The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine c
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiryPrice, service, company and transport advantage: 1.place of origin china with super quality by reasonable price. 2. it's customers' right to choose the package (ems, dhl, fedex, ups); 3. it's customers' right to
Cas:7540-51-4
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
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inquiryBETA-RHODINOL CAS:7540-51-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediate
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Appearance:off-white to white solid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for Synthesis API and Research Transportation:As customer request Port:Qingda
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:7540-51-4
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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inquiryHigh quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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inquiryWe produce carbomer by our own factory,carbomer 940 is our best seller.It is used for cosmetic and medical.And we also become agent for lubrizol.Our carbomer 940 get high viscosity and good transparency.The price will depond on the market,surely supp
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates
Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
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inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Conditions | Yield |
---|---|
With bis(norbornadiene)rhodium(l)tetrafluoroborate; (RC,SFc,SP)-1-[2-(1-N,N-dimethylaminoethyl)ferrocen-1-yl]phenylphosphino-1'-dicyclohexylphosphinoferrocene; hydrogen In dichloromethane at 20℃; under 19001.3 Torr; for 20h; Inert atmosphere; Autoclave; enantioselective reaction; | 99% |
With [RuCl(p-cymene)((R)-Tol-BINAP)]Cl; potassium hydroxide In isopropyl alcohol for 2h; Inert atmosphere; Reflux; | 70% |
Multi-step reaction with 2 steps 1: in Ficus retusa Linn. 2: in Ficus retusa Linn. nach Injektion View Scheme |
Conditions | Yield |
---|---|
With dichloro(1,5-cyclooctadiene)ruthenium(II); (R)-(+)-2,2',6,6'-tetramethoxy-4,4'-bis(diphenylphosphino)-3,3'-bipyridine; niobium pentachloride; HSiPh3 In toluene at 40℃; for 3h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Glovebox; Sealed tube; Inert atmosphere; enantioselective reaction; | 98.59% |
With (η4-cyclooctadiene)((R)-2,2'-bis(diphenylphosphanyl)-1,1'-binaphthyl)rhodium(I) tetrfluoroborate; hydrogen In methanol at 60℃; under 33753.4 Torr; for 5h; Autoclave; enantioselective reaction; | 88% |
(S)-3,7-dimethyl-6-octen-1-ol
Conditions | Yield |
---|---|
With indium; water; ammonium chloride In methanol for 1h; Heating; | 98% |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In diethyl ether | 96% |
With lithium aluminium tetrahydride In diethyl ether | 94% |
With sodium tetrahydroborate In ethanol at 0℃; | 93% |
(S)-3,7-dimethyl-6-octen-1-ol
Conditions | Yield |
---|---|
With indium; water; ammonium chloride In methanol for 0.5h; Heating; | 95% |
(S)-3,7-dimethyl-6-octen-1-ol
Conditions | Yield |
---|---|
With sodium perborate; water In tetrahydrofuran at 20℃; for 4h; enantioselective reaction; | 95% |
2,2-dimethyl-propionic acid (3S)-3,7-dimethyl-oct-6-enyl ester
(S)-3,7-dimethyl-6-octen-1-ol
Conditions | Yield |
---|---|
With sodium hydroxide In methanol Ambient temperature; | 94% |
(S)-3,7-dimethyl-6-octen-1-ol
Conditions | Yield |
---|---|
Stage #1: (S)-8-(allyloxy)-2,6-dimethyloct-2-ene With C12H37NiP4(1+)*C2F6NO4S2(1-) In tetrahydrofuran at 20℃; for 0.5h; Glovebox; Schlenk technique; Inert atmosphere; Stage #2: With toluene-4-sulfonic acid In tetrahydrofuran for 1.5h; Glovebox; Schlenk technique; Reflux; Inert atmosphere; | 94% |
(S)-3,7-Dimethyl-oct-6-enoic acid (1S,2R,3S,4R)-3-(2,2-dimethyl-propoxy)-4,7,7-trimethyl-bicyclo[2.2.1]hept-2-yl ester
A
(S)-3,7-dimethyl-6-octen-1-ol
B
(1R,2S,3R,4S)-2-(2,2-dimethylpropoxy)-1,7,7-trimethylbicyclo<2.2.1>heptan-3-ol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride | A 88% B 81% |
(S)-((3,7-dimethyloct-6-enyloxy)methyl)benzene
(S)-3,7-dimethyl-6-octen-1-ol
Conditions | Yield |
---|---|
With ammonia; lithium In tetrahydrofuran at -30℃; for 0.666667h; | 82% |
(S)-3,7-dimethyl-6-octen-1-ol
Conditions | Yield |
---|---|
With (PhSO2)2; water In dichloromethane at 80℃; | 82% |
(S)-Citronellal
A
(S)-3,7-dimethyl-6-octen-1-ol
B
(S)-(-)-citronellic acid
Conditions | Yield |
---|---|
With Fusarium concentricum In dimethyl sulfoxide at 28 - 30℃; for 120h; Reagent/catalyst; Microbiological reaction; | A 76% B 5% |
With Fusarium fujikuroi In dimethyl sulfoxide at 28 - 30℃; for 120h; Microbiological reaction; | A 36% B 43% |
With endosperms of Triticum aestivum L. cv Dariel wheat seeds In water at 27℃; Reagent/catalyst; Concentration; Darkness; Enzymatic reaction; enantioselective reaction; |
Conditions | Yield |
---|---|
With 1,1′-binaphthalene-2,2′-diylbis[bis(4-methylphenyl)phosphine]; potassium hydroxide at 100℃; for 2h; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 70% |
With hydrogen; BINAP-Ru(II) dicarboxylate In methanol at 18 - 20℃; Yield given; | |
With hydrogen; BINAP-(Ru(II) dicarboxylate In methanol at 18 - 20℃; Product distribution; examination of enantioselectivity; various complexes; |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 25℃; for 3h; Inert atmosphere; | 69% |
(S)-Citronellal
A
(S)-3,7-dimethyl-6-octen-1-ol
B
(1S,3R,4S)-p-menthane-3,8-diol
D
(−)-neo-isopulegol(−)-neo-isopulegol
Conditions | Yield |
---|---|
With Penicillium paxilli In dimethyl sulfoxide at 28 - 30℃; for 120h; Microbiological reaction; | A 10% B 50% C 20% D 5% E 2% |
(S)-3,7-dimethyl-6-octen-1-ol
Conditions | Yield |
---|---|
With potassium chloride; water In acetone | 48% |
3,7-dimethyl-oct-6-enal
A
(R)-Citronellal
B
(S)-3,7-dimethyl-6-octen-1-ol
Conditions | Yield |
---|---|
With baker's yeast | A 21% B 33% |
(S)-3,7-dimethyl-6-octen-1-ol
Conditions | Yield |
---|---|
With potassium (4-methylphenyl)trifluoroborate In dimethyl sulfoxide at 37℃; for 24h; Inert atmosphere; | 18% |
Conditions | Yield |
---|---|
in Ficus retusa Linn. nach Injektion; |
Conditions | Yield |
---|---|
With hydrogen; <(+)-CyBINAP>-RhN In benzene under 15200 Torr; Ambient temperature; Yield given. Yields of byproduct given; | |
With hydrogen; ClO4 In benzene under 7600 Torr; for 8h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts; | |
With hydrogen; Ru2Cl4-((S)-2,2'-bis[di(p-tolyl)phosphino]-1,1'-binaphthyl)2NEt3 In methanol at 19.9℃; under 1807.6 Torr; Product distribution; different pressure and temperature; | |
With 1,2-bis(2,5-diisopropylphospholano)benzene; potassium hydroxide at 100℃; for 24h; Inert atmosphere; optical yield given as %ee; enantioselective reaction; |
Geraniol
A
(S)-3,7-dimethyl-6-octen-1-ol
B
(3R)-citronellol
C
(R)-3,7-dimethyloctan-1-ol
Conditions | Yield |
---|---|
With hydrogen; {RuI((R)-2,2'-bis(diphenylphospino)-1,1'-binaphthyl)(p-cymene)}I In methanol; water at 20℃; under 76000 Torr; for 8h; Yield given. Yields of byproduct given; |
Conditions | Yield |
---|---|
With <<(-)-2,2'-bis(diphenylphosphino)-4,4',6,6'-tetramethyl-3,3'-bibenzothiophene>Ru(p-cumene)I>I; hydrogen In methanol at 25℃; under 7355.08 Torr; for 88h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; | |
With ((S)-(6,6'-dimethylbiphenyl-2,2'-diyl)bis(diphenylphosphine))Ru(O2CCF3)2; hydrogen In methanol at 20 - 25℃; under 45003.6 Torr; for 1h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; | |
With hydrogen; <(+)-BINAP>RhN In benzene under 22800 Torr; Ambient temperature; Yield given. Yields of byproduct given; |
Conditions | Yield |
---|---|
With lithium triethylborohydride In tetrahydrofuran Ambient temperature; Yield given; | |
With lithium triethylborohydride In tetrahydrofuran Ambient temperature; Yields of byproduct given; |
N,N-diethyl-N-{1-[(3S),7-dimethylocta-1,6-dienyl]}amine
(S)-3,7-dimethyl-6-octen-1-ol
Conditions | Yield |
---|---|
With oxonium; hydrogen |
Conditions | Yield |
---|---|
With sodium hydroxide; sodium tetrahydroborate; 2-methyl-but-2-ene; boron trifluoride; dihydrogen peroxide 1.) THF, room temp., 3 h.; 2.) 50 deg C, 1.5 h; Multistep reaction; |
Conditions | Yield |
---|---|
With Ru2Cl4-((S)-2,2'-bis[di(p-tolyl)phosphino]-1,1'-binaphthyl)2NEt3; hydrogen In methanol at 19.9℃; under 3750.3 Torr; Title compound not separated from byproducts; | |
With hydrogen; Ru2Cl4-((S)-2,2'-bis[di(p-tolyl)phosphino]-1,1'-binaphthyl)2NEt3 In methanol at 19.9℃; under 1807.6 Torr; Product distribution; other pressure and temperature; | |
With 1,1′-binaphthalene-2,2′-diylbis[bis(4-methylphenyl)phosphine]; potassium hydroxide at 100℃; for 6h; Inert atmosphere; optical yield given as %ee; enantioselective reaction; |
(3S)-3,7-dimethyl-6-octen-1-yl acetate
(S)-3,7-dimethyl-6-octen-1-ol
Conditions | Yield |
---|---|
Stage #1: (3S)-3,7-dimethyl-6-octen-1-yl acetate With sodium hydroxide In ethanol at 90℃; for 3h; Alkaline hydrolysis; Stage #2: With Pichia kluyveri IFO 1165 at 30℃; for 48h; |
vinyl acetate
Citronellol
A
(S)-3,7-dimethyl-6-octen-1-ol
B
(3R)-citronellol
C
(R)-1-citronellyl acetate
D
(3S)-3,7-dimethyl-6-octen-1-yl acetate
Conditions | Yield |
---|---|
With porcine pancreatic lipase In hexane for 24h; Title compound not separated from byproducts; | |
With porcine pancreatic lipase In hexane for 48h; Title compound not separated from byproducts; |
Conditions | Yield |
---|---|
With bis(norbornadiene)rhodium(l)tetrafluoroborate; (RC,SFc,SP)-1-[2-(1-N,N-dimethylaminoethyl)ferrocen-1-yl]phenylphosphino-1'-dicyclohexylphosphinoferrocene; hydrogen In dichloromethane at 20℃; under 19001.3 Torr; for 20h; Inert atmosphere; Autoclave; enantioselective reaction; | 99% |
With [RuCl(p-cymene)((R)-Tol-BINAP)]Cl; potassium hydroxide In isopropyl alcohol for 2h; Inert atmosphere; Reflux; | 70% |
Multi-step reaction with 2 steps 1: in Ficus retusa Linn. 2: in Ficus retusa Linn. nach Injektion View Scheme |
Conditions | Yield |
---|---|
With dichloro(1,5-cyclooctadiene)ruthenium(II); (R)-(+)-2,2',6,6'-tetramethoxy-4,4'-bis(diphenylphosphino)-3,3'-bipyridine; niobium pentachloride; HSiPh3 In toluene at 40℃; for 3h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Glovebox; Sealed tube; Inert atmosphere; enantioselective reaction; | 98.59% |
With (η4-cyclooctadiene)((R)-2,2'-bis(diphenylphosphanyl)-1,1'-binaphthyl)rhodium(I) tetrfluoroborate; hydrogen In methanol at 60℃; under 33753.4 Torr; for 5h; Autoclave; enantioselective reaction; | 88% |
(S)-3,7-dimethyl-6-octen-1-ol
Conditions | Yield |
---|---|
With indium; water; ammonium chloride In methanol for 1h; Heating; | 98% |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In diethyl ether | 96% |
With lithium aluminium tetrahydride In diethyl ether | 94% |
With sodium tetrahydroborate In ethanol at 0℃; | 93% |
(S)-3,7-dimethyl-6-octen-1-ol
Conditions | Yield |
---|---|
With indium; water; ammonium chloride In methanol for 0.5h; Heating; | 95% |
(S)-3,7-dimethyl-6-octen-1-ol
Conditions | Yield |
---|---|
With sodium perborate; water In tetrahydrofuran at 20℃; for 4h; enantioselective reaction; | 95% |
2,2-dimethyl-propionic acid (3S)-3,7-dimethyl-oct-6-enyl ester
(S)-3,7-dimethyl-6-octen-1-ol
Conditions | Yield |
---|---|
With sodium hydroxide In methanol Ambient temperature; | 94% |
(S)-3,7-dimethyl-6-octen-1-ol
Conditions | Yield |
---|---|
Stage #1: (S)-8-(allyloxy)-2,6-dimethyloct-2-ene With C12H37NiP4(1+)*C2F6NO4S2(1-) In tetrahydrofuran at 20℃; for 0.5h; Glovebox; Schlenk technique; Inert atmosphere; Stage #2: With toluene-4-sulfonic acid In tetrahydrofuran for 1.5h; Glovebox; Schlenk technique; Reflux; Inert atmosphere; | 94% |
(S)-3,7-Dimethyl-oct-6-enoic acid (1S,2R,3S,4R)-3-(2,2-dimethyl-propoxy)-4,7,7-trimethyl-bicyclo[2.2.1]hept-2-yl ester
A
(S)-3,7-dimethyl-6-octen-1-ol
B
(1R,2S,3R,4S)-2-(2,2-dimethylpropoxy)-1,7,7-trimethylbicyclo<2.2.1>heptan-3-ol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride | A 88% B 81% |
(S)-((3,7-dimethyloct-6-enyloxy)methyl)benzene
(S)-3,7-dimethyl-6-octen-1-ol
Conditions | Yield |
---|---|
With ammonia; lithium In tetrahydrofuran at -30℃; for 0.666667h; | 82% |
(S)-3,7-dimethyl-6-octen-1-ol
Conditions | Yield |
---|---|
With (PhSO2)2; water In dichloromethane at 80℃; | 82% |
(S)-Citronellal
A
(S)-3,7-dimethyl-6-octen-1-ol
B
(S)-(-)-citronellic acid
Conditions | Yield |
---|---|
With Fusarium concentricum In dimethyl sulfoxide at 28 - 30℃; for 120h; Reagent/catalyst; Microbiological reaction; | A 76% B 5% |
With Fusarium fujikuroi In dimethyl sulfoxide at 28 - 30℃; for 120h; Microbiological reaction; | A 36% B 43% |
With endosperms of Triticum aestivum L. cv Dariel wheat seeds In water at 27℃; Reagent/catalyst; Concentration; Darkness; Enzymatic reaction; enantioselective reaction; |
Conditions | Yield |
---|---|
With 1,1′-binaphthalene-2,2′-diylbis[bis(4-methylphenyl)phosphine]; potassium hydroxide at 100℃; for 2h; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 70% |
With hydrogen; BINAP-Ru(II) dicarboxylate In methanol at 18 - 20℃; Yield given; | |
With hydrogen; BINAP-(Ru(II) dicarboxylate In methanol at 18 - 20℃; Product distribution; examination of enantioselectivity; various complexes; |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 25℃; for 3h; Inert atmosphere; | 69% |
(S)-Citronellal
A
(S)-3,7-dimethyl-6-octen-1-ol
B
(1S,3R,4S)-p-menthane-3,8-diol
D
(−)-neo-isopulegol
E
(+)-isopulegol
Conditions | Yield |
---|---|
With Penicillium paxilli In dimethyl sulfoxide at 28 - 30℃; for 120h; Microbiological reaction; | A 10% B 50% C 20% D 5% E 2% |
(S)-3,7-dimethyl-6-octen-1-ol
Conditions | Yield |
---|---|
With potassium chloride; water In acetone | 48% |
3,7-dimethyl-oct-6-enal
A
(R)-Citronellal
B
(S)-3,7-dimethyl-6-octen-1-ol
Conditions | Yield |
---|---|
With baker's yeast | A 21% B 33% |
(S)-3,7-dimethyl-6-octen-1-ol
Conditions | Yield |
---|---|
With potassium (4-methylphenyl)trifluoroborate In dimethyl sulfoxide at 37℃; for 24h; Inert atmosphere; | 18% |
Conditions | Yield |
---|---|
in Ficus retusa Linn. nach Injektion; |
Conditions | Yield |
---|---|
With hydrogen; <(+)-CyBINAP>-RhN In benzene under 15200 Torr; Ambient temperature; Yield given. Yields of byproduct given; | |
With hydrogen; ClO4 In benzene under 7600 Torr; for 8h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts; | |
With hydrogen; Ru2Cl4-((S)-2,2'-bis[di(p-tolyl)phosphino]-1,1'-binaphthyl)2NEt3 In methanol at 19.9℃; under 1807.6 Torr; Product distribution; different pressure and temperature; | |
With 1,2-bis(2,5-diisopropylphospholano)benzene; potassium hydroxide at 100℃; for 24h; Inert atmosphere; optical yield given as %ee; enantioselective reaction; |
Geraniol
A
(S)-3,7-dimethyl-6-octen-1-ol
B
(3R)-citronellol
C
(R)-3,7-dimethyloctan-1-ol
Conditions | Yield |
---|---|
With hydrogen; {RuI((R)-2,2'-bis(diphenylphospino)-1,1'-binaphthyl)(p-cymene)}I In methanol; water at 20℃; under 76000 Torr; for 8h; Yield given. Yields of byproduct given; |
Conditions | Yield |
---|---|
With <<(-)-2,2'-bis(diphenylphosphino)-4,4',6,6'-tetramethyl-3,3'-bibenzothiophene>Ru(p-cumene)I>I; hydrogen In methanol at 25℃; under 7355.08 Torr; for 88h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; | |
With ((S)-(6,6'-dimethylbiphenyl-2,2'-diyl)bis(diphenylphosphine))Ru(O2CCF3)2; hydrogen In methanol at 20 - 25℃; under 45003.6 Torr; for 1h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; | |
With hydrogen; <(+)-BINAP>RhN In benzene under 22800 Torr; Ambient temperature; Yield given. Yields of byproduct given; |
Conditions | Yield |
---|---|
With lithium triethylborohydride In tetrahydrofuran Ambient temperature; Yield given; | |
With lithium triethylborohydride In tetrahydrofuran Ambient temperature; Yields of byproduct given; |
N,N-diethyl-N-{1-[(3S),7-dimethylocta-1,6-dienyl]}amine
(S)-3,7-dimethyl-6-octen-1-ol
Conditions | Yield |
---|---|
With oxonium; hydrogen |
Conditions | Yield |
---|---|
With sodium hydroxide; sodium tetrahydroborate; 2-methyl-but-2-ene; boron trifluoride; dihydrogen peroxide 1.) THF, room temp., 3 h.; 2.) 50 deg C, 1.5 h; Multistep reaction; |
Conditions | Yield |
---|---|
With Ru2Cl4-((S)-2,2'-bis[di(p-tolyl)phosphino]-1,1'-binaphthyl)2NEt3; hydrogen In methanol at 19.9℃; under 3750.3 Torr; Title compound not separated from byproducts; | |
With hydrogen; Ru2Cl4-((S)-2,2'-bis[di(p-tolyl)phosphino]-1,1'-binaphthyl)2NEt3 In methanol at 19.9℃; under 1807.6 Torr; Product distribution; other pressure and temperature; | |
With 1,1′-binaphthalene-2,2′-diylbis[bis(4-methylphenyl)phosphine]; potassium hydroxide at 100℃; for 6h; Inert atmosphere; optical yield given as %ee; enantioselective reaction; |
(3S)-3,7-dimethyl-6-octen-1-yl acetate
(S)-3,7-dimethyl-6-octen-1-ol
Conditions | Yield |
---|---|
Stage #1: (3S)-3,7-dimethyl-6-octen-1-yl acetate With sodium hydroxide In ethanol at 90℃; for 3h; Alkaline hydrolysis; Stage #2: With Pichia kluyveri IFO 1165 at 30℃; for 48h; |
vinyl acetate
Citronellol
A
(S)-3,7-dimethyl-6-octen-1-ol
B
(3R)-citronellol
C
(R)-1-citronellyl acetate
D
(3S)-3,7-dimethyl-6-octen-1-yl acetate
Conditions | Yield |
---|---|
With porcine pancreatic lipase In hexane for 24h; Title compound not separated from byproducts; | |
With porcine pancreatic lipase In hexane for 48h; Title compound not separated from byproducts; |
(S)-3,7-dimethyl-6-octen-1-ol
S-(-)-dihydrocitronellol
Conditions | Yield |
---|---|
With palladium on activated charcoal; hydrogen | 100% |
With palladium on activated charcoal; hydrogen In methanol; ethyl acetate at 25℃; for 18h; Inert atmosphere; | 98% |
With palladium 10% on activated carbon; hydrogen In ethyl acetate at 20℃; for 0.25h; Inert atmosphere; | 96% |
(S)-3,7-dimethyl-6-octen-1-ol
p-toluenesulfonyl chloride
(S)-3,7-dimethyl-6-octenyl tosylate
Conditions | Yield |
---|---|
With pyridine at 0℃; for 12h; Tosylation; | 100% |
With pyridine at 0℃; for 72h; | 100% |
With pyridine | 100% |
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