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Lithium tri-Tert-Butoxyaluminum Hydride 17476-04-9 Lithium tri-tert-butoxyaluminohydride
Product name | Lithium tri-tert-butoxyaluminum hydride |
Synonyms |
Lithium Tri-tert-butoxyaluminum Hydride (30% in Tetrahydrofuran, ca. 1.1mol/L);Lithium hydridotris(tert-butoxy)aluminate, nominally 1M in THF, packaged under Argon in resealable ChemSeal bottles;lithium,(beta-4)-aluminate(1-hydrotris(2-methyl-2-propanolato)-;lithiumhydrotris(2-methyl-2-propenolato)aluminate;lithiumtri-tert-butoxyhydroaluminate;tri-tert-butoxyhydruredelithium-aluminium;Lithium hydridotris(tert-butoxy)aluminate, nominally 1M in THF, packaged under Argon in resealable C;Lithium Tri-tert-butoxyaluminum Hydride (20% in Tetrahydrofuran, ca. 0.7mol/L)
|
Cas | 17476-04-9 |
MF | C12H28AlLiO3 |
MW | 254.27 |
EINECS | 241-490-8 |
Product Categories | Al (Alminum) Compounds;Classes of Metal Compounds;Li (Lithium) Compounds;Reduction;Synthetic Organic Chemistry;Typical Metal Compounds;-;Aluminum Hydrides;Synthetic Reagents;metal alkyl |
Melting point | 300-319 °C (dec.)(lit.) |
Boiling point | 66°C (THF) |
density | 0.942 g/mL at 25 °C |
Fp | 95 °F |
storage temp. | 2-8°C |
solubility | It is soluble in organic solvents at low temperatures. |
form | Solution |
color | Clear to slightly turbid colorless |
Water Solubility | Reacts with water. |
Item | Standard | Test Results | |
Identification |
A.H-NMR:Comply with the structure |
Complies |
|
B.LC-MS:Comply with the structure |
Complies |
||
C.The IR spectrum of sample should be identical with that of reference standard; |
Complies |
||
D.HPLC-ESI-MS The retention time of the major peak in the chromatogram of the Assay preparation corresponds to that in the chromatogram of the Standard preparation, as obtained in the Assay. |
Complies |
||
Loss on drying |
≤0.5% |
0.11% |
|
Heavy metals |
≤10 ppm |
<10ppm |
|
Sulphated ash |
≤0.2%, determined on 1.0 g. |
0.009% |
|
Related substances |
Unspecified impurities: for each impurity |
≤0.10% |
<0.10% |
Total Impurity |
≤1.0% |
0.18% |
|
Purity |
≥99.0% |
99.82% |
|
Assay |
99.0%~101.0% (anhydrous substance). |
99.9% |
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