1453-82-3 Isonicotinamide 4-Pyridinecarboxamide
Product Name: Isonicotinamide
Appearance: White crystal powder
M.F.: C6H6N2O
M.W.: 122.12
CAS NO.: 1453-82-3
EINECS NO.: 215-926-2
Item |
Specifications |
Results |
Characteristics |
White or almost white crystalline powder;slightly soluble in water freely soluble in formic acid,slightly soluble in anhydrous ethanol |
Almost white crystalline powder;Odorless and tasteless;The product meets the requirement or test for solubility |
Melting point |
About 155-157 °C |
155-157 °C |
Identification |
(1)Should conformed (2)specific rotation:between -17.5 and -20.5° (3)Examine by infrared absorption spectrophotmetry,compare the spectrum obtained with reference spectrum should meet the requirement (4)Should conformed |
(1)Conformed (2)-19.5°
(3)Conformed
(4)Conformed |
Related substances |
Procedure A: Largest single impurity should ≤0.1% Procedure B:largest single impurity should ≤0.1% Total impurity should ≤0.2% |
0.04%
0.003%
0.07% |
Enantiomeric purity |
Not more than 0.1% |
0.03% |
Heavy metals |
Not more than 20ppm |
Conformed |
Loss on drying |
Not more than 0.5% |
0.04% |
Sulphated ash |
Not more than0.1% |
0.03% |
Assay |
Should between 98.5 and 101.0 per sent |
99.6% |
Conclusion |
The results conforms with EP7.0 standards. |
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