438-67-5 Estrone sodium sulphate estrone 3-sulfate sodium
Items |
Specification
|
Results |
appearance |
White or slightly yellow, crystalline powder |
White crystalline |
Solubility |
Practically insoluble in water, soluble in methylene chloride, slightly soluble in anhydrousethanol |
confirms |
Identification (IR) |
same wave numbers as that of the Vinpocetine, CRS similarly prepared CRS similarly prepared. |
Conforms |
Specific Optical Rotation(On dried basis) |
Between +127° and +134° |
+132.7° |
Related Substances (External Standard method) |
||
Ethyl vincaminate(A) |
≤0.6% |
Conforms |
Apovincamine(B) |
≤0.5% |
Conforms |
Methoxyvinpocetine(C) |
≤0.3% |
Not detected |
Dihydrovinpocetine(D) |
≤ 0.5% |
Not detected |
Other single impurity |
≤0.10% |
Conforms |
Total impurity |
≤ 1.0% |
0.19% |
Loss on drying
|
≤ 0.5% |
0.04% |
Sulphated ash
|
≤ 0.1% |
0.07% |
Assay(On dried basis) |
98.5% ~101,5% , |
100.2% |
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