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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

1,3-Benzenedimethanol, α1,α1,α3,α3-tetrakis(trifluoromethyl)-

Cas:802-93-7

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

1,3-Bis-(hexafluoro-2-hydroxyisopropyl)-benzene

Cas:802-93-7

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

1,3-BIS(2-HYDROXYHEXAFLUOROISOPROPYL)BENZENE from Henan Tianfu Chemical: Henan Tianfu Chemical Co.,LTD was built in 2009 with an ISO certificate in the past 5 years, we have grown up as a famous fine chemicals supplier in china and we had establi

1,3-BIS(2-HYDROXYHEXAFLUOROISOPROPYL)BENZENE

Cas:802-93-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Pharmaceutical Grade CAS 802-93-7 with competitive price

Cas:802-93-7

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

1,3-Benzenedimethanol, α1,α1,α3,α3-tetrakis(trifluoromethyl)- 802-93-7

Cas:802-93-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

1,3-BIS(2-HYDROXYHEXAFLUOROISOPROPYL)BENZENE CAS:802-93-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in hig

1,3-BIS(2-HYDROXYHEXAFLUOROISOPROPYL)BENZENE CAS:802-93-7

Cas:802-93-7

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

1,3-Benzenedimethanol, α1,α1,α3,α3-tetrakis(trifluoromethyl)-

Cas:802-93-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

1,3-Benzenedimethanol, α1,α1,α3,α3-tetrakis(trifluoromethyl)-

Cas:802-93-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Saiwante (shanghai) New Material Technology Co., Ltd.

ProName: 1,3-Benzenedimethanol, α1,α1,α3,α3-tet... CasNo: 802-93-7 Molecular Formula: C12H6F12O2 Appearance: detailed see specifications Application: Used in Synthesis, Pharmaceuticals and... DeliveryTime: prompt PackA

1,3-Benzenedimethanol, α1,α1,α3,α3-tetrakis(trifluoromethyl)-

Cas:802-93-7

Min.Order:1 Gram

FOB Price: $6.0 / 9.0

Type:Trading Company

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply α,α,α',α'-tetrakis(trifluoromethyl)-m-xylene-α,α'-diol

Cas:802-93-7

Min.Order:0 Metric Ton

Negotiable

Type:Other

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

1,3-Benzenedimethanol, α1,α1,α3,α3-tetrakis(trifluoromethyl)-

Cas:802-93-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High Quality 1,3-Benzenedimethanol, a1,a1,a3,a3-tetrakis(trifluoromethyl)

Cas:802-93-7

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

1,1,1,3,3,3-hexafluoro-2-[3-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)phenyl]propan-2-ol

Cas:802-93-7

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

1,1,1,3,3,3-hexafluoro-2-[3-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)phenyl]propan-2-ol

Cas:802-93-7

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

1,3-BIS(2-HYDROXYHEXAFLUOROISOPROPYL)BENZENE

Cas:802-93-7

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

1,1,1,3,3,3-hexafluoro-2-[3-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)phenyl]propan-2-ol

Cas:802-93-7

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

1,1,1,3,3,3-hexafluoro-2-[3-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)phenyl]propan-2-ol

Cas:802-93-7

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

1,3-Bis(2-hydroxyhexafluoroisopropyl)benzene

Cas:802-93-7

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

1,3-BIS(2-HYDROXYHEXAFLUOROISOPROPYL)BENZENE Cas no.802-93-7 98%

Cas:802-93-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

1,1,1,3,3,3-hexafluoro-2-[3-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)phenyl]propan-2-ol

Cas:802-93-7

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

Hebei Mojin Biotechnology Co.,Ltd

1, High quality with competitive price:2, Fast and safe delivery3.Excellent pre-sales and after-sales service4. Well-trained and professional technologist and sales with rich experience in the field for 5-10 yearsAppearance:see detailed specification

1,3-Benzenedimethanol, a1,a1,a3,a3-tetrakis(trifluoromethyl)-

Cas:802-93-7

Min.Order:0

Negotiable

Type:Trading Company

inquiry

GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

1,3-Bis(Hexafluoro-Alpha-Hydroxyisopropyl)Benzene

Cas:802-93-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates

1,3-Benzenedimethanol, a1,a1,a3,a3-tetrakis(trifluoromethyl)-

Cas:802-93-7

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

1,3-Bis(hexafluoro-alpha-hydroxyisopropyl)benzene

Cas:802-93-7

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Wuxi TAA Chemical Industry Co.,LTD.

1.A strong technical force and advanced processing equipments. The quality of the products has been strictly inspected and all kinds of index have reached or exceeded domestic and international standards.2. Now we have established long-term stable re

1,3-Benzenedimethanol, α1,α1,α3,α3-tetrakis(trifluoromethyl)-

Cas:802-93-7

Min.Order:0

Negotiable

Type:Other

inquiry

Xian Changyue Biological Technology Co., Ltd.

best seller Application:API

1,3-BIS(2-HYDROXYHEXAFLUOROISOPROPYL)BENZENE

Cas:802-93-7

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Chemsigma International Co.,Ltd.

bulk productiongoods in stockswe have the best competitive price in the marketmeantime,we are committed to service to our every customer Chemsigma International Co.,Ltd. is a chemical manufacturer, specialize in custom synthesis and organic chemical

1,3-BIS(2-HYDROXYHEXAFLUOROISOPROPYL)BENZENE

Cas:802-93-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages? High purity, all above 98.5%, no impurities after dissolution? We will test each batch to ensure quality? OEM and private brand services designed for free? Various cap colors available? We can also provide MT1 peptide powder2.

1,3-BIS(2-HYDROXYHEXAFLUOROISOPROPYL)BENZENE

Cas:802-93-7

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

α,α,α',α'-Tetrakis(trifluoroMethyl)-1,3-benzenediMethanol

Cas:802-93-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

Hexafluoroacetone
684-16-2

Hexafluoroacetone

benzene
71-43-2

benzene

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

Conditions
ConditionsYield
With aluminium trichloride at 50 - 54℃; for 6h;86%
With aluminum (III) chloride at 51℃; Friedel-Crafts Acylation; Inert atmosphere;70%
Hexafluoroacetone
684-16-2

Hexafluoroacetone

benzene
71-43-2

benzene

A

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

B

1,1,1,3,3,3-hexafluoro-2-phenylisopropyl alcohol
718-64-9

1,1,1,3,3,3-hexafluoro-2-phenylisopropyl alcohol

C

1,1,1,3,3,3-hexafluoro-2-[4-(2,2,2-trifluoro-1-hydroxy-1-(trifluoromethyl)ethyl)-phenyl]-propan-2-ol
1992-15-0

1,1,1,3,3,3-hexafluoro-2-[4-(2,2,2-trifluoro-1-hydroxy-1-(trifluoromethyl)ethyl)-phenyl]-propan-2-ol

Conditions
ConditionsYield
With aluminium trichloride at 50 - 54℃; for 5h;A 54%
B 20%
C 6%
1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

5-Iodo-α,α,α',α'-tetrakis(trifluoromethyl)-1,3-benzenedimethanol
53173-72-1

5-Iodo-α,α,α',α'-tetrakis(trifluoromethyl)-1,3-benzenedimethanol

Conditions
ConditionsYield
With sulfuric acid; iodine for 7h; Ambient temperature;89%
With sulfuric acid; sulfur trioxide; iodine at 70 - 72℃; for 2h;77%
With fuming sulphuric acid; iodine at 70℃; for 2h;70%
Methyl methanesulfonate
66-27-3

Methyl methanesulfonate

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

1,3-bis<1-methoxy-2,2,2-trifluoro-1-(trifluoromethyl)ethyl>benzene
53896-18-7

1,3-bis<1-methoxy-2,2,2-trifluoro-1-(trifluoromethyl)ethyl>benzene

Conditions
ConditionsYield
Stage #1: 1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene With sodium hydride In N,N-dimethyl-formamide at -20 - -10℃;
Stage #2: Methyl methanesulfonate In N,N-dimethyl-formamide at 20℃; for 12h;
81%
4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecan-1-ol
1651-41-8

4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecan-1-ol

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

1,3-bis[1-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyloxy)-2,2,2-trifluoro-1-(trifluoromethyl)ethyl]benzene

1,3-bis[1-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyloxy)-2,2,2-trifluoro-1-(trifluoromethyl)ethyl]benzene

Conditions
ConditionsYield
With triphenylphosphine; diethylazodicarboxylate In various solvent(s) at 20℃; for 1h;61%
1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

dimethyl sulfoxide
67-68-5

dimethyl sulfoxide

1,3-bis(2-hydroxyhexafluoro-2-propyl)benzene DMSO complex

1,3-bis(2-hydroxyhexafluoro-2-propyl)benzene DMSO complex

Conditions
ConditionsYield
at 120 - 125℃; for 5h;43%
1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

A

5-Iodo-α,α,α',α'-tetrakis(trifluoromethyl)-1,3-benzenedimethanol
53173-72-1

5-Iodo-α,α,α',α'-tetrakis(trifluoromethyl)-1,3-benzenedimethanol

B

2,4,6-triiodo-1-(2-hydroxyhexafluoro-2-propyl)benzene

2,4,6-triiodo-1-(2-hydroxyhexafluoro-2-propyl)benzene

Conditions
ConditionsYield
With sulfur trioxide; iodine In sulfuric acid
1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

2,2,2-trifluoroethyl trifluoromethanesulphonate
6226-25-1

2,2,2-trifluoroethyl trifluoromethanesulphonate

1,3-bis[1-(2,2,2-trifluoroethoxy)-2,2,2-trifluoro-1-(trifluoromethyl)ethyl]benzene

1,3-bis[1-(2,2,2-trifluoroethoxy)-2,2,2-trifluoro-1-(trifluoromethyl)ethyl]benzene

Conditions
ConditionsYield
Stage #1: 1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene With sodium hydride In N,N-dimethyl-formamide at -20 - -10℃;
Stage #2: 2,2,2-trifluoroethyl trifluoromethanesulphonate In N,N-dimethyl-formamide at 60℃; for 6h;
1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

1,3-bis(2-hydroxyhexafluoro-2-propyl)benzene DMSO complex

1,3-bis(2-hydroxyhexafluoro-2-propyl)benzene DMSO complex

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 77 percent / H2SO4, SO3, I2 / 2 h / 70 - 72 °C
2: 3.8 g / Cu, 2-iodoheptafluoropropane / 10 h / 135 - 140 °C
View Scheme
1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

1,3-bis(2-hydroxyhexafluoro-2-propyl)-5-(heptafluoro-n-propyl)benzene DMSO complex

1,3-bis(2-hydroxyhexafluoro-2-propyl)-5-(heptafluoro-n-propyl)benzene DMSO complex

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 77 percent / H2SO4, SO3, I2 / 2 h / 70 - 72 °C
2: 87 percent / Cu / 135 - 140 °C
View Scheme
1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

3,5-bis(2-hydroxyhexafluoro-2-propyl)-2',3',4',5',6',-pentafluorobiphenyl DMSO complex

3,5-bis(2-hydroxyhexafluoro-2-propyl)-2',3',4',5',6',-pentafluorobiphenyl DMSO complex

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 77 percent / H2SO4, SO3, I2 / 2 h / 70 - 72 °C
2: 2.5 percent / Cu / 16 h / 145 °C
View Scheme
1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

1,3-bis(2-hydroxyhexafluoro-2-propyl)-5-(tridecafluoro-n-hexyl)benzene DMSO complex

1,3-bis(2-hydroxyhexafluoro-2-propyl)-5-(tridecafluoro-n-hexyl)benzene DMSO complex

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 77 percent / H2SO4, SO3, I2 / 2 h / 70 - 72 °C
2: 78 percent / Cu / 135 - 140 °C
View Scheme
1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

1,3-bis(2-hydroxyhexafluoro-2-propyl)-5-(pentadecafluoro-n-heptyl)benzene DMSO complex

1,3-bis(2-hydroxyhexafluoro-2-propyl)-5-(pentadecafluoro-n-heptyl)benzene DMSO complex

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 77 percent / H2SO4, SO3, I2 / 2 h / 70 - 72 °C
2: 91 percent / Cu / 135 - 140 °C
View Scheme
1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

1,3-bis(2-hydroxyhexafluoro-2-propyl)-5-(heptadecafluoro-n-octyl)benzene DMSO complex

1,3-bis(2-hydroxyhexafluoro-2-propyl)-5-(heptadecafluoro-n-octyl)benzene DMSO complex

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 77 percent / H2SO4, SO3, I2 / 2 h / 70 - 72 °C
2: 88 percent / Cu / 16 h / 120 - 125 °C
View Scheme
1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

3,5-bis<2,2,2-trifluoro-1-(2,2,2-trifluoroethoxy)-1-(trifluoromethyl)ethyl>iodobenzene
144369-52-8

3,5-bis<2,2,2-trifluoro-1-(2,2,2-trifluoroethoxy)-1-(trifluoromethyl)ethyl>iodobenzene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 89 percent / I2, 30percent H2SO4 / 7 h / Ambient temperature
2: 1.) NaH / 1.) DMF, 2.) DMF, 50 deg C, 35 min
View Scheme
ethyl bromide
74-96-4

ethyl bromide

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

C14H10F12O2

C14H10F12O2

Conditions
ConditionsYield
aluminum (III) chloride at 50℃;
1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

3-(triethoxypropyl) isocyanate
24801-88-5

3-(triethoxypropyl) isocyanate

C32H48F12N2O10Si2
813468-12-1

C32H48F12N2O10Si2

Conditions
ConditionsYield
In toluene at 20 - 25℃; for 168h;
1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

methanesulfonyl chloride
124-63-0

methanesulfonyl chloride

1,3-bis-(1-methanesulfonyloxy-1-trifluoromethyl-2,2,2-trifluoro-ethyl)-benzene

1,3-bis-(1-methanesulfonyloxy-1-trifluoromethyl-2,2,2-trifluoro-ethyl)-benzene

Conditions
ConditionsYield
With triethylamine In dichloromethane
1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

Ethanesulfonyl chloride
594-44-5

Ethanesulfonyl chloride

A

1-(1-ethanesulfonyloxy-2,2,2-trifluoro-1-tri-fluoromethylethyl)-3-(2,2,2-trifluoro-1-hydroxy-1-tri-fluoromethylethyl)-benzene

1-(1-ethanesulfonyloxy-2,2,2-trifluoro-1-tri-fluoromethylethyl)-3-(2,2,2-trifluoro-1-hydroxy-1-tri-fluoromethylethyl)-benzene

B

1,3-bis-(1-ethanesulfonyloxy-2,2,2-trifluoro-1-trifluoro-methylethyl)-benzene
161758-96-9

1,3-bis-(1-ethanesulfonyloxy-2,2,2-trifluoro-1-trifluoro-methylethyl)-benzene

Conditions
ConditionsYield
In hexane; N,N-dimethyl-formamide
1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

p-toluenesulfonyl chloride
98-59-9

p-toluenesulfonyl chloride

1,3-bis-[2,2,2-trifluoro-1-(toluene-4-sulfonyloxy)-1-trifluoromethylethyl]-benzene

1,3-bis-[2,2,2-trifluoro-1-(toluene-4-sulfonyloxy)-1-trifluoromethylethyl]-benzene

Conditions
ConditionsYield
In N,N-dimethyl-formamide
1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

4-chlorobenzenesulfonyl chloride
98-60-2

4-chlorobenzenesulfonyl chloride

1,3-bis-[1-(4-chlorobenzenesulfonyloxy)-2,2,2-trifluoro-1-trifluoromethylethyl]-benzene

1,3-bis-[1-(4-chlorobenzenesulfonyloxy)-2,2,2-trifluoro-1-trifluoromethylethyl]-benzene

Conditions
ConditionsYield
In N,N-dimethyl-formamide
triethylene

triethylene

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

acryloyl chloride
814-68-6

acryloyl chloride

1,3-Bis(2-hydroxyhexafluoro-2-propyl)benzene diacrylate
77974-91-5

1,3-Bis(2-hydroxyhexafluoro-2-propyl)benzene diacrylate

Conditions
ConditionsYield
In 1,1,2-Trichloro-1,2,2-trifluoroethane
1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

tetrabutyl-ammonium chloride
1112-67-0

tetrabutyl-ammonium chloride

C12H6F12O2*Cl(1-)*C16H36N(1+)

C12H6F12O2*Cl(1-)*C16H36N(1+)

Conditions
ConditionsYield
In [D3]acetonitrile at 24.84℃;
1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

tetrabutyl-ammonium chloride
1112-67-0

tetrabutyl-ammonium chloride

2C12H6F12O2*2C16H36N(1+)*2Cl(1-)

2C12H6F12O2*2C16H36N(1+)*2Cl(1-)

Conditions
ConditionsYield
In [D3]acetonitrile at 20℃;
1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

tetrabutylammomium bromide
1643-19-2

tetrabutylammomium bromide

C12H6F12O2*Br(1-)*C16H36N(1+)

C12H6F12O2*Br(1-)*C16H36N(1+)

Conditions
ConditionsYield
In [D3]acetonitrile at 24.84℃;
1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

tetrabutylammonium nitrate

tetrabutylammonium nitrate

C12H6F12O2*C16H36N(1+)*NO3(1-)

C12H6F12O2*C16H36N(1+)*NO3(1-)

Conditions
ConditionsYield
In [D3]acetonitrile at 24.84℃;
1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

tetrabutylammonium dihydrogen phosphate

tetrabutylammonium dihydrogen phosphate

C12H6F12O2*C16H36N(1+)*H2O4P(1-)

C12H6F12O2*C16H36N(1+)*H2O4P(1-)

Conditions
ConditionsYield
In [D3]acetonitrile at 24.84℃;
1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene
802-93-7

1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene

tetrabutylammonium acetate
10534-59-5

tetrabutylammonium acetate

C12H6F12O2*C16H36N(1+)*C2H3O2(1-)

C12H6F12O2*C16H36N(1+)*C2H3O2(1-)

Conditions
ConditionsYield
In [D3]acetonitrile at 24.84℃;

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