
Stage #1: 2-(diphenylmethylthio)acetamide With acetic acid In methanol at 30 - 40℃; for 0.25h; Stage #2: With dihydrogen peroxide In methanol; water at 38 - 43℃; for 24h; Product distribution / selectivity; |
Conditions | Yield |
---|---|
With 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate In tetrachloromethane at 20℃; for 48h; Title compound not separated from byproducts.; | |
With bis(acetylacetonate)oxovanadium; 2,4-di-tert-butyl-6-((E)-(((1R,2S)-2-hydroxy-1,2-diphenylethyl)imino)methyl)phenol; dihydrogen peroxide In chloroform at 20℃; for 3.5h; optical yield given as %ee; enantioselective reaction; | |
With NADP In isopropyl alcohol at 25℃; for 20h; pH=8; Catalytic behavior; Alkaline conditions; enantioselective reaction; | A n/a B n/a |
With tert.-butylhydroperoxide at 20℃; Enzymatic reaction; | |
Stage #1: 2-(diphenylmethylthio)acetamide With iron(III) trifluoromethanesulfonate; C37H56N4O4 In tert-butyl methyl ether at 35℃; for 0.5h; Inert atmosphere; Stage #2: With dihydrogen peroxide In tert-butyl methyl ether; water at 25℃; for 8h; Inert atmosphere; Overall yield = 94 percent; Overall yield = 25.6 mg; enantioselective reaction; | A n/a B n/a |
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