134724-55-3Relevant articles and documents
Method for preparing disperse red SBWF
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Paragraph 0015; 0017; 0018; 0020; 0021; 0023; 0024; 0026, (2020/03/06)
The invention relates to a preparation method of disperse red SBWF. The preparation method comprises the following specific steps: by using 4-(tetrahydrofuran-2-methoxy)-benzaldehyde and trichloromethane as raw materials, carrying out carbene reaction under the action of a phase transfer catalyst to prepare intermediate 4-(tetrahydrofuran-2-methoxy) mandelic acid; and carrying out condensation andoxidation of 4-(tetrahydrofuran-2-methoxy) mandelic acid and 5-hydroxy-3-phenyl-3H-benzofuran-2-one to prepare the target product 3-phenyl-7-(4-(tetrahydrofuran-2-methoxy) phenyl)-benzodifuran-2, 6-dione. The preparation method has the advantages of simplicity in operation, mild reaction conditions, environmental friendliness and the like, and has good industrial application value.
ALPHA-HYDROXY-BENZENEACETIC ACID DERIVATIVES, AND COMPOUNDS HAVING TWO 5-MEMBERED LACTONE RINGS FUSED TO CENTRAL CYCLOHEXA-1,4-DIENE NUCLEUS BASED UPON THE SAME, AND USES OF THE COMPOUNDS
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Page/Page column 37-38, (2008/06/13)
The present invention provides a-hydroxy benzeneacetic acid derivatives of the formula as defined in the specification which is a precursor indispensable for synthesis of compounds having two 5-membered lactone rings fused to central cyclohexa-1,4-dien