Diethyl allylmalona...

Diethyl allylmalonate
Diethyl allylmalonate
Diethyl allylmalonate
Diethyl allylmalonate

Diethyl allylmalonate

Min.Order / FOB Price:Get Latest Price

1 Kilogram

FOB Price:USD 156.0000 -158.0000

  • Min.Order :1 Kilogram
  • Purity: 99%
  • Payment Terms : T/T,MoneyGram,Other

Keywords

Diethyl allylmalonate 2049-80-1 Diethyl allylmalonate

Quick Details

  • Appearance:Colorless to yellowish liquid
  • Application:Used as raw materials for medicine and pesticide intermediates
  • PackAge:25 kg/cardboard barrels
  • ProductionCapacity:50|Metric Ton|Month
  • Storage:Store in a cool, dry, ventilated place
  • Transportation:seaworthy and suitable for Refrigerated container.

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Details:

Diethyl allyl malonate is an organic intermediate that can be obtained by reacting diethyl malonate with allyl bromide. It has been reported that it can be used to prepare an insecticide for Anopheles sinensis.

In a nitrogen atmosphere, diethyl malonate (20g), anhydrous potassium carbonate (43g) and anhydrous CH3CN (200mL) were added to a 500mL three-necked round-bottom flask. Stir the reaction mixture Chemicalbook at room temperature for 10 minutes, then slowly add allyl bromide (23g) to the reaction mixture at room temperature. The reaction mixture is heated to 80 ° C for 24 hours. The reaction mixture is cooled to room temperature and filtered through a bed of diatomaceous earth. The diatomite bed was washed with acetonitrile (100mL), and the combined filtrate was concentrated to obtain diethyl allyl malonate (24g), which was a colorless liquid.

Boiling Piont 222-223 °C(lit.)
Density 1.015 g/mL at 25 °C(lit.)
Refractive Index n20/D 1.431(lit.)
Flashing Piont 160 °F
pKa 12.63±0.46(Predicted)

2,2'-Azobis(2-methylpropionitrile)/AIBN used as initiator for polymers CAS 78-67-1

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