64621-41-6Relevant articles and documents
Poly(azomethine-epoxy-ether) containing phenyl and etoxy moieties: synthesis, characterization and fluorescence property
Kolcu, Feyza,Kaya, ?smet
, p. 2821 - 2832 (2018)
The design and synthesis of poly(azomethine-epoxy-ether) (PAZ-EP) containing epoxide moiety was described. The purpose of the research was the improvement of poly(azomethine-ether) containing epoxide by introduction of Schiff base moiety. PAZ-EP was synthesized using epichlorohydrin (EP). The structure of the Schiff base (SB) and PAZ-EP were verified by FT-IR, 1H-NMR, 13C-NMR and UV–Vis spectroscopic analyses. Further characterization was employed using photophysical, electrochemical and fluorescence (PL) measurements. Application of TGA and differential scanning calorimetry analyses revealed thermal stability and thus propose a thermal processibility, which makes them potential materials for many contemporary practices. The number of average molecular weight of polymer with a polydispersity index of 1.14 was found to be 6750?Da using a gel permeation chromatography instrument. The highest occupied–lowest unoccupied energy levels and electrochemical (Eg′) band gap values of PAZ-EP were determined by cyclic voltammetry (CV) measurement. Scanning electron microscopy (SEM) images were illustrated at different magnifications to study the morphologic property of PAZ-EP.
Green synthesis of novel bis(hexahydro-1H-xanthene-1,8(2H)-diones) employing p-toluenesulfonic acid (p-TSA) as a solid acid catalyst
Darweesh, Ahmed F.,Salama, Soad K.,Abdelhamid, Ismail A.,Elwahy, Ahmed H. M.
, p. 471 - 484 (2020/10/30)
Green synthesis of novel bis(hexahydro-1H-xanthene-1,8(2H)-diones) which are linked to aliphatic or aromatic spacers via ether or ester linkages were performed in good to excellent yields by the reaction of 5,5-dimethyl-1,3-cyclohexanedione with the appropriate bis-aldehydes using p-TSA as an organic acid solid catalyst. The reaction of the bis-aldehydes with barbituric acid or 1,3-dimethylbarbituric acid instead of 5,5-dimethyl-1,3-cyclohexanedione afforded the corresponding Knoevenagel condensation adducts in good yield.
Synthesis of novel bis(Pyrido[2,1-a]isoquinolines) linked to aliphatic or aromatic core via ether linkage
Saleh, Fatma M.,Hassaneen, Hamdi M.,Abdelmoniem, Amr M.,Elwahy, Ahmed H. M.,Abdelhamid, Ismail A.
, p. 1914 - 1921 (2019/07/15)
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