C10H12O2 (S)-(+)-B...

C10H12O2 (S)-(+)-Benzyl glycidyl ether 16495-13-9

C10H12O2 (S)-(+)-Benzyl glycidyl ether 16495-13-9

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(S)-(+)-Benzyl glycidyl ether 16495-13-9 C10H12O2

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(S)-(+)-Benzyl glycidyl ether Basic information
Product Name: (S)-(+)-Benzyl glycidyl ether
Synonyms: (s)-o-benzylglycidol;(S)-(+)-2-(BENZYLOXYMETHYL)OXIRANE;(S)-(+)-1-BENZYLOXY-2,3-EPOXYPROPANE;(S)-1-BENZYLOXY-2,3-EPOXYPROPANE;(S)-(+)-BENZYL GLYCIDYL ETHER;(S)-BENZYL GLYCIDYL ETHER;(S)-BENZYLOXYMETHYL-OXIRANE;(+)-BENZYL (S)-GLYCIDYL ETHER
CAS: 16495-13-9
MF: C10H12O2
MW: 164.2
EINECS: -0
Product Categories: chiral;CHIRAL COMPOUNDS;Chiral Building Blocks;Glycidyl Compounds, etc. (Chiral);Oxiranes;Simple 3-Membered Ring Compounds;Synthetic Organic Chemistry;Chiral Compound
Mol File: 16495-13-9.mol
(S)-(+)-Benzyl glycidyl ether Structure
 
(S)-(+)-Benzyl glycidyl ether Chemical Properties
Boiling point  130 °C (0.1 mmHg)
alpha  5.1 º (c=5 in toluene)
density  1.072 g/mL at 20 °C(lit.)
refractive index  n20/D 1.517
Fp  >110°C
storage temp.  2-8°C
BRN  5246495
CAS DataBase Reference 16495-13-9(CAS DataBase Reference)
 
Safety Information
Hazard Codes  Xi
Risk Statements  36/37/38
Safety Statements  26-36-37/39
WGK Germany  3
RTECS  TX2860030
MSDS Information
Provider Language
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SigmaAldrich English
ALFA English
 
(S)-(+)-Benzyl glycidyl ether Usage And Synthesis
Chemical Properties Colorless to light yellow liqui
Uses (S)-(+)-Benzyl Glycidyl Ether is used as a reactant in the synthesis of (+)-Discodermolide.
Purification Methods This ether in EtOAc is dried (Na2SO4), then purified by flash chromatography using pet ether/EtOAc (5:1) as eluent. The ether distils through a short path distillation apparatus (Kügelrohr) as a colourless liquid. Alternatively, dissolve it in CHCl3, wash it with H2O, dry (Na2SO4), evaporate and purify by silica gel chromatography. [Anisuzzamen & Owen J Chem Soc 1021 1967, Takano et al. Heterocycles 1 6 381 1981, Lipshutz et al. Org Synth 69 82 1990, Takano et al. Synthesis 539 1989, Honda et al. Chem Pharm Bull Jpn 39 1385 1991, Beilstein 12 IV 2277.]
 
(S)-(+)-Benzyl glycidyl ether Preparation Products And Raw materials

 

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