N-Boc-N-methylethylenediamine

Details:

Melting point     248-251 °C (decomp)
Boiling point     79°C/0.4mmHg(lit.)
density     0.975 g/mL at 20 °C (lit.)
refractive index     n20/D 1.447
Fp     >100 °C
storage temp.     Keep in dark place,Inert atmosphere,2-8°C
pka    9.44±0.10(Predicted)
form     Liquid
color     Clear colorless to pale yellow
BRN     3588326
InChIKey    QYJVBVKFXDHFPQ-UHFFFAOYSA-N
CAS DataBase Reference    121492-06-6(CAS DataBase Reference)
Safety Information
Hazard Codes     C
Risk Statements     34
Safety Statements     26-36/37/39-45
RIDADR     2734
WGK Germany     3
HazardClass     8
PackingGroup     Ⅲ
MSDS Information
Provider    Language
SigmaAldrich    English
N-Boc-N-methylethylenediamine Usage And Synthesis
Uses    N-Boc-N-methylethylenediamine is a compound useful in organic synthesis and other chemical processes.
Chemical Properties    Liquid
Uses    Mono-protected building block.
N-Boc-N-methylethylenediamine Preparation Products And Raw materials
Raw materials    2-(2-N-BOC-N-METHYL-AMINOETHYL)-1H-ISOINDOLE-1,3(2H)-DIONE-->tert-Butyl Methyl(2-(2,2,2-trifluoroacetaMido)ethyl)carbaMate-->tert-Butyl N-(2-bromoethyl)carbamate-->BOC-SAR-OH-->N-Boc-2-azidoethylaMine-->tert-Butyl (2-azidoethyl)(methyl)carbamate-->2-(N-BOC-METHYLAMINO)ACETONITRILE-->N-carbamoylmethyl-N-methyl-carbamic acid t-butyl ester-->Methylaminoacetonitrile hydrochloride-->(2-HYDROXYETHYL)METHYLCARBAMIC ACID 1,1-DIMETHYLETHYL ESTER-->tert-Butyl 2-(methylamino)ethylcarbamate-->Di-tert-butyl dicarbonate-->N-METHYLETHYLENEDIAMINE