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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

Iopanoic acid Manufacturer/High quality/Best price/In stock

Cas:96-83-3

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Factory Price API 99% Iopanoic acid 96-83-3 GMP Manufacturer

Cas:96-83-3

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Iopanoic acid

Cas:96-83-3

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con

96-83-3 Iopanoic acid

Cas:96-83-3

Min.Order:1 Kilogram

FOB Price: $15.0 / 50.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Manufacturer supply CAS 96-83-3 with best quality

Cas:96-83-3

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Iopanoic acid

Cas:96-83-3

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Hangzhou Sartort Biopharma Co., Ltd

Appearance:Light brown neat Storage:room temperature Package:25kg/drum Application:Iodopanoic Acid is an iodine-containing radiocontrast medium used in cholecystography. Iodopanoic Acid is a potent inhibitor of thyroid hormone release from thyroid

Iopanoic acid with high quality

Cas:96-83-3

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

Benzenepropanoic acid,3-amino-a-ethyl-2,4,6-triiodo-

Cas:96-83-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Benzenepropanoic acid,3-amino-a-ethyl-2,4,6-triiodo-

Cas:96-83-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Benzenepropanoic acid,3-amino-a-ethyl-2,4,6-triiodo-

Cas:96-83-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply iopanoic acid

Cas:96-83-3

Min.Order:0 Metric Ton

Negotiable

Type:Other

inquiry

SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

Iopanoic acid

Cas:96-83-3

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

inquiry

TaiChem Taizhou Limited

Established in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site

Iopanoic acid

Cas:96-83-3

Min.Order:10 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung, LG, Merck, Thermo Fisher Scientific and so o

96-83-3

Cas:96-83-3

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

Iopanoic acid

Cas:96-83-3

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

Iopanoic acid

Cas:96-83-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

Iopanoic acid

Cas:96-83-3

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

Iopanoic acid

Cas:96-83-3

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

Lactobionic acid

Cas:96-83-3

Min.Order:0

Negotiable

Type:Other

inquiry

GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier

Iopanoec acid

Cas:96-83-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Sinoway Industrial Co., Ltd.

Why is SINOWAY:1) Specialized in pharmaceutical and healthcare industrial since 19872) ISO 9001:2015 & SGS audited supplier . 3) Accept various payment terms : T.T 30-60 days.4) We have warehouse in USA with quickly shipment . Application:API

99% up by HPLC Iopanoic acid 96-83-3

Cas:96-83-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

DB BIOTECH CO., LTD

Q1: Are you a manufacturer Answer: Yes, we are factory founded on 2012.Q2: How to contact with us Click "contact supplier" And then send us message the product you interest in, you will get reply within 12 hours.Q3:Which kind of payment terms do you

Iopanoic acid

Cas:96-83-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

Iopanoic Acid

Cas:96-83-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Henan Sinotech Import&Export Corporation

Appearance:White powder Storage:Store in cool and dry place, away from sun light. Package:drum Application:Diagnostic aid(radiopaque medium-Cholecystographic) Transportation:By sea or by air Port:Qingdao Port

Iopanoic acid

Cas:96-83-3

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

inquiry

Hangzhou Huarong Pharm Co., Ltd.

High qualityAppearance:White powder Storage:Room temperature Package:Aluminum bag Application:Used in producing API Transportation:By air Port:Beijing

Iopanoic Acid

Cas:96-83-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages? High purity, all above 98.5%, no impurities after dissolution? We will test each batch to ensure quality? OEM and private brand services designed for free? Various cap colors available? We can also provide MT1 peptide powder2.

Iopanoic acid

Cas:96-83-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

Benzenepropanoic acid,3-amino-a-ethyl-2,4,6-triiodo-

Cas:96-83-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Ocean Chemical Co., Ltd.

★.Best quality according to requirement ★.Competitive price in China market ★.Mature Technical support ★.Professional logistic support

Iopanoic acid

Cas:96-83-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

We are a trading company aiming at providing high-quality services to customers. Established for many years, with good reputation in the industry Storage:Sealed and preserved Application:Fine chemical intermediates, used as the main raw material for

Iopanoic acid

Cas:96-83-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hubei Langyou International Trading Co., Ltd

Iopanoic acid Application:Iopanoic acid

Iopanoic acid

Cas:96-83-3

Min.Order:0

Negotiable

Type:Other

inquiry

Synthetic route

2-(3-amino-benzyl)-butyric acid
16623-25-9

2-(3-amino-benzyl)-butyric acid

iopanoic acid
96-83-3

iopanoic acid

Conditions
ConditionsYield
With hydrogenchloride; Iodine monochloride
2-(3-Nitro-benzyliden)-buttersaeure
5253-02-1

2-(3-Nitro-benzyliden)-buttersaeure

iopanoic acid
96-83-3

iopanoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Raney nickel; sodium hydroxide; diethyl ether / Hydrogenation
2: iodine monochloride; aqueous hydrochloric acid
View Scheme
dehydroepiandrosterone
53-43-0

dehydroepiandrosterone

iopanoic acid
96-83-3

iopanoic acid

dehydroepiandrosterone iopanoate
83172-20-7

dehydroepiandrosterone iopanoate

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane Ambient temperature;98%
iopanoic acid
96-83-3

iopanoic acid

chloroacetyl chloride
79-04-9

chloroacetyl chloride

3-<(chloroacetyl)amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid
80980-80-9

3-<(chloroacetyl)amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid

Conditions
ConditionsYield
With ISOPROPYLAMIDE for 0.5h; Ambient temperature;95%
With hydrogenchloride; sodium hydroxide In water; 2,4-dichlorophenoxyacetic acid dimethylamine95.3%
cholesterol
57-88-5

cholesterol

iopanoic acid
96-83-3

iopanoic acid

cholesteryl iopanoate
83172-18-3

cholesteryl iopanoate

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane Ambient temperature;95%
With sodium hydride; 1,1'-carbonyldiimidazole 1) THF, reflux, 10 min; 2) THF, room temperature, 1 h; Yield given. Multistep reaction;
Pregnenolone
145-13-1

Pregnenolone

iopanoic acid
96-83-3

iopanoic acid

pregnenolone iopanoate
83172-19-4

pregnenolone iopanoate

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane Ambient temperature;93%
1,3-dihydroxyacetone dimer
62147-49-3

1,3-dihydroxyacetone dimer

iopanoic acid
96-83-3

iopanoic acid

1,3-dihydroxypropan-2-one 1,3-diiopanoate
103959-66-6

1,3-dihydroxypropan-2-one 1,3-diiopanoate

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane for 66h;85%
ethanol
64-17-5

ethanol

iopanoic acid
96-83-3

iopanoic acid

(+/-)-iopanoic acid ethyl ester
100850-30-4

(+/-)-iopanoic acid ethyl ester

Conditions
ConditionsYield
With thionyl chloride for 3h; Heating;82.4%
oxalyl dichloride
79-37-8

oxalyl dichloride

6-<(chloroacetyl)amino>hexanoic acid
61435-75-4

6-<(chloroacetyl)amino>hexanoic acid

iopanoic acid
96-83-3

iopanoic acid

3-<<6-<(chloroacetyl)amino>-1-oxohexyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid
160982-41-2

3-<<6-<(chloroacetyl)amino>-1-oxohexyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid

Conditions
ConditionsYield
With pyridine; hydrogenchloride In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile79%
iopanoic acid
96-83-3

iopanoic acid

1-palmitoyl-3-O-trityl-rac-glycerol
69256-58-2

1-palmitoyl-3-O-trityl-rac-glycerol

1-palmitoyl-2-iopanoyl-3-O-trityl-rac-glycerol

1-palmitoyl-2-iopanoyl-3-O-trityl-rac-glycerol

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane Ambient temperature;60%
iopanoic acid
96-83-3

iopanoic acid

2-oleoylglycerol 1,3-bis

2-oleoylglycerol 1,3-bis

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane for 72h; Ambient temperature;53%
rac-1-monopalmitoylglycerol
305847-08-9

rac-1-monopalmitoylglycerol

iopanoic acid
96-83-3

iopanoic acid

1-palmitoyl-3-iopanoyl-rac-glycerol

1-palmitoyl-3-iopanoyl-rac-glycerol

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane49%
iopanoic acid
96-83-3

iopanoic acid

glyceryl 1,3-diiopanoate
103980-81-0

glyceryl 1,3-diiopanoate

glyceryl 1,2,3-triiopanoate
103959-76-8

glyceryl 1,2,3-triiopanoate

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane Ambient temperature;34%
4-morpholinecarboxaldehyde
4394-85-8

4-morpholinecarboxaldehyde

iopanoic acid
96-83-3

iopanoic acid

2-(2,4,6-triiodo-3-morpholin-4-ylmethyleneamino-benzyl)-butyric acid
101286-38-8

2-(2,4,6-triiodo-3-morpholin-4-ylmethyleneamino-benzyl)-butyric acid

Conditions
ConditionsYield
With trichlorophosphate
iopanoic acid
96-83-3

iopanoic acid

ω-(2,4,6-triiodophenyl)-α-ethyl-propionic acid
51374-95-9

ω-(2,4,6-triiodophenyl)-α-ethyl-propionic acid

Conditions
ConditionsYield
With sulfuric acid; copper; sodium nitrite 1) glac. AcOH, 12 deg C, 45 min, 2) glac. AcOH, MeOH, 20 deg C, 30 min.; Yield given. Multistep reaction;
6-<(chloroacetyl)amino>hexanoic acid
61435-75-4

6-<(chloroacetyl)amino>hexanoic acid

iopanoic acid
96-83-3

iopanoic acid

3-<<6-<(chloroacetyl)amino>-1-oxohexyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid
160982-41-2

3-<<6-<(chloroacetyl)amino>-1-oxohexyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid

Conditions
ConditionsYield
With pyridine; oxalyl dichloride 1.) DMF, CH2Cl2, 5 deg C, 1 h, 2.) THF, CH3CN, 5 deg C, then 40 deg C, 2 h, 3.) THF, reflux, 3 h; Yield given. Multistep reaction;
iopanoic acid
96-83-3

iopanoic acid

3-<<6-<<<2-<(2-aminoethyl)amino>ethyl>amino>acetylamino>-1-oxoethyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid
160982-42-3

3-<<6-<<<2-<(2-aminoethyl)amino>ethyl>amino>acetylamino>-1-oxoethyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1.) oxalyl dichloride, 2.) pyridine / 1.) DMF, CH2Cl2, 5 deg C, 1 h, 2.) THF, CH3CN, 5 deg C, then 40 deg C, 2 h, 3.) THF, reflux, 3 h
2: 48 percent / 6 h / 50 °C
View Scheme
iopanoic acid
96-83-3

iopanoic acid

α-ethyl-2,4,6-triiodo-3-<<1-oxo-6-<<(1,4,7,10-tetraazacyclododec-1-yl)acetyl>amino>hexyl>amino>benzenepropanoic acid
175732-28-2

α-ethyl-2,4,6-triiodo-3-<<1-oxo-6-<<(1,4,7,10-tetraazacyclododec-1-yl)acetyl>amino>hexyl>amino>benzenepropanoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1.) oxalyl dichloride, 2.) pyridine / 1.) DMF, CH2Cl2, 5 deg C, 1 h, 2.) THF, CH3CN, 5 deg C, then 40 deg C, 2 h, 3.) THF, reflux, 3 h
2: 59 percent / dimethylacetamide / 0.5 h / 70 °C
View Scheme
iopanoic acid
96-83-3

iopanoic acid

3-<<<2-<(2-aminoethyl)amino>ethyl>amino>acetylamino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid

3-<<<2-<(2-aminoethyl)amino>ethyl>amino>acetylamino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 95 percent / dimethylacetamide / 0.5 h / Ambient temperature
2: 57 percent / 2.) conc. HCl / 3 h / 50 °C
View Scheme
iopanoic acid
96-83-3

iopanoic acid

10-<2-<<3-(2-carboxybutyl)-2,4,6-triiodophenyl>amino>-2-oxoethyl>-1,4,7,10-tetraazacyclododecane-1,4,7-triacetic acid

10-<2-<<3-(2-carboxybutyl)-2,4,6-triiodophenyl>amino>-2-oxoethyl>-1,4,7,10-tetraazacyclododecane-1,4,7-triacetic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 95 percent / dimethylacetamide / 0.5 h / Ambient temperature
2: 60 percent / 1.) dimethylacetamide, 2.) HCl / 1.5 h / 60 °C
3: 13 percent / 2N NaOH / H2O / 20 h / 50 °C / pH = 10
View Scheme
iopanoic acid
96-83-3

iopanoic acid

3-<<<<2-<<2-ethyl>(carboxymethyl)amino>ethyl>(carboxymethyl)amino>acetyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid

3-<<<<2-<<2-ethyl>(carboxymethyl)amino>ethyl>(carboxymethyl)amino>acetyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 95 percent / dimethylacetamide / 0.5 h / Ambient temperature
2: 57 percent / 2.) conc. HCl / 3 h / 50 °C
3: 33 percent / 10N NaOH / H2O / 20 h / Ambient temperature; pH = 10
View Scheme
iopanoic acid
96-83-3

iopanoic acid

α-ethyl-2,4,6-triiodo-3-<<(1,4,7,10-tetraazacyclododec-1-yl)acetyl>amino>benzenepropanoic acid trishydrochloride

α-ethyl-2,4,6-triiodo-3-<<(1,4,7,10-tetraazacyclododec-1-yl)acetyl>amino>benzenepropanoic acid trishydrochloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 95 percent / dimethylacetamide / 0.5 h / Ambient temperature
2: 60 percent / 1.) dimethylacetamide, 2.) HCl / 1.5 h / 60 °C
View Scheme
iopanoic acid
96-83-3

iopanoic acid

10-<2-<<6-<<3-(2-carboxybutyl)-2,4,6-triiodophenyl>amino>-6-oxohexyl>amino>-2-oxoethyl>-1,4,7,10-tetraazacyclododecane-1,4,7-triacetic acid

10-<2-<<6-<<3-(2-carboxybutyl)-2,4,6-triiodophenyl>amino>-6-oxohexyl>amino>-2-oxoethyl>-1,4,7,10-tetraazacyclododecane-1,4,7-triacetic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1.) oxalyl dichloride, 2.) pyridine / 1.) DMF, CH2Cl2, 5 deg C, 1 h, 2.) THF, CH3CN, 5 deg C, then 40 deg C, 2 h, 3.) THF, reflux, 3 h
2: 59 percent / dimethylacetamide / 0.5 h / 70 °C
3: 48 percent / 10N NaOH / H2O; ethanol / 18 h / Ambient temperature; pH = 9
View Scheme
iopanoic acid
96-83-3

iopanoic acid

18-<<3-(2-carboxybutyl)-2,4,6-triiodophenyl>amino>-3,6,9-tris(carboxymethyl)-11,18-dioxo-3,6,9,12-tetraazaoctadecanoic acid

18-<<3-(2-carboxybutyl)-2,4,6-triiodophenyl>amino>-3,6,9-tris(carboxymethyl)-11,18-dioxo-3,6,9,12-tetraazaoctadecanoic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1.) oxalyl dichloride, 2.) pyridine / 1.) DMF, CH2Cl2, 5 deg C, 1 h, 2.) THF, CH3CN, 5 deg C, then 40 deg C, 2 h, 3.) THF, reflux, 3 h
2: 48 percent / 6 h / 50 °C
3: 41 percent / 10N NaOH / H2O / 3 h / 50 °C / pH = 10
View Scheme
iopanoic acid
96-83-3

iopanoic acid

1-palmitoyl-2-iopanoyl-rac-glycerol

1-palmitoyl-2-iopanoyl-rac-glycerol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 60 percent / 4-(dimethylamino)pyridine, dicyclohexylcarbodiimide / CH2Cl2 / Ambient temperature
2: 97 percent / 10 percent H3BO3/ silica gel / petroleum ether; diethyl ether
View Scheme
iopanoic acid
96-83-3

iopanoic acid

pregnenolone<ω-(2,4,6-triiodophenyl)-α-ethyl>-propionate

pregnenolone<ω-(2,4,6-triiodophenyl)-α-ethyl>-propionate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1) NaNO2, conc. H2SO4, 2) Cu powder / 1) glac. AcOH, 12 deg C, 45 min, 2) glac. AcOH, MeOH, 20 deg C, 30 min.
2: 79 percent / dicyclohexylcarbodiimide, 4-dimethylaminopyridine / CH2Cl2 / 24 h / Ambient temperature
View Scheme
iopanoic acid
96-83-3

iopanoic acid

cholesteryl<ω-(2,4,6-triiodophenyl)-α-ethyl>-propionate

cholesteryl<ω-(2,4,6-triiodophenyl)-α-ethyl>-propionate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1) NaNO2, conc. H2SO4, 2) Cu powder / 1) glac. AcOH, 12 deg C, 45 min, 2) glac. AcOH, MeOH, 20 deg C, 30 min.
2: 75 percent / dicyclohexylcarbodiimide, 4-dimethylaminopyridine / CH2Cl2 / 24 h / Ambient temperature
View Scheme
iopanoic acid
96-83-3

iopanoic acid

glyceryl 1,3-diiopanoate
103980-81-0

glyceryl 1,3-diiopanoate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 85 percent / 4-dimethylaminopyridine (DMAP), 1,3-dicyclohexylcarbodiimide (DCC) / CH2Cl2 / 66 h
2: 75 percent / NaBH4 / tetrahydrofuran; benzene; H2O / 0.5 h / 5 °C
View Scheme
iopanoic acid
96-83-3

iopanoic acid

2-palmitoylglycerol 1,3-diiopanoate
103959-73-5

2-palmitoylglycerol 1,3-diiopanoate

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 85 percent / 4-dimethylaminopyridine (DMAP), 1,3-dicyclohexylcarbodiimide (DCC) / CH2Cl2 / 66 h
2: 75 percent / NaBH4 / tetrahydrofuran; benzene; H2O / 0.5 h / 5 °C
3: 75 percent / 4-dimethylaminopyridine (DMAP), 1,3-dicyclohexylcarbodiimide (DCC) / CH2Cl2 / 66 h
View Scheme
iopanoic acid
96-83-3

iopanoic acid

glyceryl 1,2,3-triiopanoate
103959-76-8

glyceryl 1,2,3-triiopanoate

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 85 percent / 4-dimethylaminopyridine (DMAP), 1,3-dicyclohexylcarbodiimide (DCC) / CH2Cl2 / 66 h
2: 75 percent / NaBH4 / tetrahydrofuran; benzene; H2O / 0.5 h / 5 °C
3: 34 percent / 4-dimethylaminopyridine (DMAP), 1,3-dicyclohexylcarbodiimide (DCC) / CH2Cl2 / Ambient temperature
View Scheme

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