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Items |
Specification |
Results |
Appearance |
White or almost white crystalline powder |
Confirms |
|
Practically insoluble in water, freely |
|
|
soluble in methylene chloride, soluble |
|
|
in methanol, sparingly soluble in alcohol. |
|
Identification |
IR |
Confirms |
Melting range, °C |
148.0~152.0 |
148.0~150. |
Specific Rotation |
-1.0o~+1.0o |
0o |
Loss on Drying, % |
≤ 0.50 |
0.1 |
Residue on Ignition, % |
≤ 0.10 |
0.06 |
Heavy Metals, % |
≤ 0.002 |
< 0.002 |
Chromatographic purity, % |
≤ 2.0 |
Confirms |
Residue Solvent, % |
|
|
Acetoacetate |
≤ 0.50 |
0.3 |
Dimethyl sulfoxide |
≤ 0.50 |
0 |
Bacteria |
Not more than 10 per g |
Confirms |
Mold & yeast |
None-detected |
Confirms |
Assay, % |
98.0~102.0 |
99.2 |
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