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73602-61-6 Triethylamine trihydrofluoride 73602-61-6 Triethylamine trihydrofluoride 73602-61-6 Triethylamine trihydrofluoride
Product Name: Triethylamine trihydrofluoride
Synonyms: MEC-82;HF 37% IN TRIETHYLAMINE;HF;HYDROGEN FLUORIDE TRIETHYLAMINE;TRIETHYLAMINE TRIHYDROFLUORIDE;TRIETHYLAMINE TRISHYDROFLUORIDE;TRIETHYLAMINE TRIS(HYDROGEN FLUORIDE);Triethylamin-trihydrofluoride
CAS: 73602-61-6
MF: C6H18F3N
MW: 161.21
EINECS: 277-550-5
Product Categories: Fluorinating Reagents;Fluorinating Reagents & Building Blocks for Fluorinated Biochemical Compounds;Fluorination;Halogenation;Nucleophilic Fluorinating Reagents;Synthetic Organic Chemistry
Mol File: 73602-61-6.mol
Triethylamine trihydrofluoride Chemical Properties
Melting point -29--27°C
Boiling point 70 °C15 mm Hg(lit.)
density 0.989 g/mL at 25 °C(lit.)
refractive index n20/D 1.3915(lit.)
Fp 190 °F
storage temp. Keep Cold
form Liquid
color Clear yellow to brown
Specific Gravity 0.989
PH 3 (H2O, 20℃)(saturated aqueous solution)
Water Solubility soluble
Sensitive Hygroscopic
BRN 5522945
CAS DataBase Reference 73602-61-6(CAS DataBase Reference)
EPA Substance Registry System Ethanamine, N,N-diethyl-, trihydrofluoride (73602-61-6)
Safety Information
Hazard Codes T+,T,C,Xi,F
Risk Statements 26/27/28-35-36/37/38-20/21/22-11
Safety Statements 26-36/37/39-45-7/9-36/37-36-61-29-16-3
RIDADR UN 3265 8/PG 2
WGK Germany 3
Hazard Note Corrosive
TSCA Yes
HazardClass 8
PackingGroup II
HS Code 29211910
Triethylamine trihydrofluoride Usage And Synthesis
Application
The t-butyldimethylsilyl (TBDMS) group is the most widely used 2'-OH protection in synthesis of oligoribonucleotides. The TBDMS-group became much used particularly after it was combined with phosphoroamidite methodology and was also the choice when H-phosphonate based RNA-synthesis was introduced. Removal of TBDMS-protection is most commonly done with 1 M tetrabutylammonium fluoride (TBAF) in tetrahydrofuran (THF). These conditions has proven efficient.
Chemical Properties clear yellow liquid
Product Name: Triethylamine trihydrofluoride
Synonyms: MEC-82;HF 37% IN TRIETHYLAMINE;HF;HYDROGEN FLUORIDE TRIETHYLAMINE;TRIETHYLAMINE TRIHYDROFLUORIDE;TRIETHYLAMINE TRISHYDROFLUORIDE;TRIETHYLAMINE TRIS(HYDROGEN FLUORIDE);Triethylamin-trihydrofluoride
CAS: 73602-61-6
MF: C6H18F3N
MW: 161.21
EINECS: 277-550-5
Product Categories: Fluorinating Reagents;Fluorinating Reagents & Building Blocks for Fluorinated Biochemical Compounds;Fluorination;Halogenation;Nucleophilic Fluorinating Reagents;Synthetic Organic Chemistry
Mol File: 73602-61-6.mol
Triethylamine trihydrofluoride Chemical Properties
Melting point -29--27°C
Boiling point 70 °C15 mm Hg(lit.)
density 0.989 g/mL at 25 °C(lit.)
refractive index n20/D 1.3915(lit.)
Fp 190 °F
storage temp. Keep Cold
form Liquid
color Clear yellow to brown
Specific Gravity 0.989
PH 3 (H2O, 20℃)(saturated aqueous solution)
Water Solubility soluble
Sensitive Hygroscopic
BRN 5522945
CAS DataBase Reference 73602-61-6(CAS DataBase Reference)
EPA Substance Registry System Ethanamine, N,N-diethyl-, trihydrofluoride (73602-61-6)
Safety Information
Hazard Codes T+,T,C,Xi,F
Risk Statements 26/27/28-35-36/37/38-20/21/22-11
Safety Statements 26-36/37/39-45-7/9-36/37-36-61-29-16-3
RIDADR UN 3265 8/PG 2
WGK Germany 3
Hazard Note Corrosive
TSCA Yes
HazardClass 8
PackingGroup II
HS Code 29211910
Triethylamine trihydrofluoride Usage And Synthesis
Application
The t-butyldimethylsilyl (TBDMS) group is the most widely used 2'-OH protection in synthesis of oligoribonucleotides. The TBDMS-group became much used particularly after it was combined with phosphoroamidite methodology and was also the choice when H-phosphonate based RNA-synthesis was introduced. Removal of TBDMS-protection is most commonly done with 1 M tetrabutylammonium fluoride (TBAF) in tetrahydrofuran (THF). These conditions has proven efficient.
Chemical Properties clear yellow liquid
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