25038-86-2Relevant articles and documents
2 - methyl - 5 - vinyl pyridine synthesis method (by machine translation)
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Paragraph 0033; 0036; 0037; 0041; 0042; 0046; 0047; 0051, (2017/08/27)
The invention discloses a 2 - methyl - 5 - vinyl pyridine synthesis method, for the purpose of, reduce the synthesis step, to simplify the processing process, and improving the yield and save the cost, reducing chemical raw material consumption, effective protection of the environment, the use of the technical proposal is: (1) the raw material 6 - methyl nicotinic acid methyl ester is reduced to the 2 - methyl - 5 - pyridine base formaldehyde; (2) preparing the phosphorus ylide reagent; (3) the 2 - methyl - 5 - pyridyl formaldehyde and phosphorus ylide reagent in the reaction of 2 - methyl - 5 - vinyl pyridine, concentrated rectification to obtain the product. (by machine translation)
AZA-RING FUSED INDOLE AND INDOLINE DERIVATIVES
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Page/Page column 24, (2011/07/06)
The present application relates to indole and indoline derivatives of formula (I) wherein a, R1, m, L, and Q are as defined in the specification. The present application also relates to compositions comprising such compounds, and methods of treating disease conditions using such compounds and compositions of such compounds.
2-METHYL-5-VINYLPYRIDINIUM SALTS
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Page/Page column 6, (2011/12/14)
Disclosed are novel salts of 2-methyl-5-vinylpyridine (MVP), such as hydrogentartrates, bromide, and dihydrogenphosphate. In contrast to the free base, these salts are crystalline and stable and can be safely stored and transported. The salts can also be used to purify MVP, in particular to reduce its content of 5-ethyl-2-methylpyridine and unwanted isomers.