102-84-1Relevant articles and documents
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Laible et al.
, p. 376 (1959)
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Method for preparing unsaturated propyl phosphite ester and unsaturated propyl phosphate
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Paragraph 0065-0068, (2019/08/15)
The invention relates to a method for preparing unsaturated propyl phosphite ester or unsaturated propyl phosphate. The unsaturated propyl phosphite ester is selected from triallyl phosphite and tripropargyl phosphite, and the unsaturated propyl phosphate is selected from triallyl phosphate and tripropargyl phosphate. The method comprises the steps: enabling phosphorus trichloride or phosphorus oxychloride to react with allyl ester to form triallyl phosphite or triallyl phosphate; or enabling phosphorus trichloride or phosphorus oxychloride to react with propargyl ester to form propargyl phosphite or propargyl phosphate. The method for preparing unsaturated propyl phosphite ester or unsaturated propyl phosphate does not need any catalyst, and a by-product acyl chloride compound has a low boiling point and is easy to separate so that the unsaturated propyl phosphite ester or unsaturated propyl phosphate with high yield and high purity can be obtained.
The composite body deproteinizing chitosanoligosaccharide-
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Page/Page column 87, (2016/10/09)
Provided herein are conjugates comprising a protein and an oligosaccharide of one of Formulae I-VI. Also provided herein are pharmaceutical compositions comprising such conjugates. Further provided herein are methods of treating a lysosomal storage disorder in a mammal by administration of an oligosaccharide-glycoprotein conjugate.