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100 Kilogram |
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179324-87-9 C17H29BF3NO4 (aR,3aS,4S,6S,7aR) -Hexahydro-3A,8,8-Trimethyl-Alpha- (2-methylpropyl) -4,6-Methano-1,3,2-Benzodioxaborole-2-Methanamine 2,2,2-Trifluoroacetate
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Product Description
Item |
Specifications |
Results |
Appearance |
White or off-white powder |
Conforms |
Identification |
HNMR:correspond to the known structure |
Conforms |
Water content |
NMT 2.0% |
0.4% |
Diastereomer |
The impurity 312-2P(RRT1.05), NMT 0.10% |
0.09% |
Assay(non-aqueous titration) |
97.0-103.0%(anhydrous substance) |
99.8% |
Conclusion |
The results conforms with enterprise standards |
Diastereomer with derivatization by HPLC | |||||||
Column:C8 150mm*4.6mm 3.5μm | Wavelength:225nm | ||||||
Column temperature:35ºC | Diluent:Acetonitrile | ||||||
Flow rate:1.0ml/min | Sample concentration:0.5mg/ml | ||||||
Injection:10μl | Run time:30min | ||||||
Mobile phase A:Acetonitrile | |||||||
Mobile phase B:Water | |||||||
Gradient elution table: | |||||||
Time | 0 | 5 | 20 | 25 | 25.1 | 30 | \ |
A% | 10 | 55 | 55 | 75 | 10 | 10 | \ |
B% | 90 | 45 | 45 | 25 | 90 | 90 | \ |
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