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3-Nitrophthalic acid price 603-11-2 3-Nitrophthalic acid 3-Nitrophthalic acid supplier
price 603-11-2 3-Nitrophthalic acid supplier
Preparation method
Into the reactor into the 1200Kg concentrated sulfuric acid, 560Kg benzene stirring heating to 50 degrees C, began to add 500 KG thick nitric acid, reaction heating mixture heating, control reaction temperature does not exceed 100 degrees C, nitric acid drops added, 100 degrees C/2h, 110 degrees C / 2h insulation reaction completely. After the reaction, cool down, the nitrification material into the hydrolysis kettle, hydrolysis kettle pre-added 1500Kg ice water, after adding at 80 degrees C /3h, cooling extraction filter nitro phthalates. In the separation pot pre-added 1500Kg water, added the above nitro phthalates, stirred at room temperature 4h, and then separated 3-nitro phthalates crude. Add the same amount of water and 3-nitro phthalates crudes to the recrystallization pot and cool to normal temperature after heating back to 1h, centrifugation to 3-nitro phthalates, analyzed by HPLC, the content is greater than 99%.
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