img height Storage:Store in dry, dark and ventilated place. Package:according to the clients requirement Application:It is an important raw material and intermediate used in Organic Synthesis, Pharmaceuticals, Agrochemicals and Dyestuff. Transporta
Cas:93-83-4
Min.Order:1 Gram
Negotiable
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inquiryAbout Product Details N,N-DIETHANOLOLEAMIDE Basic information Product Name: N,N-DIETHAN
Cas:93-83-4
Min.Order:1 Kilogram
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Type:Lab/Research institutions
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inquiryN,N-DIETHANOLOLEAMIDE Basic information Product Name: N,N-DIETHANOLOLEAMIDE Synonyms: N,N-DIETHANOLOLEAMIDE;OLEIC DIETHANOLAMIDE;OLEIC ACID DIETHANOLAMIDE;(9Z)-N,N-
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Min.Order:1 Kilogram
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(Z)-9-octadecenoyl chloride
2,2'-iminobis[ethanol]
N,N-bis(2-hydroxyethyl)-oleamide
Conditions | Yield |
---|---|
In methanol; diethyl ether; water | 75% |
In dichloromethane at -40 - -10℃; Inert atmosphere; | 75.5% |
With dmap; triethylamine In dichloromethane at 0 - 20℃; |
cis-Octadecenoic acid
2,2'-iminobis[ethanol]
N,N-bis(2-hydroxyethyl)-oleamide
Conditions | Yield |
---|---|
Stage #1: cis-Octadecenoic acid With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 2h; Stage #2: 2,2'-iminobis[ethanol] In dichloromethane at 20℃; for 18h; | 58.2% |
With Candida antarctica lipase In acetonitrile at 60℃; for 24h; | 23% |
With Candida antarctica lipase In acetonitrile at 50℃; for 24h; Kinetics; | 12.1% |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 21 °C / Inert atmosphere 2: dichloromethane / -40 - -10 °C / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
With potassium hydroxide at 160℃; for 4h; Temperature; |
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 0 - 20℃; | 81% |
Conditions | Yield |
---|---|
Stage #1: 3,4,5-tribenzyloxybenzoic acid With dmap; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In dichloromethane at 20℃; for 0.5h; Stage #2: N,N-bis(2-hydroxyethyl)-oleamide In dichloromethane at 20℃; | 66% |
N,N-bis(2-hydroxyethyl)-oleamide
A
cis-Octadecenoic acid
B
2,2'-iminobis[ethanol]
Conditions | Yield |
---|---|
With Candida antarctica lipase In acetonitrile at 50℃; for 24h; Kinetics; |
N,N-bis(2-hydroxyethyl)-oleamide
pivaloyl chloride
N,n-bis(2-trimethylacetoxyethyl)oleamide
Conditions | Yield |
---|---|
With tetrabutyl-ammonium chloride; sodium hydroxide In water at 0 - 20℃; for 12.5h; |
Conditions | Yield |
---|---|
In water at 95℃; for 1h; Inert atmosphere; |
N,N-bis(2-hydroxyethyl)-oleamide
Conditions | Yield |
---|---|
at 120℃; under 15.0015 Torr; for 7h; | 905 g |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; dmap / dichloromethane / 0.5 h / 20 °C 1.2: 20 °C 2.1: hydrogen; palladium 10% on activated carbon / methanol; tetrahydrofuran / 30 °C View Scheme |
Conditions | Yield |
---|---|
Stage #1: N,N-bis(2-hydroxyethyl)-oleamide With sodium hydride In tetrahydrofuran at 60℃; for 1h; Inert atmosphere; Stage #2: N-(2-bromoethyl)morpholine In tetrahydrofuran at 60℃; for 16h; Inert atmosphere; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium hydride / tetrahydrofuran / 1 h / 60 °C / Inert atmosphere 1.2: 16 h / 60 °C / Inert atmosphere 2.1: hydrogen; palladium on activated charcoal / methanol / 18 h / 20 °C View Scheme |
Conditions | Yield |
---|---|
Stage #1: pyridine-4-methanol With methanesulfonyl chloride; triethylamine In tetrahydrofuran at 0℃; for 1h; Stage #2: N,N-bis(2-hydroxyethyl)-oleamide With sodium hydride In tetrahydrofuran at 0 - 60℃; Inert atmosphere; |
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