504-17-6 2-Thiobarbituric acid 4,6-Dihydroxy-2-mercaptopyrimidine
English Name: TBA; 2-thiobarbituric acid; 4,6-dihydroxy-2-mercaptopyrimidine
Other names: 4,6-dihydroxy-2-mercaptopyrimidine; propionyl thiourea; 2-thiobarbituric acid; 4,6-dioxo-2-mercaptopyrimidine; dihydro-2-thio-4,6 (1H, 5H) - pyrimidinedione; malodiene thiourea
CAS No.: 504-17-6
C4H4N2O2S=144.15
Level: AR
Content: ≥ 98.5%
Sodium hydroxide dissolution test: acceptable
Burning residue: ≤ 0.2%
Character: white or light yellow flake crystal.
Item |
Standard |
Test Results |
Identification |
A.H-NMR:Comply with the structure |
Complies |
B.LC-MS:Comply with the structure |
Complies |
|
C.The IR spectrum of sample should be identical with that of reference standard. |
Complies |
|
D.HPLC-ESI-MS The retention time of the major peak in the chromatogram of the Assay preparation corresponds to that in the chromatogram of the Standard preparation, as obtained in the Assay. |
Complies |
|
Loss on drying |
≤2.0% |
0.19% |
Heavy metals |
≤10 ppm |
<10ppm |
Water |
≤1.0% |
0.1% |
Sulphated ash |
≤0.5% determined on 1.0 g. |
0.009% |
Residue on ignition |
≤0.1% |
0.03% |
Related Substances |
Unspecified impurities: for each impurity ≤0.10% |
<0.10% |
Total Impurity ≤0.5% |
0.18% |
|
Purity |
≥99.0% |
99.7% |
Assay |
99.0%~101.0% (anhydrous substance). |
99.8% |
Storage |
Preserve in well-closed, light-resistant and airtight containers. |
Complies |
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