CAS No.84414-90-4,1-(2,3-DIDEOXY-A-D-GLYCERO-PENT-2-ENOFURANOSYL)THYMINE Suppliers

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1-(2,3-DIDEOXY-A-D-GLYCERO-PENT-2-ENOFURANOSYL)THYMINEAppearance:Off white to slight yellow solid Storage:Stored in shaded, cool and dry places Package:1L 5L 10L 25L bottle Application:pharma intermediate Transportation:Handle with cares to avoid dam

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Synthetic route

: 134660-13-2
1-((2S,3R,5S)-3-Bromo-5-hydroxymethyl-tetrahydro-furan-2-yl)-5-methyl-1H-pyrimidine-2,4-dione

A: 134660-21-2
1-(2,5-anhydro-3-deoxy-α-D-threo-pentofuranosyl)thymine

B: 84414-90-4
1-(2,3-dideoxy-α-D-glycero-pent-2-enofuranosyl)thymine

Conditions

Conditions	Yield
With methanol; sodium methylate for 30h; Heating;	A 50% B 20%

: 5-Methyl-1-((S)-5-trityloxymethyl-2,5-dihydro-furan-2-yl)-1H-pyrimidine-2,4-dione

A: 84414-90-4
1-(2,3-dideoxy-α-D-glycero-pent-2-enofuranosyl)thymine

B: 3056-17-5
stavudin

Conditions

Conditions	Yield
With Dowex R 50W; hydrogen cation In methanol Yield given. Yields of byproduct given;

: 452-51-7, 13046-70-3, 29780-54-9, 36792-87-7, 36792-88-8, 113890-35-0, 113890-38-3
D-2-deoxyribose

: 84414-90-4
1-(2,3-dideoxy-α-D-glycero-pent-2-enofuranosyl)thymine

Conditions

Conditions	Yield
Multi-step reaction with 6 steps 1: conc. HCl / dimethylformamide / Ambient temperature 2: 91 percent / imidazole / CH2Cl2 3: pyridine 4: DBU 5: 8 percent / NBS, 2,4-(trimethylsilyloxy)-6-methyl-pyrimidine, mol sieves 4A / CH2Cl2 / 0 °C 6: Dowex R 50W, H(1+) form / methanol View Scheme
Multi-step reaction with 6 steps 1: conc. HCl / dimethylformamide / Ambient temperature 2: 91 percent / imidazole / CH2Cl2 3: pyridine 4: DBU 5: 83 percent / NBS, mol. sieves 4A / CH2Cl2 / -78 °C 6: Dowex R 50W, H(1+) form / methanol View Scheme
Multi-step reaction with 6 steps 1: conc. HCl / Ambient temperature 2: 91 percent / imidazole / CH2Cl2 3: pyridine 4: DBU 5: 8 percent / NBS, 2,4-(trimethylsilyloxy)-6-methyl-pyrimidine, mol sieves 4A / CH2Cl2 / 0 °C 6: Dowex R 50W, H(1+) form / methanol View Scheme
Multi-step reaction with 6 steps 1: conc. HCl / Ambient temperature 2: 91 percent / imidazole / CH2Cl2 3: pyridine 4: DBU 5: 83 percent / NBS, mol. sieves 4A / CH2Cl2 / -78 °C 6: Dowex R 50W, H(1+) form / methanol View Scheme

: 183075-04-9
phenyl 2-deoxy-1-thio-D-erythro-pentofuranoside

: 84414-90-4
1-(2,3-dideoxy-α-D-glycero-pent-2-enofuranosyl)thymine

Conditions

Conditions	Yield
Multi-step reaction with 5 steps 1: 91 percent / imidazole / CH2Cl2 2: pyridine 3: DBU 4: 8 percent / NBS, 2,4-(trimethylsilyloxy)-6-methyl-pyrimidine, mol sieves 4A / CH2Cl2 / 0 °C 5: Dowex R 50W, H(1+) form / methanol View Scheme
Multi-step reaction with 5 steps 1: 91 percent / imidazole / CH2Cl2 2: pyridine 3: DBU 4: 83 percent / NBS, mol. sieves 4A / CH2Cl2 / -78 °C 5: Dowex R 50W, H(1+) form / methanol View Scheme

: 182957-26-2
(2R,3S)-5-Phenylsulfanyl-2-trityloxymethyl-tetrahydro-furan-3-ol

: 84414-90-4
1-(2,3-dideoxy-α-D-glycero-pent-2-enofuranosyl)thymine

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: pyridine 2: DBU 3: 8 percent / NBS, 2,4-(trimethylsilyloxy)-6-methyl-pyrimidine, mol sieves 4A / CH2Cl2 / 0 °C 4: Dowex R 50W, H(1+) form / methanol View Scheme
Multi-step reaction with 4 steps 1: pyridine 2: DBU 3: 83 percent / NBS, mol. sieves 4A / CH2Cl2 / -78 °C 4: Dowex R 50W, H(1+) form / methanol View Scheme

: Trifluoro-methanesulfonic acid (2R,3S)-5-phenylsulfanyl-2-trityloxymethyl-tetrahydro-furan-3-yl ester

: 84414-90-4
1-(2,3-dideoxy-α-D-glycero-pent-2-enofuranosyl)thymine

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: DBU 2: 8 percent / NBS, 2,4-(trimethylsilyloxy)-6-methyl-pyrimidine, mol sieves 4A / CH2Cl2 / 0 °C 3: Dowex R 50W, H(1+) form / methanol View Scheme
Multi-step reaction with 3 steps 1: DBU 2: 83 percent / NBS, mol. sieves 4A / CH2Cl2 / -78 °C 3: Dowex R 50W, H(1+) form / methanol View Scheme

: 190725-02-1
(S)-2-Phenylsulfanyl-5-trityloxymethyl-2,5-dihydro-furan

: 84414-90-4
1-(2,3-dideoxy-α-D-glycero-pent-2-enofuranosyl)thymine

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 8 percent / NBS, 2,4-(trimethylsilyloxy)-6-methyl-pyrimidine, mol sieves 4A / CH2Cl2 / 0 °C 2: Dowex R 50W, H(1+) form / methanol View Scheme
Multi-step reaction with 2 steps 1: 83 percent / NBS, mol. sieves 4A / CH2Cl2 / -78 °C 2: Dowex R 50W, H(1+) form / methanol View Scheme

: (2R,5S)-2-Phenylsulfanyl-5-trityloxymethyl-2,5-dihydro-furan

: 84414-90-4
1-(2,3-dideoxy-α-D-glycero-pent-2-enofuranosyl)thymine

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 72 percent / NBS, mol. sieves 4A / CH2Cl2 / -78 °C 2: Dowex R 50W, H(1+) form / methanol View Scheme

: (2S,5S)-2-Phenylsulfanyl-5-trityloxymethyl-2,5-dihydro-furan

: 84414-90-4
1-(2,3-dideoxy-α-D-glycero-pent-2-enofuranosyl)thymine

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 98 percent / NBS, mol. sieves 4A / CH2Cl2 / -78 °C 2: Dowex R 50W, H(1+) form / methanol View Scheme

: 7288-28-0
2,4-bis(trimethylsiloxy)-5-methylpyrimidine

: 84414-90-4
1-(2,3-dideoxy-α-D-glycero-pent-2-enofuranosyl)thymine

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 83 percent / NBS, mol. sieves 4A / CH2Cl2 / -78 °C 2: Dowex R 50W, H(1+) form / methanol View Scheme
Multi-step reaction with 2 steps 1: 72 percent / NBS, mol. sieves 4A / CH2Cl2 / -78 °C 2: Dowex R 50W, H(1+) form / methanol View Scheme
Multi-step reaction with 2 steps 1: 98 percent / NBS, mol. sieves 4A / CH2Cl2 / -78 °C 2: Dowex R 50W, H(1+) form / methanol View Scheme

: 133635-44-6
methyl 2,3-dideoxy-5-O-(4-methylbenzoyl)-D-glycero-pentofuranoside

: 84414-90-4
1-(2,3-dideoxy-α-D-glycero-pent-2-enofuranosyl)thymine

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: 60 percent / Br2, CaCO3 / diethyl ether / 1 h / Heating 2: 68 percent / trimethylsilyl triflate / acetonitrile / 24 h 3: 30 percent / NaOMe, MeOH / 3 h / Ambient temperature 4: 20 percent / NaOMe, MeOH / 30 h / Heating View Scheme

: 134660-06-3
methyl 2-bromo-2,3-dideoxy-5-O-(4-methylbenzoyl)-D-erythropentofuranoside

: 84414-90-4
1-(2,3-dideoxy-α-D-glycero-pent-2-enofuranosyl)thymine

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 68 percent / trimethylsilyl triflate / acetonitrile / 24 h 2: 30 percent / NaOMe, MeOH / 3 h / Ambient temperature 3: 20 percent / NaOMe, MeOH / 30 h / Heating View Scheme

: 134660-10-9, 134660-42-7
4-Methyl-benzoic acid (2S,4R)-4-bromo-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester

: 84414-90-4
1-(2,3-dideoxy-α-D-glycero-pent-2-enofuranosyl)thymine

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 30 percent / NaOMe, MeOH / 3 h / Ambient temperature 2: 20 percent / NaOMe, MeOH / 30 h / Heating View Scheme

: 84414-90-4
1-(2,3-dideoxy-α-D-glycero-pent-2-enofuranosyl)thymine

: 1-(2,3-didehydro-2,3-dideoxy-β-d-pentofuranosyl-4-carboxy)thymine

Conditions

Conditions	Yield
With ruthenium(III) chloride trihydrate; potassium persulfate; potassium hydroxide at 20℃; for 8h;	50%

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