4-Bromo-N,N-dimethylaniline 4-N,N-dimethylaminobromobenzene CAS:586-77-6
Product Name: 4-Bromo-N,N-dimethylaniline
Synonym: 4-N,N-dimethylaminobromobenzene; 4-Dimethylaminobromobenzene;Intermediate of Mifepristone
Cas No.: 586-77-6
Formula: C8H10BrN
MW: 200.08
EINECS No.:209-582-2
Density: 1.4±0.1 g/cm3
Boiling point: 264.0±0.0 °C at 760 mmHg
Melting point: 52-54 °C(lit.)
Flash point: 104.7±19.8 °C
Refractive index: 1.587
HS Code: 2921499090
Application
4-Bromo-N,N-dimethylaniline is an internal standard used in the determination of iodine present as iodide in pharmaceuticals and iodate in iodized table salt.
Intermediate of Mifepristone.
Item |
Standard |
Test Results |
|
Identification |
A.H-NMR:Comply with the structure |
Complies |
|
B.LC-MS:Comply with the structure |
Complies |
||
C.The IR spectrum of sample should be identical with that of reference standard; |
Complies |
||
D.HPLC-ESI-MS |
Complies |
||
The retention time of the major peak in the chromatogram of the Assay preparation corresponds to that in the chromatogram of the Standard preparation, as obtained in the Assay. |
|||
Heavy metals |
≤10 ppm |
<10ppm |
|
Water |
≤1.0% |
0.10% |
|
Sulphated ash |
≤0.5%, determined on 1.0 g. |
0.01% |
|
Related substances |
Unspecified impurities: for each impurity |
≤0.10% |
<0.10% |
Total Impurity |
≤0.5% |
0.18% |
|
Purity |
≥99.0% |
99.70% |
|
Assay |
99.0%~101.0% (anhydrous substance). |
99.80% |
|
Storage |
Preserve in well-closed, light-resistant and airtight containers. |
Complies |
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