2-methoxyethyl 2-bromoacetate
2-Bromoacetyl bromide
ethane-1,2-diyl bis(2-bromoacetate)
Conditions | Yield |
---|---|
at 70℃; for 24h; | 88% |
Conditions | Yield |
---|---|
In neat (no solvent) at 80℃; for 48h; Inert atmosphere; | 68% |
With sulfuric acid at 125℃; for 12h; |
ethylene glycol
2-Bromoacetyl bromide
ethane-1,2-diyl bis(2-bromoacetate)
Conditions | Yield |
---|---|
With pyridine In diethyl ether; toluene at 20℃; Esterification; | 62% |
With triethylamine In toluene at 23℃; for 18h; | |
With pyridine; dmap In dichloromethane at -0.01℃; for 12h; Inert atmosphere; |
bromoacetic anhydride
ethylene glycol
ethane-1,2-diyl bis(2-bromoacetate)
Conditions | Yield |
---|---|
at 80 - 85℃; |
Conditions | Yield |
---|---|
With xylene |
ethylene glycol
2-Bromoacetyl bromide
A
ethane-1,2-diyl bis(2-bromoacetate)
Conditions | Yield |
---|---|
at 50 - 60℃; |
ethane-1,2-diyl bis(2-bromoacetate)
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
With potassium hydrogencarbonate In ethanol at 50 - 55℃; Inert atmosphere; | 94% |
ethane-1,2-diyl bis(2-bromoacetate)
Conditions | Yield |
---|---|
In acetone the bromo-compd. is added to a soln. of the starting complex in acetone; ppt. is filtd., washed with ether, dried under vac., elem. anal.; | 61% |
dimethyl(2,2'-bipyridine)platinum(II)
ethane-1,2-diyl bis(2-bromoacetate)
Conditions | Yield |
---|---|
In acetone the bromo-compd. is added to a soln. of the starting complex in acetone; ppt. is filtd., washed with ether, dried under vac., elem. anal.; | 53% |
ethane-1,2-diyl bis(2-bromoacetate)
5-(4'-pyridylazo)-25,26,27-tris(ethoxycarbonylmethoxy)-28-hydroxycalix[4]arene
Conditions | Yield |
---|---|
With potassium carbonate In tetrahydrofuran Heating; |
Conditions | Yield |
---|---|
With potassium carbonate In tetrahydrofuran Heating; |
ethane-1,2-diyl bis(2-bromoacetate)
Conditions | Yield |
---|---|
With sodium disulfide In tetrahydrofuran for 20h; cyclocondensation; Heating; | 16 % Spectr. |
ethane-1,2-diyl bis(2-bromoacetate)
4-(Diethylamino)salicylaldehyde
C28H36N2O8
Conditions | Yield |
---|---|
With potassium iodide; potassium bromide In butanone for 24h; Heating / reflux; |
Conditions | Yield |
---|---|
In chloroform at 60℃; for 5h; |
Conditions | Yield |
---|---|
In chloroform at 60℃; for 5h; |
Conditions | Yield |
---|---|
In chloroform at 60℃; for 5h; |
Conditions | Yield |
---|---|
In chloroform at 60℃; for 5h; |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide; acetonitrile at 80℃; for 24h; Temperature; Concentration; |
ethane-1,2-diyl bis(2-bromoacetate)
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: acetonitrile / 20 h / 23 °C 2: water; chloroform / 15 h / 23 °C View Scheme |
Conditions | Yield |
---|---|
In acetonitrile at 23℃; for 20h; |
ethane-1,2-diyl bis(2-bromoacetate)
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium hydrogencarbonate / ethanol / 50 - 55 °C / Inert atmosphere 2: N-Bromosuccinimide / dichloromethane; water; dimethyl sulfoxide / 0 - 5 °C View Scheme |
Conditions | Yield |
---|---|
In acetone at 40℃; for 48h; | 1 g |
ethane-1,2-diyl bis(2-bromoacetate)
Conditions | Yield |
---|---|
at 59.99℃; for 6h; Inert atmosphere; |
Chemical Name: 1,2-Bis(bromoacetoxy)ethane
IUPAC NAME: 2-(2-Bromoacetyl)oxyethyl 2-bromoacetate
CAS No.: 3785-34-0
EINECS: 223-250-4
Molecular Formula: C6H8Br2O4
Molecular Weight: 303.93 g/mol
Density: 1.888 g/cm3
Flash Point: 141.7 °C
Boiling Point: 310.7 °C at 760 mmHg
Following is the structure of 1,2-Bis(bromoacetoxy)ethane (3785-34-0):
The chemical synonymous of 1,2-Bis(bromoacetoxy)ethane (3785-34-0) are BBAE ; Ethylene glycol bis(bromoacetate) ; 1,2-Bis(bromoacetoxy)ethane ; 1,2-Ethanediylbromoacetate ; Aceticacid,bromo-,1,2-ethanediylester ; Bromoaceticacidethyleneester ; Bromo-aceticacidiesterwithethyleneglycol ; Bromo-aceticaciethyleneester
1,2-Bis(bromoacetoxy)ethane (3785-34-0) is a highly effective antiseptic fungicide, widely used as industrial circulating water, industrial cooling water, water treatment agents, sterilizing agents algae.
1. | ipr-mus LD50:39 mg/kg | JNCIAM Journal of the National Cancer Institute. 31 (1963),297. | ||
2. | ivn-mus LD50:56 mg/kg | CSLNX* U.S. Army Armament Research & Development Command, Chemical Systems Laboratory, NIOSH Exchange Chemicals. (Aberdeen Proving Ground, MD 21010) NX#03918 . | ||
3. | ivn-dog LD50:15 mg/kg | JNCIAM Journal of the National Cancer Institute. 31 (1963),297. |
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