Chloroacetamido-2,6-xylidine 2,6-Acetoxylidide, 2-chloro- (8CI) 2-Chloro-2,6-acetoxylidide
useusedaspharmaceuticalintermediates.ProductionmethodItisobtainedbythereactionof2,6-dimethylanilineandchloroacetylchloride:anhydrousbenzeneand2,6-dimethylanilinearecooledtobelow28°C,chloroacetylchlorideissChemicalbooklowlydroppedunderstirring,thetemperaturedoesnotexceed30°C,theadditioniscompleted,thestirringreactionis1h,andthenheatedandrefluxedfor8h.Coolingcrystallization,filtration,anddryingtoobtainthefinishedproduct.useusedaspharmaceuticalintermediates.ProductionmethodItisobtainedbythereactionof2,6-dimethylanilineandchloroacetylchloride:anhydrousbenzeneand2,6-dimethylanilinearecooledtobelow28°C,chloroacetylchlorideissChemicalbooklowlydroppedunderstirring,thetemperaturedoesnotexceed30°C,theadditioniscompleted,thestirringreactionis1h,andthenheatedandrefluxedfor8h.Coolingcrystallization,filtration,anddryingtoobtainthefinishedproduct.useusedaspharmaceuticalintermediates.ProductionmethodItisobtainedbythereactionof2,6-dimethylanilineandchloroacetylchloride:anhydrousbenzeneand2,6-dimethylanilinearecooledtobelow28°C,chloroacetylchlorideissChemicalbooklowlydroppedunderstirring,thetemperaturedoesnotexceed30°C,theadditioniscompleted,thestirringreactionis1h,andthenheatedandrefluxedfor8h.Coolingcrystallization,filtration,anddryingtoobtainthefinishedproduct.useusedaspharmaceuticalintermediates.ProductionmethodItisobtainedbythereactionof2,6-dimethylanilineandchloroacetylchloride:anhydrousbenzeneand2,6-dimethylanilinearecooledtobelow28°C,chloroacetylchlorideissChemicalbooklowlydroppedunderstirring,thetemperaturedoesnotexceed30°C,theadditioniscompleted,thestirringreactionis1h,andthenheatedandrefluxedfor8h.Coolingcrystallization,filtration,anddryingtoobtainthefinishedproduct.
useusedaspharmaceuticalintermediates.ProductionmethodItisobtainedbythereactionof2,6-dimethylanilineandchloroacetylchloride:anhydrousbenzeneand2,6-dimethylanilinearecooledtobelow28°C,chloroacetylchlorideissChemicalbooklowlydroppedunderstirring,thetemperaturedoesnotexceed30°C,theadditioniscompleted,thestirringreactionis1h,andthenheatedandrefluxedfor8h.Coolingcrystallization,filtration,anddryingtoobtainthefinishedproduct.useusedaspharmaceuticalintermediates.ProductionmethodItisobtainedbythereactionof2,6-dimethylanilineandchloroacetylchloride:anhydrousbenzeneand2,6-dimethylanilinearecooledtobelow28°C,chloroacetylchlorideissChemicalbooklowlydroppedunderstirring,thetemperaturedoesnotexceed30°C,theadditioniscompleted,thestirringreactionis1h,andthenheatedandrefluxedfor8h.Coolingcrystallization,filtration,anddryingtoobtainthefinishedproduct.useusedaspharmaceuticalintermediates.ProductionmethodItisobtainedbythereactionof2,6-dimethylanilineandchloroacetylchloride:anhydrousbenzeneand2,6-dimethylanilinearecooledtobelow28°C,chloroacetylchlorideissChemicalbooklowlydroppedunderstirring,thetemperaturedoesnotexceed30°C,theadditioniscompleted,thestirringreactionis1h,andthenheatedandrefluxedfor8h.Coolingcrystallization,filtration,anddryingtoobtainthefinishedproduct.
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