5-Bromo-3-pyridinecarboxaldehyde 113118-81-3

Details:

Introduction: 

5-Bromopyridine-3-carbaldehyde, Chinese alias 5-Bromonicotinaldehyde, is an organic chemical substance, which can be used as an intermediate in pharmaceutical chemical synthesis

In the prior art, the synthetic method of 5-bromopyridine-3-carbaldehyde is based on 3,5-dibromopyridine as the original, and exchanged with butyllithium bromide under ultra-low temperature (-78°C) to prepare 5-bromopyridine-3. -formaldehyde, or using 3,5-dibromo Chemicalbook pyridine as raw material, at -15°C, butyllithium and n-butylmagnesium chloride are combined to synthesize 5-bromopyridine-3-carbaldehyde; the above two synthesis methods are reacted in It can only be carried out under ultra-low temperature conditions, the reaction conditions are harsh, and it is difficult to industrialize.

 

5-Bromo-3-pyridinecarboxaldehyde Basic information

Product Name:	5-Bromo-3-pyridinecarboxaldehyde
Synonyms:	CHEMBRDG-BB 4011095;AURORA KA-3030;5-BROMO-PYRIDINE-3-CARBALDEHYDE;5-BROMOPYRIDINE-3-CARBOXALDEHYDE;5-BROMONICOTINALDEHYDE;3-BROMOPYRIDINE-5-CARBALDEHYDE;3-BROMOPYRIDINE-5-CARBOXALDEHYDE;5-BROMO-3-PYRIDINECARBOXALDEHYDE
CAS:	113118-81-3
MF:	C6H4BrNO
MW:	186.01
EINECS:	628-546-0
Product Categories:	C6Heterocyclic Building Blocks;Halogenated Heterocycles;Halogenated;Pyridine;Heterocyclic Building Blocks;Heterocycle-Pyridine series;pharmacetical;Aldehydes;Pyridines;Building Blocks
Mol File:	113118-81-3.mol

5-Bromo-3-pyridinecarboxaldehyde Chemical Properties

Melting point	98-102 °C
Boiling point	251.1±20.0 °C(Predicted)
density	1.683±0.06 g/cm3(Predicted)
storage temp.	Keep in dark place,Sealed in dry,Room Temperature
pka	1.07±0.20(Predicted)
form	Crystalline Powder
color	White to off-white
Sensitive	Air Sensitive
CAS DataBase Reference	113118-81-3(CAS DataBase Reference)

Safety Information

Hazard Codes	Xi,Xn
Risk Statements	22-36/38-43
Safety Statements	26-36/37/39
WGK Germany	3
Hazard Note	Irritant
HazardClass	IRRITANT

MSDS Information

5-Bromo-3-pyridinecarboxaldehyde Usage And Synthesis

5-Bromo-3-pyridinecarboxaldehyde Preparation Products And Raw materials

Raw materials	Hydrochloric acid-->Diethyl ether-->Dichloromethane-->Sodium-->N,N-Dimethylformamide-->Magnesium sulfate-->Sodium chloride-->n-Butyllithium-->Nitrogen-->2,5-Dibromopyridine
Preparation Products	6-MORPHOLINONICOTINALDEHYDE-->3-Bromo-5-(Chloromethyl)Pyridine Hydrochloride-->3-(TRIMETHYLSILYLETHYNYL)PYRIDINE-->(5-BROMO-PYRIDIN-3-YL)-METHANOL

 

 

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