5-Methyl furfural

Min.Order / FOB Price:Get Latest Price

10 Milligram	Negotiable

10 Milligram

Negotiable

Min.Order :10 Milligram
Purity: ≥98%
Payment Terms : T/T

Keywords

5-Methyl furfural 620-02-0 standard supplier in China

Quick Details

Appearance:detailed see specifications
Application:analysis,activity test,Botanical Reference Materials,Standard materials
PackAge:According to the clients requirement.
ProductionCapacity:1|Metric Ton|Day
Storage:Store at 2~8°C
Transportation:by air or by ocean shipping

Superiority:

Hubei CuiRan Biotechnology Co., Ltd is a leading company in the research, development, manufacture and marketing of High Quality Phytochemicals and Extracts(especially Active Ingredients from Traditional Chinese Medicine，Traditional Chinese Medicine), Natural Active Pharmaceutical Ingredients worldwide. From small quantities for R&D or reference standard, to large quantities for customizing or manufacturing, Biopurify emphasizes on consistent and reliable services for his customers.
With excellent quality products and good service, we have clients from more than dozens countries and regions, and we pride ourselves in providing our customers with a total satisfaction experiences.
We are doing our best to be your reliable partner for high quality Phytochemicals and Reference Standards from china.

Our main services:
A. Supply active ingredients and reference standards ofTraditional Chinese Medicine, from mgs to kgs scale.
B. Custom extraction and purification, target Herb Active Ingredients
C. Custom synthesis and semi-synthesis for Natural Active Ingredients
D. CR, CM and PD services from lab scale, pilot scale to commercial scale(GMP is also available)
E.Traditional Chinese Medicine compounds library

1.Provide traditional Chinese medicine reference materials and natural active ingredients;
2.More than 2200 compounds are available for selection, continuously building high-quality natural product libraries for drug research and development;
3.Provide various screening libraries and more inhibitor products;
4.Provide separation and structural determination of natural products;
5.Laboratory scale pilot to commercial scale collaborative research and process development services.More than 180 experiences in phytochemistry (still increasing)
Each product has passed very strict testing (NMR/MS/HPLC)
Agents from many countries

General tips：For obtaining a higher solubility , please warm the tube at 37 ℃ and shake it in the ultrasonic bath for a while.Stock solution can be stored below -20℃ for several months.
We recommend that you prepare and use the solution on the same day. However, if the test schedule requires, the stock solutions can be prepared in advance, and the stock solution must be sealed and stored below -20℃. In general, the stock solution can be kept for several months.
Before use, we recommend that you leave the vial at room temperature for at least an hour before opening it.
About Packaging：1. The packaging of the product may be reversed during transportation, cause the high purity compounds to adhere to the neck or cap of the vial.Take the vail out of its packaging and shake gently until the compounds fall to the bottom of the vial.
2. For liquid products, please centrifuge at 500xg to gather the liquid to the bottom of the vial.
3. Try to avoid loss or contamination during the experiment.
Shipping Condition：Packaging according to customer requirements(5mg, 10mg, 20mg and more). Ship via FedEx, DHL, UPS, EMS or other couriers with RT, or blue ice upon request.

Details:

Chemical Properties of 5-Methyl-2-furaldehyde

Cas No.	620-02-0
PubChem ID	12097	Appearance	Oil
Formula	C₆H₆O₂	M.Wt	110.1
Type of Compound	Miscellaneous	Storage	Desiccate at -20°C
Solubility	Soluble in Chloroform,Dichloromethane,Ethyl Acetate,DMSO,Acetone,etc.
Chemical Name	5-methylfuran-2-carbaldehyde
SMILES	CC1=CC=C(O1)C=O
Standard InChIKey	OUDFNZMQXZILJD-UHFFFAOYSA-N
General tips	For obtaining a higher solubility , please warm the tube at 37 ℃ and shake it in the ultrasonic bath for a while.Stock solution can be stored below -20℃ for several months. We recommend that you prepare and use the solution on the same day. However, if the test schedule requires, the stock solutions can be prepared in advance, and the stock solution must be sealed and stored below -20℃. In general, the stock solution can be kept for several months. Before use, we recommend that you leave the vial at room temperature for at least an hour before opening it.
About Packaging	1. The packaging of the product may be reversed during transportation, cause the high purity compounds to adhere to the neck or cap of the vial.Take the vail out of its packaging and shake gently until the compounds fall to the bottom of the vial. 2. For liquid products, please centrifuge at 500xg to gather the liquid to the bottom of the vial. 3. Try to avoid loss or contamination during the experiment.
Shipping Condition	Packaging according to customer requirements(5mg, 10mg, 20mg and more). Ship via FedEx, DHL, UPS, EMS or other couriers with RT, or blue ice upon request.

Source of 5-Methyl-2-furaldehyde

The rhizome of Typhonium giganteum Engl.

Biological Activity of 5-Methyl-2-furaldehyde

Description

5-?Methylfurfural is a naturally occurring substance, found in cigarette smoke condensate, licorice essential oil, stored dehydrated orange powder, baked potato flour, volatile compounds of roast beef, aroma concentrate of sponge cake. bread and in coffee, tea and cocoa. A flavoring agent.

In vitro

Characterization of high molecular mass material in ECF and TCF bleaching liquors by Py-GC/MS with and without TMAH methylation[Reference: WebLink]

Journal of Analytical & Applied Pyrolysis, 2006 , 76 (1–2) :214-21.

METHODS AND RESULTS:
Typical major pyrolysis products formed from lignin in the ECF bleaching liquor were phenol, 2-methylphenol, guaiacol and 4-vinylguaiacol, whereas crotonolactone and 2-furfural were characteristic degradation products of carbohydrates. Guaiacol, 2-furfural, 2-methylphenol, 2- or 3-ethylphenol, 2-methyl-2-cyclopenten-1-one, 5-Methyl-2-furaldehyde, 2,4-dimethylphenol and 2-methoxy-3-methylphenol were major degradation products formed from HMW TCF bleaching liquors. Only small amounts of chlorinated degradation products were formed from HMW material in the ECF bleaching liquors. The amounts of HMW carbohydrates (such as hemicelluloses) were slightly higher in the liquor obtained after the last step of the TCF than that of the ECF bleaching sequence.
CONCLUSIONS:
Both these liquors consist mainly of lignin matter.

Preparing Stock Solutions of 5-Methyl-2-furaldehyde

	1 mg	5 mg	10 mg	20 mg	25 mg
1 mM	9.0827 mL	45.4133 mL	90.8265 mL	181.653 mL	227.0663 mL
5 mM	1.8165 mL	9.0827 mL	18.1653 mL	36.3306 mL	45.4133 mL
10 mM	0.9083 mL	4.5413 mL	9.0827 mL	18.1653 mL	22.7066 mL
50 mM	0.1817 mL	0.9083 mL	1.8165 mL	3.6331 mL	4.5413 mL
100 mM	0.0908 mL	0.4541 mL	0.9083 mL	1.8165 mL	2.2707 mL
* Note: If you are in the process of experiment, it's necessary to make the dilution ratios of the samples. The dilution data above is only for reference. Normally, it's can get a better solubility within lower of Concentrations.

References on 5-Methyl-2-furaldehyde

Vortex- and CO2 -gas-assisted liquid-liquid microextraction with salt addition for the high-performance liquid chromatographic determination of furanic compounds in concentrated juices and dried fruits.[Pubmed:26718308]

J Sep Sci. 2016 Mar;39(5):947-55.

A novel microextraction method based on vortex- and CO2 -assisted liquid-liquid microextraction with salt addition for the isolation of furanic compounds (5-hydroxymethyl-2-furaldehyde, 5-Methyl-2-furaldehyde, 2-furaldehyde, 3-furaldehyde, 2-furoic and 3-furoic acids) was developed. Purging the sample with CO2 was applied after vortexing to enhance the phase separation and mass transfer of the analytes. The optimum extraction conditions were: extraction solvent (volume), propyl acetate (125 muL); sample pH, 2.4; vortexing time, 45 s; salt concentration, 25% w/v and purging time, 5 min. The analytes were separated using an ODS Hypersil C18 column (250x4.6 mm i.d, 5 mum) under gradient flow. The proposed method showed good linearities (r(2) >0.999), low detection limits (0.08-1.9 mug/L) and good recoveries (80.7-122%). The validated method was successfully applied for the determination of the furanic compounds in concentrated juice (mango, date, orange, pomegranate, roselle, mangosteen and soursop) and dried fruit (prune, date and apricot paste) samples.

Quantification of furanic derivatives in fortified wines by a highly sensitive and ultrafast analytical strategy based on digitally controlled microextraction by packed sorbent combined with ultrahigh pressure liquid chromatography.[Pubmed:25618358]

J Chromatogr A. 2015 Feb 13;1381:54-63.

An improved, reliable and powerful analytical strategy based on digitally controlled microextraction by packed sorbent (MEPS) combined with ultrahigh pressure liquid chromatography (UHPLC) was validated for the simultaneous identification and quantification of major furanic derivatives, namely 5-hydroxymethyl-2-furaldehyde (5HMF), 5-Methyl-2-furaldehyde (5MF), 2-furaldehyde (2F) and 2-furyl methyl ketone (2FMK), in fortified wines. To enhance the extraction efficiency of the target furanic derivates, several influencing extraction parameters, such as number of loading cycles, nature of elution solvent and elution volume, were evaluated and optimized. In addition the ability of different MEPS sorbent materials, namely C2, C8, C18, SIL, M1, R-AX, R-CX and PGC, were also tested. The optimal analytical conditions involved loading 3x200 muL of wine samples through a C8 sorbent in a MEPS syringe placed in the semi-automatic eVolH syringe followed by elution using 200 muL MeOH:H2O (95:5, v/v). The furanic derivates separation was achieved using a CORTECS UPLC((R)) C18 analytical column in an ultrafast chromatographic run (within 4 min). The method performance was assessed for dry/medium dry (D/MD) and sweet/medium sweet (S/MS) model wines in terms of selectivity, linearity, limit of detection (LOD), limit of quantitation (LOQ), accuracy, precision and matrix effect, using model wine matrix-matched calibration. Good linearity was obtained with a regression coefficient (r(2)) higher than 0.992. A good precision was attained (RSD<5%) and low LODs were achieved for D/MD (4.5-129.3 ng L(-1)) and S/MS (6.9-285.2 ng L(-1)) model wines. The quantification limits (LOQ) for D/MD model wines ranged from 14.9 to 431.0 ng L(-1), whereas for S/MS model wines range from 23.1 to 950.5 ng L(-1). The method also afforded satisfactory results in terms of accuracy, ranging from 74 to 97% for D/MD wines and between 84 and 99% for S/MS wines. The MEPS(C8)/UHPLC-PDA analytical strategy was successfully applied to analyze furanic derivates in 26 fortified Madeira wines from different types (D/MD, S/MS) and ages. The obtained results revealed the analytical strategy as a suitable tool which combines sensitivity, effectiveness, reduced analysis time and simple analytical procedure. Principal component analysis (PCA) suggested that fortified wines can be organized based on their age on PC1, which are mainly characterized by 5HMF.

Description

5-Methylfurfural is a naturally occurring substance, found in cigarette smoke condensate, licorice essential oil, stored dehydrated orange powder, baked potato flour, volatile compounds of roast beef, aroma concentrate of sponge cake. bread and in coffee, tea and cocoa. A flavoring agent.

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