methyl 1-pentyl-1H-indole-3-carboxylate
1-amino-naphthalene
N-(naphthalen-1-yl)-1-pentyl-1H-indole-3-carboxamide
Conditions | Yield |
---|---|
Stage #1: 1-amino-naphthalene With trimethylaluminum In 1,2-dichloro-ethane; toluene at 20℃; for 0.166667h; Inert atmosphere; Stage #2: methyl 1-pentyl-1H-indole-3-carboxylate In 1,1,1-trichloroethane; toluene for 24h; Inert atmosphere; Reflux; | 85% |
3-methoxycarbonylindole
N-(naphthalen-1-yl)-1-pentyl-1H-indole-3-carboxamide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere 1.2: 16 h / 0 - 20 °C / Inert atmosphere 2.1: trimethylaluminum / 1,2-dichloro-ethane; toluene / 0.17 h / 20 °C / Inert atmosphere 2.2: 24 h / Inert atmosphere; Reflux View Scheme |
1-Bromopentane
N-(naphthalen-1-yl)-1-pentyl-1H-indole-3-carboxamide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere 1.2: 16 h / 0 - 20 °C / Inert atmosphere 2.1: trimethylaluminum / 1,2-dichloro-ethane; toluene / 0.17 h / 20 °C / Inert atmosphere 2.2: 24 h / Inert atmosphere; Reflux View Scheme |
N-1-Naphthalenyl-1-pentyl-1H-indole-3-carboxamide is a novel indole and azaindole cannabinoid receptor agonists.
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