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reasonable price 5337-93-9 5337-93-9 4-Methylpropiophenone 4-Methylpropiophenone reliable manufacturers
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P-methylpropiophenone is a chemical reagent used in electrocarboxylation reactions.
application
P-methylpropiophenone is an intermediate of the drug Naomaining, which can be used as an organic synthesis intermediate and a pharmaceutical intermediate, and is mainly used in the laboratory research and development process and the chemical production process.
resolve resolution
The use of chiral adsorption inducer alkaloids to induce p-methylpropiophenone to fix carbon dioxide to electrosynthesize α-7,yl-α-hydroxy-4-methyl-phenylacetic acid, and obtain higher results by constant current electrolysis and high performance liquid gun.
Yield and certain ee value, through preliminary investigation of the reacted electrode material, current density, inducer and other factors, it is found that the ring-shaped stainless steel is used as the cathode, the magnesium rod is used as the sacrificial anode, and the tetrabutylammonium iodide is used as the electrolysis supporting salt.
, 0.016g cinchonine as an inducer and constant current electrolysis with a current density of 1,1mA·Cm-2 at a temperature of 0°C can obtain a yield of 37.39% and an ee value of S-32.78%.
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